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20320-59-6

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Basic Information
CAS No.: 20320-59-6
Name: Diethyl(phenylacetyl)malonate
Article Data: 13
Molecular Structure:
Molecular Structure of 20320-59-6 (Diethyl(phenylacetyl)malonate)
Formula: C15H18O5
Molecular Weight: 278.305
Synonyms: phenylacetyl-malonic acid diethyl ester;Phenylacetyl-malonsaeure-diaethylester;Phenylacetylmalonsaeurediethylester;Phenylacetylmalonic acid ethylester;
Density: 1.148±0.06 g/cm3(Predicted)
Boiling Point: 120 °C(Press: 0.01 Torr)
PSA: 69.67000
LogP: 1.54060
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Conditions
ConditionsYield
Stage #1: diethyl malonate With ethanol; magnesium In tetrachloromethane; toluene for 1h; Heating;
Stage #2: phenylacetyl chloride In tetrachloromethane; toluene at 20℃; for 1h;		90%
With chloroform; magnesium
With magnesium
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sodium diethylmalonate

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phenylacetyl chloride

A

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ConditionsYield
...Expand

diethyl ethoxymagnesium malonate

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Conditions
ConditionsYield
With diethyl ether; ethanol
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Conditions
ConditionsYield
With sodium dann mit Phenylessigsaeurechlorid versetzen;

C7H11O4(1-)*C2H5O(1-)*Mg(2+)

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20320-59-6

diethyl 2-(2-phenylacetyl)malonate

Conditions
ConditionsYield
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diethyl acetylmalonate

20320-59-6

diethyl 2-(2-phenylacetyl)malonate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 24 percent / NH2NH2 / ethanol / 3 h / Heating
2.1: Mg; EtOH / CCl4; toluene / 1 h / Heating
2.2: 90 percent / CCl4; toluene / 1 h / 20 °C
View Scheme
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ethyl 3-amino-2-ethoxycarbonyl-2-butenoate

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diethyl 2-(2-phenylacetyl)malonate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 14 percent / 80 percent NH2NH2 / ethanol / 3 h / Heating
2.1: Mg; EtOH / CCl4; toluene / 1 h / Heating
2.2: 90 percent / CCl4; toluene / 1 h / 20 °C
View Scheme
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cycl-isopropylidene malonate

20320-59-6

diethyl 2-(2-phenylacetyl)malonate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 3.5 h / 20 °C / Cooling with ice
2: 3 h / Reflux
View Scheme
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phenylacetyl chloride

20320-59-6

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Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 3.5 h / 20 °C / Cooling with ice
2: 3 h / Reflux
View Scheme
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ethanol

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diethyl 2-(2-phenylacetyl)malonate

Conditions
ConditionsYield
for 3h; Reflux;
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