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223437-11-4

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Basic Information
CAS No.: 223437-11-4
Name: 1-BUTYL-1-METHYLPYRROLIDINIUM BIS(TRIFLUOROMETHYLSULFONYL)IMIDE
Article Data: 53
Molecular Structure:
Molecular Structure of 223437-11-4 (1-BUTYL-1-METHYLPYRROLIDINIUM BIS(TRIFLUOROMETHYLSULFONYL)IMIDE)
Formula: C11H20F6N2O4S2
Molecular Weight: 422.413
Synonyms: N-BUTYL-N-METHYLPYRROLIDINIUM BIS(TRIFLUOROMETHANESULFONYL)IMIDE;1-BUTYL-1-METHYLPYRROLIDINIUM BIS(TRIFLUOROMETHANESULFONYL)IMIDE;1-BUTYL-1-METHYLPYRROLIDINIUM BIS(TRIFLUOROMETHYLSULFONYL)IMIDE;1-BUTYL-METHYLPYRROLIDINIUM BIS(TRIFLUOROMETHYLSULFONYL)IMIDE;1-n-Butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide, 98%
Density: g/cm3
Melting Point: -6°C
Boiling Point: 190.5°Cat760mmHg
Flash Point: 69°C
Solubility: Miscible with methanol, acetonitrile, acetone, dichloromethane and dimethyl sulfoxide. Immiscible with water and diethyl ether.
Hazard Symbols:
Risk Codes: 36/37/38
Safety:
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 26
WGK Germany 3
F 10-21
PSA: 85.04000
LogP: 5.20660
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Synthetic route

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223437-11-4

1-butyl-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide

Conditions
ConditionsYield
In methanol; acetone at 20℃; for 1h; Large scale;99%
90076-65-6

bis(trifluoromethane)sulfonimide lithium

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N-methyl-N-butylpyrrolidinium bromide

223437-11-4

1-butyl-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide

Conditions
ConditionsYield
In dichloromethane; water98%
With water In dichloromethane95%
In dichloromethane at 20℃; for 72h; Inert atmosphere;95.8%

1-n-butyl-1-methylpyrrolidinium hydroxide

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bis(trifluoromethanesulfonyl)amide

223437-11-4

1-butyl-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide

Conditions
ConditionsYield
In water pH=6 - 7;94%
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1-butyl-3-methylimidazolium chloride

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bis(trifluoromethane)sulfonimide lithium

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1-butyl-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide

Conditions
ConditionsYield
In dichloromethane at 20℃; for 72h; Inert atmosphere;93%
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bis(trifluoromethane)sulfonimide lithium

1-butyl-1-methylpyrrolidinium chloride

223437-11-4

1-butyl-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide

Conditions
ConditionsYield
In dichloromethane at 120℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox;90%
In dichloromethane at 20℃; for 24h;89%
In water at 20℃; for 17h;88%
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1-n-Butyl-1-methylpyrrolidinium iodide

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bis(trifluoromethane)sulfonimide lithium

223437-11-4

1-butyl-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide

Conditions
ConditionsYield
With water at 20℃; for 3h; Substitution;88%
110-52-1

1,4-dibromo-butane

110-68-9

N-n-butyl-N-methylamine

90076-65-6

bis(trifluoromethane)sulfonimide lithium

223437-11-4

1-butyl-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide

Conditions
ConditionsYield
Stage #1: 1,4-dibromo-butane; N-n-butyl-N-methylamine With potassium carbonate In water at 120℃; for 0.333333h; Autoclave; Microwave irradiation; Green chemistry;
Stage #2: bis(trifluoromethane)sulfonimide lithium In water at 20℃; for 1h; Green chemistry;		83%
...Expand
120-94-5

1-Methylpyrrolidine

223437-11-4

1-butyl-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: H2O
View Scheme
Multi-step reaction with 2 steps
1: 90 percent / 24 h / 20 °C
2: H2O / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: 92 percent / propan-2-ol / 24 h / Heating
2: 86 percent / CH2Cl2 / 72 h
View Scheme
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lithium trifluoromethanesulfonate

93457-69-3

N-methyl-N-butylpyrrolidinium bromide

223437-11-4

1-butyl-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide

Conditions
ConditionsYield
Inert atmosphere;
120-94-5

1-Methylpyrrolidine

109-69-3

n-Butyl chloride

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bis(trifluoromethane)sulfonimide lithium

223437-11-4

1-butyl-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide

Conditions
ConditionsYield
Stage #1: 1-Methylpyrrolidine; n-Butyl chloride In isopropyl alcohol
Stage #2: bis(trifluoromethane)sulfonimide lithium In dichloromethane
...Expand
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    223437-11-4

    1-Butyl-1-methylpyrrolidinium Bis(trifluoromethanesulfonyl)imide

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     China (Mainland)  |  Contact Details

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