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CAS No.: | 24748-23-0 |
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Name: | 3,6,9-TRIETHYL-3,6,9-TRIMETHYL-1,4,7-TRIPEROXYNONANE |
Article Data: | 5 |
Molecular Structure: | |
Formula: | C12H24O6 |
Molecular Weight: | 264.319 |
Synonyms: | 1,2,4,5,7,8-Hexoxonane,3,6,9-triethyl-3,6,9-trimethyl;3,6,9-Triethyl-3,6,9-trimethyl-1,4,7-triperoxynonane;3,6,9-triethyl-3,6,9-trimethyl-1,2,4,5,7,8-hexoxonane;3,6,9-Triethyl-3,6,9-trimethyl-1,4,7-triperoxonane; |
Density: | 0.875 |
Melting Point: | -20oC |
Boiling Point: | 246.6oC at 760 mmHg |
Flash Point: | 58oC |
Solubility: | 13.1mg/L at 20℃ |
Hazard Symbols: | Xi,O |
Risk Codes: | R38; R43; R65; R7 |
PSA: | 55.38000 |
LogP: | 3.22320 |
Conditions | Yield |
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With sulfuric acid; dihydrogen peroxide at -1 - 1℃; for 2.25h; | A 18.9% B 5.9% C 17.6% |
butanone
3,6,9-triethyl-3,6,9-trimethyl-[1,2,4,5,7,8]hexoxonane
Conditions | Yield |
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With sulfuric acid; dihydrogen peroxide | |
With sulfuric acid; dihydrogen peroxide at 0℃; for 48h; |
sulfuric acid
dihydrogen peroxide
butanone
A
3,6,9-triethyl-3,6,9-trimethyl-[1,2,4,5,7,8]hexoxonane
butanone
A
3,6,9-triethyl-3,6,9-trimethyl-[1,2,4,5,7,8]hexoxonane
B
methyl ethyl ketone peroxide
Conditions | Yield |
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Stage #1: butanone; nitric acid In 2-methylundecane; water; acetic acid at 15 - 18℃; Stage #2: With dihydrogen peroxide In 2-methylundecane; water; acetic acid at 14 - 18℃; for 1h; |
3,6,9-triethyl-3,6,9-trimethyl-[1,2,4,5,7,8]hexoxonane
4-tert-Butylstyrene
Conditions | Yield |
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With iron(III) trifluoromethanesulfonate In 1,4-dioxane at 80℃; for 12h; Heck Reaction; | 81% |