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CAS No.: | 2618-96-4 |
---|---|
Name: | Dibenzenesulfonimide |
Article Data: | 27 |
Molecular Structure: | |
Formula: | C12H11NO4S2 |
Molecular Weight: | 297.356 |
Synonyms: | Bis benzene sulphonylimide (BBI);Dibenzenesulfonamide(6CI,7CI,8CI);Bis(phenylsulfonyl)amine;Di(benzenesulfonyl)amine; |
EINECS: | 220-051-4 |
Density: | 1.418 g/cm3 |
Melting Point: | 150-155 ºC |
Boiling Point: | 480.6 ºC at 760 mmHg |
Flash Point: | 244.5 ºC |
Solubility: | Slightly soluble in water,well soluble in alkaline solution |
Appearance: | white powder |
Safety: | 22-24/25 |
PSA: | 97.07000 |
LogP: | 3.90630 |
N-nitrobenzenesulfonimide
dibenzenesulfonamide
Conditions | Yield |
---|---|
With water | 100% |
N-fluorobis(benzenesulfon)imide
A
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical
B
dibenzenesulfonamide
Conditions | Yield |
---|---|
With 1,1,1,2,2,2-hexamethyldisilane; copper(l) chloride In acetonitrile at 70℃; for 1h; Schlenk technique; Inert atmosphere; | A 86% B 100% |
tert-butyl 2-phenoxyethaneperoxoate
N-fluorobis(benzenesulfon)imide
A
dibenzenesulfonamide
B
fluoromethyl phenyl ether
Conditions | Yield |
---|---|
In [D3]acetonitrile at 110℃; for 0.0833333h; Inert atmosphere; Sealed tube; | A 94% B n/a |
Conditions | Yield |
---|---|
With sodium hydroxide at 60℃; Concentration; | 93% |
With sodium hydroxide In isopropyl alcohol at 50 - 55℃; for 2h; pH=8 - 10; | 89% |
With dmap; triethylamine In dichloromethane for 2h; Reflux; | 80% |
N-chloro-N-(benzenesulfonyl)benzenesulfonamide
silver(I) trifluoromethanethiolate
A
dibenzenesulfonamide
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 2h; | A n/a B 74% |
2,2-dimethyl-N-(4-methylphenyl)propanamide
N-fluorobis(benzenesulfon)imide
A
N-(4-((N-( phenylsulfonyl)phenylsulfonamido)methyl)phenyl)pivalamide
B
dibenzenesulfonamide
Conditions | Yield |
---|---|
With palladium diacetate In 1,2-dichloro-ethane at 90℃; for 1.5h; | A 73% B 17% |
Conditions | Yield |
---|---|
With hydrogenchloride In acetone for 2h; | 72% |
Conditions | Yield |
---|---|
In acetone at 20℃; for 2h; Product distribution; other p-substituted arenesulfinic acids and their sodium salts, other N-sodio-N-chloroarenesulfonamides; | 64% |
In acetone at 20℃; for 2h; | 64% |
N-fluorobis(benzenesulfon)imide
dibenzenesulfonamide
Conditions | Yield |
---|---|
With copper(l) chloride In acetonitrile at 70℃; for 1h; Schlenk technique; Inert atmosphere; | 62% |
N-(4,5-dimethyl-[1,1'-biphenyl]-2-yl)pivalamide
N-fluorobis(benzenesulfon)imide
A
N-(4-methyl-5-((N-(phenylsulfonyl)phenylsulfonamido)methyl)biphenyl-2-yl)pivalamide
B
dibenzenesulfonamide
Conditions | Yield |
---|---|
With palladium diacetate; sodium hydrogencarbonate In 1,2-dichloro-ethane at 90℃; for 13h; | A 58% B 15% |
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EINECS of Dibenzenesulfonimide (CAS NO.2618-96-4): 220-051-4
Empirical Formula: C12H11NO4S2
Molecular Weight: 297.35 g/mol
Index of Refraction: 1.61
Density: 1.418 g/cm3
Flash Point: 244.5 °C
Melting point: 150-155 °C
Enthalpy of Vaporization: 74.52 kJ/mol
Boiling Point: 480.6 °C at 760 mmHg
Vapour Pressure: 2.13E-09 mmHg at 25 °C
Structure of Dibenzenesulfonimide (CAS NO.2618-96-4):
IUPAC Name: N-(Benzenesulfonyl)benzenesulfonamide
Dibenzenesulfonimide (CAS NO.2618-96-4) can be used for electroplating additive intermediate for the preparation of electroless nickel plating brightener with a good soft and light effect.
Safety Statements: 22-24/25
S22:Do not breathe dust.
S24/25:Avoid contact with skin and eyes.
Dibenzenesulfonimide , its cas register number is 2618-96-4. It also can be N-(Phenylsulphonyl)benzenesulphonamide ; Bis(benzene sulphonyl)-imide ; and BBI .