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Basic Information
CAS No.: 2842-44-6
Name: N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE
Molecular Structure:
Molecular Structure of 2842-44-6 (N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE)
Formula: C10H15 N O
Molecular Weight: 165.235
Synonyms: Ethanol,2-(N-methyl-p-toluidino)- (7CI,8CI); 2-(N-Methyl-N-4-tolylamino)ethanol;FirstCure MHPT; N-(2-Hydroxyethyl)-N-methyl-p-toluidine;N-Methyl-N-(2-hydroxyethyl)-p-toluidine
Density: 1.047g/cm3
Boiling Point: 298.1°Cat760mmHg
Flash Point: 148.8°C
PSA: 23.47000
LogP: 1.42350
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2-(methyl(p-tolyl)amino)ethan-1-ol

Conditions
ConditionsYield
With N-methyl-1-(thiophen-2-yl)methanamine; tris(triphenylphosphine)ruthenium(II) chloride; 1,1'-bis(dicyclohexylphosphinocyclopentadienyl)iron; potassium tert-butylate In 1,4-dioxane at 150℃; for 20h;91%
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2842-44-6

2-(methyl(p-tolyl)amino)ethan-1-ol

Conditions
ConditionsYield
With copper(l) iodide; sodium hydroxide In water; dimethyl sulfoxide at 90℃; for 16h; Buchwald-Hartwig Coupling; Sealed tube; Inert atmosphere;82%
87-72-9, 608-45-7, 608-46-8, 608-47-9, 2460-44-8, 6748-95-4, 6763-34-4, 7261-26-9, 7283-06-9, 7283-07-0, 7296-55-1, 7296-56-2, 7296-58-4, 7296-59-5, 7296-60-8, 7296-61-9, 7296-62-0, 7322-30-7, 10257-31-5, 10257-32-6, 10257-33-7, 10257-34-8, 10257-35-9, 19982-83-3, 20242-88-0, 28697-53-2, 36562-42-2, 41546-41-2, 89299-64-9, 107655-34-5, 115794-06-4, 115794-07-5, 130550-15-1, 130606-21-2

D-Xylose

623-08-5

N-methyl-p-toluidine

2842-44-6

2-(methyl(p-tolyl)amino)ethan-1-ol

Conditions
ConditionsYield
With [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); acetic acid; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane at 150℃; for 16h; Inert atmosphere; Glovebox; chemoselective reaction;75%
hydriodide of methyl-<β-oxy-ethyl>-p-toluidine

hydriodide of methyl-<β-oxy-ethyl>-p-toluidine

2842-44-6

2-(methyl(p-tolyl)amino)ethan-1-ol

Conditions
ConditionsYield
With potassium carbonate
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N-(4-methylphenyl)-N-methylglycine ethyl ester

2842-44-6

2-(methyl(p-tolyl)amino)ethan-1-ol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; Inert atmosphere;

3-{2-[methyl(4'-methylphenyl)amino]ethyl}-4-oxo-3H,4H-imidazo[1,5-d][1,2,3,5]tetrazine-8-carboxamide

A

C10H14NO4P(2-)

B

2842-44-6

2-(methyl(p-tolyl)amino)ethan-1-ol

C

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5-Aminoimidazole-4-carboxamide

Conditions
ConditionsYield
With disodium hydrogenphosphate; citric acid In dimethyl sulfoxide at 37℃; Kinetics; pH-value;
...Expand
2842-44-6

2-(methyl(p-tolyl)amino)ethan-1-ol

N-(2-iodoethyl)-N-methyl-4-methylaniline

Conditions
ConditionsYield
With 1H-imidazole; iodine; triphenylphosphine In toluene at 100℃; for 28h; Inert atmosphere;79%
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2-(methyl(p-tolyl)amino)ethan-1-ol

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benzyl bromide

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Conditions
ConditionsYield
Stage #1: 2-(methyl(p-tolyl)amino)ethan-1-ol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.5h; Inert atmosphere;
Stage #2: benzyl bromide In tetrahydrofuran; mineral oil at 0 - 20℃; Inert atmosphere;
2842-44-6

2-(methyl(p-tolyl)amino)ethan-1-ol

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Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 1H-imidazole; triphenylphosphine; iodine / toluene / 28 h / 100 °C / Inert atmosphere
2.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 1.08 h / 0 - 20 °C / Inert atmosphere
2.2: 18 h / 80 °C / Inert atmosphere
View Scheme
2842-44-6

2-(methyl(p-tolyl)amino)ethan-1-ol

diethyl 1,6-dimethyl-2,3-dihydroquinoline-4,4(1H)-dicarboxylate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 1H-imidazole; triphenylphosphine; iodine / toluene / 28 h / 100 °C / Inert atmosphere
2.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 1.08 h / 0 - 20 °C / Inert atmosphere
2.2: 18 h / 80 °C / Inert atmosphere
3.1: copper(II) 2-ethylhexanoate; N-ethyl-N,N-diisopropylamine / toluene / 19 h / 120 °C
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    Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop producing and selling high quality intermediates, Fine chemicals and Specialty Chemicals.

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    Characteristic N-(2-Hydroxyethyl)-N-Methyl-4-Toluidine Appearance Light yellow solid Formula Weight 165.23 Structural Formula Appea

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    2842-44-6

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    Wuhan Vanz Pharm Inc. is a manufacturer&trading company.

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