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Basic Information
| CAS No.: | 3077-85-8 |
|---|---|
| Name: | 3-nitrocarbazole |
| Article Data: | 63 |
| Molecular Structure: | |
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| Formula: | C12H8 N2 O2 |
| Molecular Weight: | 212.208 |
| Synonyms: | Carbazole,3-nitro- (6CI,7CI,8CI); 3-Nitro-9H-carbazole; 3-Nitrocarbazole; INF 51; NSC67708 |
| Density: | 1.435g/cm3 |
| Melting Point: | 216-217℃ |
| Boiling Point: | 448.6°Cat760mmHg |
| Flash Point: | 225.1°C |
| PSA: | 61.61000 |
| LogP: | 3.75250 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With aluminium trichloride In dichloromethane Ambient temperature; | A 98% B 2% |
| With aluminium trichloride In dichloromethane Ambient temperature; | A 98% B n/a |
| With trifluorormethanesulfonic acid; trifluoroacetic acid In dichloromethane Ambient temperature; | A 93% B 5% |
| With trifluorormethanesulfonic acid In dichloromethane Ambient temperature; | A 84% B 15% |
- 89672-04-8
1-(3-nitrocarbazol-9-yl)ethanone
- 3077-85-8
3-Nitro-carbazol
Conditions
| Conditions | Yield |
|---|---|
| With 1,8-diazabicyclo[5.4.0]undec-7-ene In methanol for 1h; Product distribution; Further Variations:; Solvents; reaction time; Heating; | 96% |
- 92683-72-2
N-(p-toluenesulfonyl)-3-nitrocarbazole
- 3077-85-8
3-Nitro-carbazol
Conditions
| Conditions | Yield |
|---|---|
| With 1,8-diazabicyclo[5.4.0]undec-7-ene In methanol for 1h; Product distribution; Further Variations:; Solvents; reaction time; Heating; | 96% |
- 3077-85-8
3-Nitro-carbazol
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: C14H16N2O2 With dichloro[1,3-bis(2-methylphenyl)-2-imidazolidinylidene](benzylidene) (tricyclohexylphosphine) ruthenium(II) In ethyl acetate at 70℃; under 760.051 Torr; for 2h; Sealed tube; Inert atmosphere; Stage #2: With oxygen In ethyl acetate at 70℃; under 760.051 Torr; for 24h; Sealed tube; | 95% |
- 50823-86-4
6-nitro-2,3,4,9-tetrahydro-1H-carbazole
- 3077-85-8
3-Nitro-carbazol
Conditions
| Conditions | Yield |
|---|---|
| With copper(II) choride dihydrate In dimethyl sulfoxide at 100℃; for 24h; | 90% |
| With chloranil In xylene for 6h; Heating; | 35% |
| With chloranil; xylene |
Conditions
| Conditions | Yield |
|---|---|
| With nitric acid; acetic acid at 60℃; | 89.68% |
| With uronium nitrate In acetic acid for 10h; | 86% |
| With nitric acid; acetic acid at 65℃; for 6h; | 77% |
Conditions
| Conditions | Yield |
|---|---|
| With silver hexafluoroantimonate; chloro[di(1-adamantyl)-2-dimethylaminophenylphosphine]gold(I) In methanol at 0 - 80℃; for 24h; Inert atmosphere; | 85% |
Conditions
| Conditions | Yield |
|---|---|
| With air; potassium carbonate; Trimethylacetic acid; palladium diacetate at 110℃; for 14h; | 76% |
| With palladium diacetate; potassium carbonate; Trimethylacetic acid Heating; |
- 91330-60-8
2-azido-5-nitrobiphenyl
- 3077-85-8
3-Nitro-carbazol
Conditions
| Conditions | Yield |
|---|---|
| In decalin at 161℃; for 2h; | 73% |
- 1058740-47-8
9-(2-phenylsulphonyl-ethyl)-3-nitro-9H-carbazole
- 3077-85-8
3-Nitro-carbazol
Conditions
| Conditions | Yield |
|---|---|
| With potassium tert-butylate In tetrahydrofuran at 20 - 50℃; for 8h; | 73% |
Raw Materials
Downstream Products
