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CAS No.: | 3128-32-3 |
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Name: | 2-Propenoic acid, hydrazide |
Article Data: | 4 |
Molecular Structure: | |
Formula: | C3H6N2O |
Molecular Weight: | 86.0934 |
Synonyms: | acrylic acid hydrazide;acryloyl hydrazine;Acrylsaeure-hydrazid;2-methyleneacethydrazide;amino acrylamide;2-Propenoic acid,hydrazide;Acryloylhydrazin;acrylhydrazide; |
PSA: | 58.61000 |
LogP: | 0.70290 |
acrylic acid cyanomethyl ester
acryloyl hydrazine
Conditions | Yield |
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With chloroform; hydrazine hydrate |
potassium acrylate
acryloyl hydrazine
Conditions | Yield |
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(i) Py, ClCO2Et, CH2Cl2, (ii) N2H4*H2O; Multistep reaction; |
acryloyl hydrazine
Conditions | Yield |
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With dichloromethane; hydrazine hydrate |
Conditions | Yield |
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With hydrazine hydrate In ethanol Microwave irradiation; | |
With hydrazine hydrate In tetrahydrofuran at 80℃; for 1h; |
Conditions | Yield |
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In ethanol at 80℃; Inert atmosphere; | 60% |
Conditions | Yield |
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palladium In water; benzene |
Conditions | Yield |
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With 2,2'-azobisisobutyronitrile In N,N-dimethyl-formamide refluxing anhyd. Cd-salt with acryloyl hydrazine in DMF and 2,2'-azobisisobutyronitrile as initiator for 8 h; poured into a large excess of distilled water containing dilute HCl, filtered, washed with water, dried in a vac. oven at 40°C for several days; elem. anal.; |
Conditions | Yield |
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With 2,2'-azobisisobutyronitrile In N,N-dimethyl-formamide refluxing anhyd. Fe-salt with acryloyl hydrazine in DMF and 2,2'-azobisisobutyronitrile as initiator for 8 h; poured into a large excess of distilled water containing dilute HCl, filtered, washed with water, dried in a vac. oven at 40°C for several days; elem. anal.; |
Conditions | Yield |
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With 2,2'-azobisisobutyronitrile In N,N-dimethyl-formamide refluxing anhyd. Cu-salt with acryloyl hydrazine in DMF and 2,2'-azobisisobutyronitrile as initiator for 8 h; poured into a large excess of distilled water containing dilute HCl, filtered, washed with water, dried in a vac. oven at 40°C for several days; elem. anal.; |
Conditions | Yield |
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With 2,2'-azobisisobutyronitrile In N,N-dimethyl-formamide refluxing anhyd. UO2-salt with acryloyl hydrazine in DMF and 2,2'-azobisisobutyronitrile as initiator for 8 h; poured into a large excess of distilled water containing dilute HCl, filtered, washed with water, dried in a vac. oven at 40°C for several days; elem. anal.; |