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| CAS No.: | 320-60-5 |
|---|---|
| Name: | 2,4-Dichlorobenzotrifluoride |
| Molecular Structure: | |
|
|
|
| Formula: | C7H3Cl2F3 |
| Molecular Weight: | 215.002 |
| Synonyms: | Toluene,2,4-dichloro-a,a,a-trifluoro- (8CI);1,3-Dichloro-4-(trifluoromethyl)benzene;2,4-Dichloro(trifluoromethyl)benzene;2,4-Dichloro-1-(trifluoromethyl)benzene;2,4-Dichloro-a,a,a-trifluorotoluene;2,4-Dichlorobenzotrifluoride; |
| EINECS: | 206-278-1 |
| Density: | 1.464 g/cm3 |
| Melting Point: | -26 °C |
| Boiling Point: | 193.2 °C at 760 mmHg |
| Flash Point: | 78.1 °C |
| Solubility: | 8.67mg/L at 25℃ |
| Appearance: | colourless clear liquid |
| Hazard Symbols: |
 C, Xi
|
| Risk Codes: | 34 |
| Safety: | 26-27-36/37/39-45 |
| Transport Information: | UN 3265 8/PG 2 |
| PSA: | 0.00000 |
| LogP: | 4.01220 |
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- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 852475-26-4MC1568
- 7664-39-3
hydrogen fluoride
- 13014-18-1
2,4-dichlorobenzotrichloride
- 320-60-5
2,4-dichloro-benzotrifluoride
| Conditions | Yield |
|---|---|
| at 140 - 150℃; | |
| at 140 - 150℃; |
- 13014-18-1
2,4-dichlorobenzotrichloride
- 320-60-5
2,4-dichloro-benzotrifluoride
| Conditions | Yield |
|---|---|
| With hydrogen fluoride at 110℃; under 11251.1 - 12751.3 Torr; Pressure; Temperature; | |
| With hydrogen fluoride at 110℃; under 11251.1 - 12751.3 Torr; Temperature; Pressure; | |
| With hydrogen fluoride at 110℃; under 11251.1 - 12751.3 Torr; Temperature; Pressure; Green chemistry; |
- 462-06-6
fluorobenzene
- 320-60-5
2,4-dichloro-benzotrifluoride
- 656803-77-9
2,4-dichloro-1-[dichloro-(4-fluorophenyl)methyl]benzene
| Conditions | Yield |
|---|---|
| With aluminum (III) chloride In 1,2-dichloro-ethane at 0 - 5℃; for 5h; | 100% |
| With aluminium trichloride In 1,2-dichloro-ethane at 0℃; for 5h; | |
| With aluminum (III) chloride In 1,2-dichloro-ethane at 0 - 5℃; for 5h; |
- 320-60-5
2,4-dichloro-benzotrifluoride
- 5720-05-8
4-methylphenylboronic acid
- 1419798-74-5
3-chloro-4'-methyl-4-(trifluoromethyl)biphenyl
| Conditions | Yield |
|---|---|
| With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 80℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere; | 97% |
- 320-60-5
2,4-dichloro-benzotrifluoride
- 17933-03-8
m-tolylboronic acid
- 1419798-73-4
3-chloro-3'-methyl-4-(trifluoromethyl)biphenyl
| Conditions | Yield |
|---|---|
| With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 80℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere; | 95% |
- 320-60-5
2,4-dichloro-benzotrifluoride
- 16419-60-6
2-Methylphenylboronic acid
- 1419798-72-3
3'-chloro-2-methyl-4'-(trifluoromethyl)biphenyl
| Conditions | Yield |
|---|---|
| With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 80℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere; | 93% |
| Conditions | Yield |
|---|---|
| Stage #1: 2,4-dichloro-benzotrifluoride; (R)-S-methyl-S-phenylsulfoximine With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate In toluene at 20℃; for 0.5h; Stage #2: In toluene at 135℃; for 1.5h; microwave irradiation; Further stages.; | 92% |
| Conditions | Yield |
|---|---|
| With sulfuric acid; potassium nitrate at 15 - 20℃; for 18.5h; | 87% |
| With sulfuric acid; nitric acid | |
| Nitrierung; | |
| Nitrierung; |
- 75-77-4
chloro-trimethyl-silane
- 320-60-5
2,4-dichloro-benzotrifluoride
- 871254-70-5
[2,6-dichloro-3-(trifluoromethyl)phenyl]trimethylsilane
| Conditions | Yield |
|---|---|
| With n-butyllithium In tetrahydrofuran; hexane at -75℃; | 82% |
- 124-38-9
carbon dioxide
- 320-60-5
2,4-dichloro-benzotrifluoride
- 25922-41-2
2,6-dichloro-3-(trifluoromethyl)benzoic acid
| Conditions | Yield |
|---|---|
| With n-butyllithium In tetrahydrofuran; hexane at -75℃; | 75% |
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Chemistry
IUPAC Name of o-Aminotrifluoromethylbenzene (320-60-5): 2,4-dichloro-1-(trifluoromethyl)benzene
Product Categories: Chlorine Compounds;Fluorine Compounds
Molecular Formula: C7H3Cl2F3
Molecular Weight: 214.99993
Appearance:colourless clear liquid
Surface Tension: 27.4 dyne/cm
Index of Refraction: 1.47
odor: penetrating
BRN: 2098743
Melting Point: -26 °C
Density: 1.464 g/cm3
Flash Point: 78.1 °C
Enthalpy of Vaporization: 41.18 kJ/mol
Boiling Point: 193.2 °C at 760 mmHg
Vapour Pressure: 0.656 mmHg at 25 °C
CAS DataBase Reference:320-60-5(CAS DataBase Reference)
NIST Chemistry Reference:320-60-5(NIST)
EPA Substance Registry System:320-60-5(EPA Substance)
Synonyms of o-Aminotrifluoromethylbenzene (320-60-5):
2,4-dichloro-1-(trifluoromethyl)-benzen;2,4-dichloro-alpha,alpha,alpha-trifluoro-toluen;2,4-Dichlorotrifluoromethylbenzene;1,3-DICHLORO-4-(TRIFLUOROMETHYL)BENZENE;2,4-Dichloro-1-(triflouromethyl)-benzene;2,4-DICHLORO-1-(TRIFLUOROMETHYL)BENZENE;2,4-DCBTF;2,4-DICHLORO-A,A,A-TRIFLUOROTOLUENE; 2,4-Dichlorobenzotrifluoride;2,4-Dichloro-1-(trifluoromethyl)benzene;Benzene, 2,4-dichloro-1-(trifluoromethyl)-;2,4-Dichloro-alpha,alpha,alpha-trifluorotoluene;Toluene, 2,4-dichloro-alpha,alpha,alpha-trifluoro-
Uses
o-Aminotrifluoromethylbenzene (320-60-5) is raw material of madinitramine which is weedicide used in the dry soil.
Production
o-Aminotrifluoromethylbenzene(320-60-5) is synthesized by the method of chloridizing parachlorotoluene.
Safety Profile
Safety Information of o-Aminotrifluoromethylbenzene(320-60-5):
Hazard Codes:C 
,Xi 
Risk Statements:34
34:Causes burns
Safety Statements:26-27-36/37/39-45
26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
27:Take off immediately all contaminated clothing
36/37/39:Wear suitable protective clothing, gloves and eye/face protection
45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
RIDADR:UN 3265 8/PG 2
WGK Germany:2
RTECS:CZ5566877
Hazard Note:Corrosive
TSCA:T
HazardClass:8
PackingGroup:III