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3524-68-3

Basic Information
CAS No.: 3524-68-3
Name: Pentaerythritol triacrylate
Article Data: 8
Molecular Structure:
Molecular Structure of 3524-68-3 (Pentaerythritol triacrylate)
Formula: C14H18O7
Molecular Weight: 298.293
Synonyms: 2-Propenoicacid, 2-(hydroxymethyl)-2-[[(1-oxo-2-propenyl)oxy]methyl]-1,3-propanediyl ester(9CI);Acrylic acid, triester with pentaerythritol (7CI,8CI);Pentaerythritol,triacrylate (8CI);A-TMM 3OHV122;A-TMMA;Agi Syn 2884;Aronix M 30;Aronix M305;Aronix M 306;Gafgard 233;Hipenny;Kayarad PET 30;Light Acrylate PE 3A;Light Ester PE 3A;M 305;NK Ester A-TMN 3LM-N;NK Ester TMM 50T;NewfrontierPET 3;P 300;P 300 (acrylate);PE 3A;PET 30;PETA;PETIA;Pentaerythrityltriacrylate;SR 444;SR 444C;SR 444D;Sartomer 444;Sartomer SR 444;SetaluxUV 2242;Tetramethylolmethane triacrylate;Viscoat 300PETA;2-Propenoic acid,1,1'-[2-(hydroxymethyl)-2-[[(1-oxo-2-propen-1-yl)oxy]methyl]-1,3-propanediyl]ester;
EINECS: 222-540-8
Density: 1.179 g/cm3
Melting Point: 15℃
Boiling Point: 427.9 ºC at 760 mmHg
Flash Point: 153.5 °C
Solubility: insoluble in water
Appearance: viscous yellow liquid
Hazard Symbols: IrritantXi
Risk Codes: 36/38-43
Safety: 39
Transport Information: UN 3265
PSA: 99.13000
LogP: 0.15270
Synthetic route
115-77-5

Pentaerythritol

79-10-7

acrylic acid

3524-68-3

pentaerythritol triacrylate

Conditions
ConditionsYield
Stage #1: Pentaerythritol; acrylic acid With IR-120 strong acid type ion exchange resin at 100℃; for 0.5h;
Stage #2: In benzene at 100℃; for 3h; Temperature;
88%
1471-17-6

pentaerythritol triallyl ether

3524-68-3

pentaerythritol triacrylate

Conditions
ConditionsYield
With triethylamine; trichlorophosphate In (2S)-N-methyl-1-phenylpropan-2-amine hydrate
115-77-5

Pentaerythritol

3121-61-7

2-methoxyethyl acrylate

A

2,2-bis(hydroxymethyl)-1,3-propanediyl diacrylate

B

4986-89-4

pentaerythritol tetraacrylate

C

3524-68-3

pentaerythritol triacrylate

Conditions
ConditionsYield
With zinc diacetate; oxygen; 4-methoxy-phenol; 1,8-diazabicyclo[5.4.0]undec-7-ene at 105 - 120℃; for 5h; Reagent/catalyst; Inert atmosphere; Overall yield = 48 %;
115-77-5

Pentaerythritol

3121-61-7

2-methoxyethyl acrylate

A

4986-89-4

pentaerythritol tetraacrylate

B

3524-68-3

pentaerythritol triacrylate

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane; zinc diacetate; oxygen; 4-methoxy-phenol at 105 - 120℃; under 130 - 760 Torr; for 30h; Inert atmosphere; Overall yield = 96 %;
With 1,4-diaza-bicyclo[2.2.2]octane; zinc diacetate; oxygen; 4-methoxy-phenol at 105 - 120℃; under 130 - 760 Torr; for 30h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Overall yield = 88 %;
With 1,4-diaza-bicyclo[2.2.2]octane; zinc diacetate; oxygen; 4-methoxy-phenol at 105 - 120℃; under 130 - 760 Torr; for 30h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Overall yield = 88 %;
108-30-5

succinic acid anhydride

3524-68-3

pentaerythritol triacrylate

C19H22O11

Conditions
ConditionsYield
With triphenylphosphine at 90℃; for 8h;99.9%
542-92-7

cyclopenta-1,3-diene

3524-68-3

pentaerythritol triacrylate

C29H36O7

Conditions
ConditionsYield
In toluene for 3h; Diels-Alder Cycloaddition; Inert atmosphere; Schlenk technique;97%
3524-68-3

pentaerythritol triacrylate

polymer resin; monomer(s): pentaerythritol triacrylate

polymer resin; monomer(s): pentaerythritol triacrylate

Conditions
ConditionsYield
With acetic acid butyl ester; hydroxyethyl cellulose; dibenzoyl peroxide In water at 80℃; for 8h; Product distribution; Further Variations:; Reagents;96.6%
3524-68-3

pentaerythritol triacrylate

2451-62-9

teroxirone

C66H81N3O36

Conditions
ConditionsYield
With 4-methoxy-phenol; triphenylphosphine at 95℃; for 14h;94.58%
19438-60-9

4-methyl-hexahydrophthalic anhydride

3524-68-3

pentaerythritol triacrylate

C22H28O10

Conditions
ConditionsYield
With 4-methoxy-phenol; triphenylphosphine at 90℃; for 8h;91.2%

C29H22O4

3524-68-3

pentaerythritol triacrylate

C57H54O16

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 20h;85%
Downstream Products
57116-45-7
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Chemistry


IUPAC Name: [2-(Hydroxymethyl)-3-prop-2-enoyloxy-2-(prop-2-enoyloxymethyl)propyl] prop-2-enoate 
Empirical Formula: C14H18O7
Molecular Weight: 298.2885 
EINECS: 222-540-8
Product Categories: Functional Monomer; RAW material for negative PR 
storage temp.: 2-8 °C
Sensitive: Hygroscopic
Stability: Stable at room temperature, but potentially explosive at elevated temperatures. Combustible, but may explode if involved in a fire. 
Index of Refraction: 1.488
Molar Refractivity: 72.91 cm3
Molar Volume: 252.9 cm3
Surface Tension: 41.5 dyne/cm
Density: 1.179 g/cm3
Flash Point: 153.5 °C
Enthalpy of Vaporization: 78.86 kJ/mol
Boiling Point: 427.9 °C at 760 mmHg
Vapour Pressure: 4.08E-09 mmHg at 25 °C
Appearance: Thick clear yellow liquid.
Classification Code of Pentaerythritol triacrylate (CAS NO.3524-68-3): Mutation data; Reproductive Effect; Skin / Eye Irritant; Tumor data

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
rabbit LD50 skin 4mL/kg (4mL/kg)   Toxicology and Applied Pharmacology. Vol. 28, Pg. 313, 1974.
rat LD50 intraperitoneal 25mg/kg (25mg/kg) BEHAVIORAL: ATAXIA

GASTROINTESTINAL: OTHER CHANGES

SKIN AND APPENDAGES (SKIN): HAIR: OTHER
National Technical Information Service. Vol. OTS0555706,
rat LD50 oral 1830mg/kg (1830mg/kg) GASTROINTESTINAL: ULCERATION OR BLEEDING FROM SMALL INTESTINE

GASTROINTESTINAL: ULCERATION OR BLEEDING FROM LARGE INTESTINE

GASTROINTESTINAL: OTHER CHANGES
National Technical Information Service. Vol. OTS0555713,

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Moderately toxic by ingestion and skin contact. Skin and severe eye irritant. Questionable carcinogen with experimental tumorigenic data. Used for radiation-cured adhesives, coatings, inks, textiles, photo resists, and coatings. When heated to decomposition it emits acrid smoke and irritating fumes.
Hazard Codes: IrritantXi
Risk Statements: 36/38-43 
R36/38:Irritating to eyes and skin. 
R43:May cause sensitization by skin contact.
Safety Statements: 39 
S39:Wear eye / face protection.
RIDADR: UN3265
WGK Germany: 1
RTECS: UD3370000
HazardClass: 8
PackingGroup: III

Specification

  Pentaerythritol triacrylate (CAS NO.3524-68-3), its Synonyms are Pentaerythrityl triacrylate ; Acrylic acid, triester with pentaerythritol ; Aronix M 305 ; Gafgard 233 ; Kayarad PET 30 ; Light Acrylate PE 3A ; NK Ester A-TMM 3 ; NK Ester A-TMM 3L ; NK Ester TMM 50T ; 2-(Hydroxymethyl)-2-(((1-oxoallyl)oxy)methyl)-1,3-propanediyl diacrylate ; 2-Propenoic acid, 1,1'-(2-(hydroxymethyl)-2-(((1-oxo-2-propen-1-yl)oxy)methyl)-1,3-propanediyl) ester ; 2-Propenoic acid, 2-(hydroxymethyl)-2-(((1-oxo-2-propenyl)oxy)methyl)-1,3-propanediyl ester .