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Basic Information
CAS No.: 4992-63-6
Name: 3,4-DIETHOXY NITROBENZENE
Molecular Structure:
Molecular Structure of 4992-63-6 (3,4-DIETHOXY NITROBENZENE)
Formula: C10H13 N O4
Molecular Weight: 211.218
Synonyms: 1,2-Diethoxy-4-nitrobenzene;1,2-Ethoxy-4-nitrobenzene
Density: 1.158g/cm3
Melting Point: 75 °C
Boiling Point: 328.6oC at 760 mmHg
Flash Point: 145.8oC
PSA: 64.28000
LogP: 2.91540
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Synthetic route
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1,2-dihydroxy-4-nitrobenzene

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ethyl iodide

4992-63-6

1,2-diethoxy-4-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 70℃; for 12h;95.6%
Stage #1: 1,2-dihydroxy-4-nitrobenzene With sodium hydride In DMF (N,N-dimethyl-formamide) at 20℃; for 0.5h;
Stage #2: ethyl iodide at 0 - 20℃; for 12h;		76%
With sodium hydride In 1,4-dioxane
Stage #1: 1,2-dihydroxy-4-nitrobenzene With sodium hydride In N,N-dimethyl-formamide at 50℃; for 0.75h;
Stage #2: ethyl iodide In N,N-dimethyl-formamide at 50℃; for 2h;
2050-46-6

1,2-diethoxybenzene

4992-63-6

1,2-diethoxy-4-nitrobenzene

Conditions
ConditionsYield
With Montmorillonite KSF; nitric acid; hafnium oxychloride In tetrahydrofuran at 20℃; for 18h;92%
With Yb-Mo-modified montmorillonite HKSF; nitric acid In tetrahydrofuran at 20℃; for 12h;66%
With nitric acid; acetic acid
(nitration);
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2-Ethoxyphenol

4992-63-6

1,2-diethoxy-4-nitrobenzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: alcoholic KOH-solution
2: glacial acetic acid; nitric acid
View Scheme
120-80-9

benzene-1,2-diol

1,2-bis<2-(-p-toluenesulfonyloxy)ethoxy>amine

1,2-bis<2-(-p-toluenesulfonyloxy)ethoxy>amine

4992-63-6

1,2-diethoxy-4-nitrobenzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: KOH / 2-methoxy-ethanol
2: (nitration)
View Scheme
4992-63-6

1,2-diethoxy-4-nitrobenzene

113489-36-4

2-Ethoxy-4-nitrophenol K-Salt

Conditions
ConditionsYield
With potassium hydroxide In water for 9h; Heating;98%
4992-63-6

1,2-diethoxy-4-nitrobenzene

39052-12-5

3,4-diethoxyaniline

Conditions
ConditionsYield
With hydrogen; palladium 10% on activated carbon In ethanol for 6h;92.9%
With sodium sulfide
67-56-1

methanol

4992-63-6

1,2-diethoxy-4-nitrobenzene

36160-52-8

2-ethoxy-4-nitroanisole

Conditions
ConditionsYield
With sodium hydroxide at 100℃;
4992-63-6

1,2-diethoxy-4-nitrobenzene

40294-27-7

1,2-diethoxy-4,5-dinitrobenzene

Conditions
ConditionsYield
With nitric acid
With ammonium nitrate; sulfuric acid In acetic acid
4992-63-6

1,2-diethoxy-4-nitrobenzene

40130-25-4

3-ethoxy-4-hydroxynitrobenzene

Conditions
ConditionsYield
With sodium hydroxide
With potassium hydroxide In 2-methoxy-ethanol Heating;
Stage #1: 4-Nitro-1,2-diethoxybenzene With water; potassium hydroxide In 2-methoxy-ethanol for 18h; Reflux;
Stage #2: With hydrogenchloride In water pH=1;
4992-63-6

1,2-diethoxy-4-nitrobenzene

7260-32-4

2-ethoxy-5-nitro-phenol

Conditions
ConditionsYield
With hydrogen bromide; acetic acid
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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Product Name: 3,4-DIETHOXY NITROBENZENE Synonyms: 3,4-DIETHOXY NITROBENZENE;1,2-Diethoxy-4-nitrobenzene;Benzene, 1,2-diethoxy-4-nitro-;MFCD00186132 CAS: 4992-63-6 MF: C10H13NO4 MW: 211.22 EINECS: Product Categories: Mol File: 499

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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