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75-03-6

Basic Information
CAS No.: 75-03-6
Name: Ethyl iodide
Article Data: 308
Molecular Structure:
Molecular Structure of 75-03-6 (Ethyl iodide)
Formula: C2H5I
Molecular Weight: 155.966
Synonyms: AI3-28593;Ethyl iodide;Ethyljodid;Hydriodic ether;Jodethan;Monoiodoethane;NSC 8825;
EINECS: 200-833-1
Density: 1.94 g/cm3
Melting Point: -108 °C
Boiling Point: 72.8 °C at 760 mmHg
Flash Point: 21.1 °C
Solubility: 4 g/L in water at 20 °C
Appearance: Colorless to yellow liquid
Hazard Symbols: HarmfulXn,ToxicT
Risk Codes: 20-36/37/38-42/43-10-23/24/25
Safety: 23-26-45-16-36/37/39-27
PSA: 0.00000
LogP: 1.44130
Synthetic route

[CoEt(dimethylglyoximate(1-))2(pyridine)]

7553-56-2

iodine

A

iodobisdimethylglyoximepyridine cobalt(III)

B

75-03-6

ethyl iodide

Conditions
ConditionsYield
In tetrachloromethane Kinetics; Irradiation (UV/VIS); Kinetics of the reaction of Co(C2H5)(H3CCNOHONCCH3)2(C5H5N) with I2 under irradiation with light at 517 nm is investigated.; MeI and CoI(H3CCNOHONCCH3)2(C5H5N) are the products.;A n/a
B 100%

[CoEt(dimethylglyoximate(1-))2(pyridine)]

75-03-6

ethyl iodide

Conditions
ConditionsYield
With iodine In acetonitrile Kinetics; byproducts: {Co(bis(dimethylglyoximato))py(I)}; one-electron oxidn. of Co complex by I2 at 298 K; monitored by (1)H-NMR and UV spect. (361 nm);100%

ethyl 4-(diethoxyphosphorylmethyl)-5-(iodomethyl)furan-3-carboxylate

122-52-1

triethyl phosphite

A

78-38-6

ethylphosphonic acid diethyl ester

B

ethyl 4,5-bis-(diethoxyphosphorylmethyl)furan-3-carboxylate

C

75-03-6

ethyl iodide

Conditions
ConditionsYield
at 90 - 170℃; for 0.166667h; Arbuzov Reaction;A n/a
B 98%
C n/a
122-52-1

triethyl phosphite

74-88-4

methyl iodide

A

683-08-9

Diethyl methylphosphonate

B

75-03-6

ethyl iodide

Conditions
ConditionsYield
at 130℃; for 0.0833333h; Michaelis-Arbuzov reaction; microwave irradiation;A 97%
B n/a

cis-{(C2H5)2Co(2,2'-bipyridine)2}(ClO4)

A

74-84-0

ethane

B

74-85-1

ethene

C

75-03-6

ethyl iodide

D

106-97-8

n-butane

Conditions
ConditionsYield
With iodine In acetonitrile Kinetics; byproducts: I3(1-), {(C2H5)Co(2,2'-bipyridine)2I}(1+); one-electron oxidn. of cis-Co complex by I2 at 298 K; monitored by (1)H-NMR and UV spect. (361 nm);A <1
B <1
C 97%
D 3.2%
107-25-5

methoxyethene

107-19-7

propargyl alcohol

A

38987-67-6

3-(1-methoxy-ethoxy)-propyne

B

75-03-6

ethyl iodide

Conditions
ConditionsYield
With toluene-4-sulfonic acidA 96%
B n/a
591-50-4

iodobenzene

122-52-1

triethyl phosphite

A

1754-49-0

diethyl phenylphosphonate

B

75-03-6

ethyl iodide

Conditions
ConditionsYield
tetrakis(triethylphosphite)nickel(0) at 160℃;A 94%
B n/a
at 160℃; Mechanism; var. catalysts, var. temp.;
20502-50-5

diethyl phosphoriodidite

7020-81-7

N-(propylidene)-tert-butylamine

A

75-03-6

ethyl iodide

B

1,4-di-tert-butyl-2-ethoxy-3,5-diethyl-1,4,2-diazaphospholidine 2-oxide

Conditions
ConditionsYield
In diethyl ether for 2h; Ambient temperature;A n/a
B 92%
16029-98-4

trimethylsilyl iodide

141-78-6

ethyl acetate

A

2754-27-0

trimethylsilyl acetate

B

75-03-6

ethyl iodide

Conditions
ConditionsYield
at 100℃; for 0.5h; Mechanism; Product distribution;A n/a
B 92%
45817-37-6

4-vinylbenzyl iodide

122-52-1

triethyl phosphite

A

726-61-4

[(4-ethenylphenyl)methyl]phosphonic acid diethyl ester

B

75-03-6

ethyl iodide

Conditions
ConditionsYield
at 20℃; for 6h;A 91%
B n/a
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    Formula: C2H5IMolecular Weight : 155.97 Synonyms: AI3-28593;Ethyl iodide;Ethyljodid;Hydriodic ether;Jodethan;Monoiodoethane;NSC 8825; EINECS: 200-833-1Density: 1.94 g/cm3Melting Point:Boiling Point: 72.8 °C at 760 mmHgFlash Point: 21.1 &d

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Consensus Reports

Reported in EPA TSCA Inventory.

Specification

The Ethane, iodo-, with the CAS registry number 75-03-6, is also known as Monoiodoethane. Its EINECS number is 200-833-1. This chemical's molecular formula is C2H5I and molecular weight is 155.97. What's more, its systematic name is iodoethane. Its classification code is Mutation data. Ethyl iodide is very good with alkylation reactions. It is used as organic reagents and pharmaceutical intermediates. It is also used as the hydrogen radical promoter. It should be sealed and stored in a cool, ventilated and dry place. Moreover, it should be protected from light, heat and fire.

Physical properties of Ethane, iodo- are: (1)ACD/LogP: 2.03; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): 2.03; (4)ACD/LogD (pH 7.4): 2.03; (5)ACD/BCF (pH 5.5): 20.48; (6)ACD/BCF (pH 7.4): 20.48; (7)ACD/KOC (pH 5.5): 302.23; (8)ACD/KOC (pH 7.4): 302.23; (9)Index of Refraction: 1.516; (10)Molar Refractivity: 24.28 cm3; (11)Molar Volume: 80.3 cm3; (12)Polarizability: 9.62×10-24cm3; (13)Surface Tension: 28.5 dyne/cm; (14)Density: 1.94 g/cm3; (15)Flash Point: 21.1 °C; (16)Enthalpy of Vaporization: 29.44 kJ/mol; (17)Boiling Point: 72.8 °C at 760 mmHg; (18)Vapour Pressure: 128 mmHg at 25°C.

Preparation: this chemical can be prepared by ethanol and PI3 by heating and reflux.

2P + 3I→ 2PI3

3C2H5OH + PI3 →3CH3CH2I + H3PO4

Uses of Ethane, iodo-: it can be used to produce 1-ethyl-3-nitro-2-phenyl-indole by heating. It will need reagent Na and solvent ethanol with the reaction time of 2 hours. The yield is about 59%.

Ethane, iodo- can be used to produce 1-ethyl-3-nitro-2-phenyl-indole by heating

When you are using this chemical, please be cautious about it as the following:
This chemical is flammable, so you should keep it away from sources of ignition - No smoking. It is harmful by inhalation. It is toxic by inhalation, in contact with skin and if swallowed. It is irritating to eyes, respiratory system and skin. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. You must not breathe gas/fumes/vapour/spray (appropriate wording to be specified by the manufacturer). You should take off immediately all contaminated clothing. When using it, you need wear suitable protective clothing, gloves and eye/face protection. In case of accident or if you feel unwell, you must seek medical advice immediately (show the label where possible).

You can still convert the following datas into molecular structure:
(1)InChI: InChI=1S/C2H5I/c1-2-3/h2H2,1H3
(2)InChIKey: HVTICUPFWKNHNG-UHFFFAOYSA-N
(3)Canonical SMILES: CCI

The toxicity data is as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
guinea pig LD50 intraperitoneal 322mg/kg (322mg/kg)   "Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects, GKNT, 1982Vol. -, Pg. 68, 1982.
mouse LD50 intraperitoneal 560mg/kg (560mg/kg)   "Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects, GKNT, 1982Vol. -, Pg. 68, 1982.
mouse LD50 subcutaneous 1gm/kg (1000mg/kg) PERIPHERAL NERVE AND SENSATION: FLACCID PARALYSIS WITHOUT ANESTHESIA (USUALLY NEUROMUSCULAR BLOCKAGE)

LUNGS, THORAX, OR RESPIRATION: RESPIRATORY STIMULATION

LUNGS, THORAX, OR RESPIRATION: OTHER CHANGES
Japanese Journal of Pharmacology. Vol. 3, Pg. 99, 1954.
rabbit LDLo oral 300mg/kg (300mg/kg)   "Patty's Industrial Hygiene and Toxicology," 3rd rev. ed., Clayton, G.D., and F.E. Clayton, eds., New York, John Wiley & Sons, Inc., 1978-82. Vol. 3 originally pub. in 1979; pub. as 2n rev. ed. in 1985.Vol. 2B, Pg. 3487, 1981.
rat LC50 inhalation 65gm/m3/30M (65000mg/m3)   Fiziologicheski Aktivnye Veshchestva. Physiologically Active Substances. Vol. 7, Pg. 35, 1975.
rat LD50 intraperitoneal 330mg/kg (330mg/kg)   "Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects, GKNT, 1982Vol. -, Pg. 68, 1982.