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CAS No.: | 5281-20-9 |
---|---|
Name: | acetone hydrazone |
Article Data: | 20 |
Molecular Structure: | |
Formula: | C3H8 N2 |
Molecular Weight: | 72.1099 |
Synonyms: | Acetone,hydrazone (6CI,7CI,8CI); Isopropylidene hydrazine |
Density: | 0.9g/cm3 |
Melting Point: | 128 °C |
Boiling Point: | 110.5°C at 760 mmHg |
Flash Point: | 20.7°C |
PSA: | 38.38000 |
LogP: | 1.04120 |
Conditions | Yield |
---|---|
With barium(II) oxide; hydrazine In methanol at -5 - 20℃; | 89% |
With hydrazine hydrate; barium(II) oxide | |
With hydrazine |
Conditions | Yield |
---|---|
With hydrazine hydrate |
Conditions | Yield |
---|---|
With hydrazine at 100℃; | |
With hydrazine at 100℃; for 16h; Inert atmosphere; Schlenk technique; | |
With hydrazine at 100℃; for 16h; Inert atmosphere; |
Conditions | Yield |
---|---|
With potassium bromate; perchloric acid In water; acetic acid at 19.9℃; Rate constant; Kinetics; Thermodynamic data; E(a), ΔH(excit.), ΔS(excit.), ΔG(excit.); var. reagent concentrations, var. pH values; |
Conditions | Yield |
---|---|
at 100℃; |
hydrogenchloride
propan-2-one azine
A
acetone hydrazone
B
acetone
C
hydrazine
Conditions | Yield |
---|---|
at 15℃; Gleichgewicht;pH=4.60 bis 5.35; | |
at 20℃; Gleichgewicht;pH=4.60 bis 5.35; |
acetone
1-phenylbutan-1,3-dione
A
acetone hydrazone
B
2-(3'-methyl-5'-phenylpyrazol-1'-yl)-5-methyl-7-phenylpyrazolo[1,5-a]pyrimidine
C
3-methyl-5-phenylpyrazole
Conditions | Yield |
---|---|
In water for 4h; Reflux; regioselective reaction; | A 60 %Spectr. B 8 %Spectr. C 32 %Spectr. |
Conditions | Yield |
---|---|
With C24H20B(1-)*C27H39AuClN*K(1+); hydrazine at 130℃; for 14h; Inert atmosphere; |