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56796-66-8

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CAS No.: 56796-66-8
Name: 4-(benzyloxy)-alpha-[[tert-butylamino]methyl]-m-xylene-alpha,alpha'-diol
Article Data: 2
Molecular Structure:
Molecular Structure of 56796-66-8 (4-(benzyloxy)-alpha-[[tert-butylamino]methyl]-m-xylene-alpha,alpha'-diol)
Formula: C20H27 N O3
Molecular Weight: 329.439
Synonyms: 4-(benzyloxy)-alpha-[[tert-butylamino]methyl]-m-xylene-alpha,alpha'-diol;Salbutamol [-Alpha[ (Tert-Butylamino) Methyl)-4-Benzyloxy Sulphate 1,3-Benzene Dimethanol];1-(4-Benzyloxy-3-hydroxymethyl-phenyl)-2-(tert-butylamino)ethanol;4-Benzyl Albuterol;a1-[[(1,1-Dimethylethyl)amino]methyl]-4-(phenylmethoxy)-1,3-benzenedimethanol;4-(BENZYLOXY)-ALPHA1-[(TERT-BUTYLAMINO)METHYL]BENZENE-1,3-DIMETHANOL;4-(Benzyloxy)-ALPHA-[(tert-butylamino)-methyl]-m-xylene- ALPHA,ALPHA''-di
Density: 1.12g/cm3
Boiling Point: 510.1°Cat760mmHg
Flash Point: 262.3°C
PSA: 61.72000
LogP: 3.57030
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56796-66-8

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Conditions
ConditionsYield
With sodium bis(2-methoxyethoxy)aluminium dihydride In toluene at 60℃; for 1h; Inert atmosphere;90%
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56796-66-8

α1-[[(1,1-dimethylethyl)amino]methyl]-4-(benzyloxy)-1,3-benzenedimethanol

Conditions
ConditionsYield
With sodium hydroxide; water at 80 - 85℃; for 15 - 16h;
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56796-66-8

α1-[[(1,1-dimethylethyl)amino]methyl]-4-(benzyloxy)-1,3-benzenedimethanol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: hydrogen bromide; water; dimethyl sulfoxide / acetonitrile / 4 h / 40 - 60 °C / Inert atmosphere
2: Isopropyl acetate / 2.5 h / 40 °C / Inert atmosphere
3: sodium tetrahydroborate / methanol / 2.33 h / 20 - 35 °C / Inert atmosphere
4: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 1 h / 60 °C / Inert atmosphere
View Scheme

C17H16O6

56796-66-8

α1-[[(1,1-dimethylethyl)amino]methyl]-4-(benzyloxy)-1,3-benzenedimethanol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: Isopropyl acetate / 2.5 h / 40 °C / Inert atmosphere
2: sodium tetrahydroborate / methanol / 2.33 h / 20 - 35 °C / Inert atmosphere
3: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 1 h / 60 °C / Inert atmosphere
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methyl 5-[[(1,1-dimethylethyl)imino]acetyl]-2-(benzyloxy)benzoate

56796-66-8

α1-[[(1,1-dimethylethyl)amino]methyl]-4-(benzyloxy)-1,3-benzenedimethanol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / methanol / 2.33 h / 20 - 35 °C / Inert atmosphere
2: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 1 h / 60 °C / Inert atmosphere
View Scheme
100-39-0

benzyl bromide

56796-66-8

α1-[[(1,1-dimethylethyl)amino]methyl]-4-(benzyloxy)-1,3-benzenedimethanol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: potassium carbonate / acetonitrile / 0.75 h / Inert atmosphere
1.2: 2 h / Reflux; Inert atmosphere
2.1: hydrogen bromide; water; dimethyl sulfoxide / acetonitrile / 4 h / 40 - 60 °C / Inert atmosphere
3.1: Isopropyl acetate / 2.5 h / 40 °C / Inert atmosphere
4.1: sodium tetrahydroborate / methanol / 2.33 h / 20 - 35 °C / Inert atmosphere
5.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 1 h / 60 °C / Inert atmosphere
View Scheme
16475-90-4

estere metilico dell'acido 5-acetilsalicilico

56796-66-8

α1-[[(1,1-dimethylethyl)amino]methyl]-4-(benzyloxy)-1,3-benzenedimethanol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: potassium carbonate / acetonitrile / 0.75 h / Inert atmosphere
1.2: 2 h / Reflux; Inert atmosphere
2.1: hydrogen bromide; water; dimethyl sulfoxide / acetonitrile / 4 h / 40 - 60 °C / Inert atmosphere
3.1: Isopropyl acetate / 2.5 h / 40 °C / Inert atmosphere
4.1: sodium tetrahydroborate / methanol / 2.33 h / 20 - 35 °C / Inert atmosphere
5.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 1 h / 60 °C / Inert atmosphere
View Scheme
56796-66-8

α1-[[(1,1-dimethylethyl)amino]methyl]-4-(benzyloxy)-1,3-benzenedimethanol

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Lg-tartaric acid mono-(4-nitro-anilide)

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4-nitro tartranilic acid salt of (R)-isomer of 4-benzyl salbutamol

Conditions
ConditionsYield
Stage #1: α1-[[(1,1-dimethylethyl)amino]methyl]-4-(benzyloxy)-1,3-benzenedimethanol; Lg-tartaric acid mono-(4-nitro-anilide) In ethyl acetate; isopropyl alcohol at 75℃; for 44h; Resolution of racemate;
Stage #2: In ethyl acetate; isopropyl alcohol at 70 - 75℃; for 2h;		90%
In ethyl acetate; isopropyl alcohol at 75℃; for 44h;90%
56796-66-8

α1-[[(1,1-dimethylethyl)amino]methyl]-4-(benzyloxy)-1,3-benzenedimethanol

2-tert-butylamino-1-(4-hydroxy-2-hydroxymethyl-phenyl)ethanol

Conditions
ConditionsYield
Stage #1: α1-[[(1,1-dimethylethyl)amino]methyl]-4-(benzyloxy)-1,3-benzenedimethanol With palladium 10% on activated carbon; hydrogen In ethanol at 50℃; under 1500.15 Torr; for 2h;
Stage #2: With sulfuric acid In ethanol at 15℃;		77%
56796-66-8

α1-[[(1,1-dimethylethyl)amino]methyl]-4-(benzyloxy)-1,3-benzenedimethanol

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In methanol at 21 - 60℃; for 18.33h; Product distribution / selectivity;14.2%
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