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6276-54-6

Basic Information
CAS No.: 6276-54-6
Name: 1-Propanamine,3-chloro-, hydrochloride (9CI)
Article Data: 4
Cas Database
Molecular Structure:
Molecular Structure of 6276-54-6 (1-Propanamine,3-chloro-, hydrochloride (9CI))
Formula: C3H9Cl2N
Molecular Weight: 130.017
Synonyms: Propylamine,3-chloro-, hydrochloride (6CI,8CI);1-Amino-3-chloropropane hydrochloride;1-Chloro-3-aminopropane hydrochloride;3-Amino-1-chloropropane hydrochloride;3-Aminopropyl chloride hydrochloride;3-Chloro-1-propanamine hydrochloride;
EINECS: 228-474-6
Density: 1.004 g/cm3
Melting Point: 145-150 °C(lit.)
Boiling Point: 130.7 °C at 760 mmHg
Flash Point: 32.9 °C
Solubility: N/A
Appearance: off-white to yellow-beige crystalline
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36/37-36
Transport Information: N/A
PSA: 26.02000
LogP: 2.07630
Synthetic route
156-87-6

propan-1-ol-3-amine

6276-54-6

3-chloropropylamine hydrochloride

Conditions
ConditionsYield
With thionyl chloride In chloroform at 0℃; Reflux;93%
With thionyl chloride In chloroform at 0 - 20℃; for 3h; Reflux;93%
With thionyl chloride In chloroform at 0 - 20℃;

3-hydroxypropylamine hydrochloride

6276-54-6

3-chloropropylamine hydrochloride

Conditions
ConditionsYield
With thionyl chloride at 25℃; for 1h;83%
24424-99-5

di-tert-butyl dicarbonate

6276-54-6

3-chloropropylamine hydrochloride

116861-31-5

tert-butyl N-(3-chloropropyl)carbamate

Conditions
ConditionsYield
With sodium hydrogencarbonate; sodium chloride In chloroform; water for 1.5h; Heating;100%
With triethylamine In dichloromethane at 0 - 25℃; for 21h;100%
With triethylamine In chloroform Acylation;95%
6276-54-6

3-chloropropylamine hydrochloride

88192-19-2

3-azidopropylamine

Conditions
ConditionsYield
With sodium azide In water at 80℃; for 15h;100%
With sodium azide In water at 80℃; for 15h;100%
With sodium azide In water at 80℃; for 15h;99%
6276-54-6

3-chloropropylamine hydrochloride

100-52-7

benzaldehyde

1026774-25-3

benzylidene-(3-chloro-1-propylamine)

Conditions
ConditionsYield
With triethylamine In chloroform at 20℃; for 16h;100%
With magnesium sulfate; triethylamine In dichloromethane at 20℃; for 1h;83%
With magnesium sulfate; triethylamine In dichloromethane for 12h;
6276-54-6

3-chloropropylamine hydrochloride

123-11-5

4-methoxy-benzaldehyde

4-methoxybenzylidene-(3-chloro-1-propylamine)

Conditions
ConditionsYield
Stage #1: 3-chloropropylamine hydrochloride With triethylamine In chloroform at 20℃; for 0.0833333h;
Stage #2: 4-methoxy-benzaldehyde With magnesium sulfate In chloroform at 20℃; for 16h;
100%
With triethylamine In chloroform at 20℃; for 16h;100%
With magnesium sulfate; triethylamine In dichloromethane for 12h;
7791-25-5

sulfuryl dichloride

6276-54-6

3-chloropropylamine hydrochloride

42065-72-5

(3-chloropropyl)sulfamyl chloride

Conditions
ConditionsYield
In acetonitrile at 0 - 85℃;100%
6276-54-6

3-chloropropylamine hydrochloride

42065-72-5

(3-chloropropyl)sulfamyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride In acetonitrile at 0 - 85℃;100%
With sulfuryl dichloride In acetonitrile at 85℃; Cooling with ice;100%
With sulfuryl dichloride In acetonitrile at 85℃; Cooling with ice;100%
6276-54-6

3-chloropropylamine hydrochloride

501-53-1

benzyl chloroformate

53602-19-0

1-[(benzyloxycarbonyl)amino]-3-chloropropane

Conditions
ConditionsYield
With sodium hydroxide In water at 0 - 25℃; for 24h;100%
With sodium hydroxide In water at 0℃; for 12h; Inert atmosphere;90%
Stage #1: 3-chloropropylamine hydrochloride With sodium hydroxide In water at 0℃; for 0.25h; Schlenk technique;
Stage #2: benzyl chloroformate In water at 0℃; for 12h;
2.48 g

C82H125CoN15O15P

6276-54-6

3-chloropropylamine hydrochloride

C84H133CoN15O15P

Conditions
ConditionsYield
Stage #1: C82H125CoN15O15P With ammonium bromide; zinc In ethanol for 0.333333h; Inert atmosphere;
Stage #2: 3-chloropropylamine hydrochloride In ethyl [2]alcohol for 3h; Inert atmosphere;
100%
Raw Materials
156-87-6
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Chemistry

IUPAC Name: 3-Chloropropan-1-amine
Following is the structure of 3-chloropropylamine hydrochloride (CAS NO.6276-54-6):
                               
Empirical Formula: C3H8ClN
Molecular Weight: 93.5553 g/mol
EINECS: 228-474-6
Index of Refraction: 1.435
Molar Refractivity: 24.33 cm3
Molar Volume: 93.1 cm3
Density: 1.004 g/cm3
Flash Point: 32.9 °C
Surface Tension: 30.5 dyne/cm
Melting point: 145-150 °C(lit.)
Enthalpy of Vaporization: 36.84 kJ/mol
Boiling Point: 130.7 °C at 760 mmHg
Vapour Pressure: 9.58 mmHg at 25 °C
Product Categories of 3-chloropropylamine hydrochloride (CAS NO.6276-54-6): omega-Functional Alkanols, Carboxylic Acids, Amines & Halides; omega-Haloalkylamines
Appearance of 3-chloropropylamine hydrochloride (CAS NO.6276-54-6): off-white to yellow-beige crystalline
Canonical SMILES: C(CN)CCl
InChI: InChI=1S/C3H8ClN/c4-2-1-3-5/h1-3,5H2
InChIKey: BZFKSWOGZQMOMO-UHFFFAOYSA-N

Uses

 3-chloropropylamine hydrochloride (CAS NO.6276-54-6) , aliphatic amine with halogen, is used in manufacturing other compounds.
 

Toxicity Data With Reference

 3-chloropropylamine hydrochloride (CAS NO.6276-54-6) hasn't been listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65. And the toxicological properties have not been fully investigated.

Safety Profile

The Hazard Codes of 3-chloropropylamine hydrochloride(6276-54-6):  Xi
The Risk Statements information of  3-chloropropylamine hydrochloride (CAS NO.6276-54-6):
36/37/38:  Irritating to eyes, respiratory system and skin 
The Safety Statements information of  3-chloropropylamine hydrochloride (CAS NO.6276-54-6):
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
36:  Wear suitable protective clothing 
36/37:  Wear suitable protective clothing and gloves 
WGK Germany:  3

Specification

 3-chloropropylamine hydrochloride , its cas register number is 6276-54-6. It also can be called 1-Amino-3-chloropropane hydrochloride ; and 3-Chloropropylammonium chloride .
 3-chloropropylamine hydrochloride (CAS NO.6276-54-6) could be stable under normal temperatures and pressures.  It absorbs moisture or water from the air.It should avoid the condition like incompatible materials, exposure to moist air or water. It is not compatible with strong oxidizing agents. And also prevent it to broken down into hazardous decomposition products: hydrogen chloride, carbon monoxide, carbon dioxide. However, its hazardous polymerization will not occur.

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