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6276-54-6

Basic Information
CAS No.: 6276-54-6
Name: 1-Propanamine,3-chloro-, hydrochloride (9CI)
Molecular Structure:
Molecular Structure of 6276-54-6 (1-Propanamine,3-chloro-, hydrochloride (9CI))
Formula: C3H9Cl2N
Molecular Weight: 130.02 .
Synonyms: Propylamine,3-chloro-, hydrochloride (6CI,8CI);1-Amino-3-chloropropane hydrochloride;1-Chloro-3-aminopropane hydrochloride;3-Amino-1-chloropropane hydrochloride;3-Aminopropyl chloride hydrochloride;3-Chloro-1-propanamine hydrochloride;
EINECS: 228-474-6
Density: 1.004 g/cm3
Melting Point: 145-150 °C(lit.)
Boiling Point: 130.7 °C at 760 mmHg
Flash Point: 32.9 °C
Solubility:
Appearance: off-white to yellow-beige crystalline
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36/37-36
Transport Information:
PSA: 26.02000
LogP: 2.07630
Synthetic route
156-87-6

propan-1-ol-3-amine

6276-54-6

3-chloropropylamine hydrochloride

Conditions
ConditionsYield
With thionyl chloride In chloroform at 0℃; Reflux;93%
With thionyl chloride In chloroform at 0 - 20℃; for 3h; Reflux;93%
With thionyl chloride In chloroform at 0 - 20℃;

3-hydroxypropylamine hydrochloride

6276-54-6

3-chloropropylamine hydrochloride

Conditions
ConditionsYield
With thionyl chloride at 25℃; for 1h;83%
24424-99-5

di-tert-butyl dicarbonate

6276-54-6

3-chloropropylamine hydrochloride

116861-31-5

tert-butyl N-(3-chloropropyl)carbamate

Conditions
ConditionsYield
With sodium hydrogencarbonate; sodium chloride In chloroform; water for 1.5h; Heating;100%
With triethylamine In dichloromethane at 0 - 25℃; for 21h;100%
With triethylamine In chloroform Acylation;95%
6276-54-6

3-chloropropylamine hydrochloride

88192-19-2

3-azidopropylamine

Conditions
ConditionsYield
With sodium azide In water at 80℃; for 15h;100%
With sodium azide In water at 80℃; for 15h;100%
With sodium azide In water at 80℃; for 15h;99%
6276-54-6

3-chloropropylamine hydrochloride

100-52-7

benzaldehyde

1026774-25-3

benzylidene-(3-chloro-1-propylamine)

Conditions
ConditionsYield
With triethylamine In chloroform at 20℃; for 16h;100%
With magnesium sulfate; triethylamine In dichloromethane at 20℃; for 1h;83%
With magnesium sulfate; triethylamine In dichloromethane for 12h;
6276-54-6

3-chloropropylamine hydrochloride

123-11-5

4-methoxy-benzaldehyde

4-methoxybenzylidene-(3-chloro-1-propylamine)

Conditions
ConditionsYield
Stage #1: 3-chloropropylamine hydrochloride With triethylamine In chloroform at 20℃; for 0.0833333h;
Stage #2: 4-methoxy-benzaldehyde With magnesium sulfate In chloroform at 20℃; for 16h;
100%
With triethylamine In chloroform at 20℃; for 16h;100%
With magnesium sulfate; triethylamine In dichloromethane for 12h;
7791-25-5

sulfuryl dichloride

6276-54-6

3-chloropropylamine hydrochloride

42065-72-5

(3-chloropropyl)sulfamyl chloride

Conditions
ConditionsYield
In acetonitrile at 0 - 85℃;100%
6276-54-6

3-chloropropylamine hydrochloride

42065-72-5

(3-chloropropyl)sulfamyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride In acetonitrile at 0 - 85℃;100%
With sulfuryl dichloride In acetonitrile at 85℃; Cooling with ice;100%
With sulfuryl dichloride In acetonitrile at 85℃; Cooling with ice;100%
6276-54-6

3-chloropropylamine hydrochloride

501-53-1

benzyl chloroformate

53602-19-0

1-[(benzyloxycarbonyl)amino]-3-chloropropane

Conditions
ConditionsYield
With sodium hydroxide In water at 0 - 25℃; for 24h;100%
With sodium hydroxide In water at 0℃; for 12h; Inert atmosphere;90%
Stage #1: 3-chloropropylamine hydrochloride With sodium hydroxide In water at 0℃; for 0.25h; Schlenk technique;
Stage #2: benzyl chloroformate In water at 0℃; for 12h;
2.48 g

C82H125CoN15O15P

6276-54-6

3-chloropropylamine hydrochloride

C84H133CoN15O15P

Conditions
ConditionsYield
Stage #1: C82H125CoN15O15P With ammonium bromide; zinc In ethanol for 0.333333h; Inert atmosphere;
Stage #2: 3-chloropropylamine hydrochloride In ethyl [2]alcohol for 3h; Inert atmosphere;
100%
6276-54-6

3-chloropropylamine hydrochloride

120-14-9

3,4-dimethoxy-benzaldehyde

3,4-dimethoxybenzylidene-(3-chloro-1-propylamine)

Conditions
ConditionsYield
With magnesium sulfate; triethylamine In chloroform at 20℃;99%
6276-54-6

3-chloropropylamine hydrochloride

103-72-0

phenyl isothiocyanate

66268-31-3, 133524-17-1, 3420-40-4, 864524-22-1

phenyl(1,3-thiazan-2-yliden)amine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 4h;99%
6276-54-6

3-chloropropylamine hydrochloride

2131-61-5

p-nitrophenyl isothiocyanate

(4-nitrophenyl)(1,3-thiazan-2-yliden)amine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 4h;99%
6276-54-6

3-chloropropylamine hydrochloride

135-02-4

ortho-anisaldehyde

2-methoxybenzylidene-(3-chloro-1-propylamine)

Conditions
ConditionsYield
Stage #1: 3-chloropropylamine hydrochloride With triethylamine In chloroform at 20℃; for 0.0833333h;
Stage #2: ortho-anisaldehyde With magnesium sulfate In chloroform at 20℃; for 16h;
99%
4122-56-9

methyl o-formylbenzoate

6276-54-6

3-chloropropylamine hydrochloride

1377966-35-2

methyl 2-[(3-chloropropylimino)methyl]benzoate

Conditions
ConditionsYield
With magnesium sulfate; triethylamine In chloroform at 20℃; for 2h;99%
6276-54-6

3-chloropropylamine hydrochloride

2530-87-2

3-Chloropropyltrimethoxysilan

C9H22ClNO3Si

Conditions
ConditionsYield
Stage #1: 3-chloropropylamine hydrochloride With sodium hydroxide In water for 2h; Cooling with ice;
Stage #2: 3-Chloropropyltrimethoxysilan In toluene at 100℃; for 24h; Inert atmosphere;
99%
6276-54-6

3-chloropropylamine hydrochloride

18171-19-2

3-chloropropylmethyldimethoxysilane

C9H22ClNO2Si

Conditions
ConditionsYield
Stage #1: 3-chloropropylamine hydrochloride With ammonium hydroxide for 2.5h; Cooling with ice;
Stage #2: 3-chloropropylmethyldimethoxysilane In dimethyl sulfoxide at 120℃; for 12h; Inert atmosphere;
99%
13508-63-9

chloropropyl(dimethyl)ethoxysilane

6276-54-6

3-chloropropylamine hydrochloride

C10H24ClNOSi

Conditions
ConditionsYield
Stage #1: 3-chloropropylamine hydrochloride With potassium carbonate for 2h; Cooling with ice;
Stage #2: chloropropyl(dimethyl)ethoxysilane In N,N-dimethyl-formamide at 110℃; for 24h; Inert atmosphere;
99%
5089-70-3

(3-chloropropyl)triethoxysilane

6276-54-6

3-chloropropylamine hydrochloride

C12H28ClNO3Si

Conditions
ConditionsYield
Stage #1: 3-chloropropylamine hydrochloride With potassium hydroxide for 1h; Cooling with ice;
Stage #2: (3-chloropropyl)triethoxysilane In N,N-dimethyl-formamide at 110℃; for 24h; Inert atmosphere;
99%
N2-atmosphere

N2-atmosphere

6276-54-6

3-chloropropylamine hydrochloride

106-54-7

p-Chlorothiophenol

78540-43-9

N-[3-[(4-Chlorophenyl)thio]propyl]amine hydrochloride

Conditions
ConditionsYield
With sodium ethanolate In ethanol; water98%
34619-03-9

tert-butyldicarbonate

6276-54-6

3-chloropropylamine hydrochloride

116861-31-5

tert-butyl N-(3-chloropropyl)carbamate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃;98%
With triethylamine In chloroform at 20℃;95%
6276-54-6

3-chloropropylamine hydrochloride

107-13-1

acrylonitrile

3-(3-chloro-propylamino)-propionitrile

Conditions
ConditionsYield
With sodium In ethanol at 25℃; for 8h;97%
6276-54-6

3-chloropropylamine hydrochloride

591-31-1

3-methoxy-benzaldehyde

3-methoxybenzylidene-(3-chloro-1-propylamine)

Conditions
ConditionsYield
Stage #1: 3-chloropropylamine hydrochloride With triethylamine In chloroform at 20℃; for 0.0833333h;
Stage #2: 3-methoxy-benzaldehyde With magnesium sulfate In chloroform at 20℃; for 16h;
97%
With magnesium sulfate; triethylamine In dichloromethane for 12h;
40615-36-9

4,4'-dimethoxytrityl chloride

6276-54-6

3-chloropropylamine hydrochloride

153652-94-9

3-chloro-N-4,4'-dimethoxytritylpropanamine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 3h;96%
574-66-3

Benzophenone oxime

6276-54-6

3-chloropropylamine hydrochloride

O-(3-aminopropyl)benzophenone oxime

Conditions
ConditionsYield
With potassium hydroxide In dimethyl sulfoxide at 20℃; for 3h; Alkylation;96%
865998-76-1

1-methyl-4-[({[4-(trifluoromethoxy)phenyl]amino}carbonyl)amino]-1H-imidazole-2-carboxylic acid

6276-54-6

3-chloropropylamine hydrochloride

N-(3-chloropropyl)-1-methyl-4-[({[4-(trifluoromethoxy)phenyl]amino}carbonyl)amino]-1H-imidazole-2-carboxamide

Conditions
ConditionsYield
Stage #1: 1-methyl-4-[({[4-(trifluoromethoxy)phenyl]amino}carbonyl)amino]-1H-imidazole-2-carboxylic acid With dmap; HATU In DMF (N,N-dimethyl-formamide) at 20℃; for 0.25h;
Stage #2: 3-chloropropylamine hydrochloride With triethylamine In DMF (N,N-dimethyl-formamide)
96%
6276-54-6

3-chloropropylamine hydrochloride

1571-08-0

methyl 4-formylbenzoate

4-methoxycarbonylbenzylidene-(3-chloro-1-propylamine)

Conditions
ConditionsYield
With triethylamine In chloroform at 20℃; for 16h;95%
164356-70-1

[CpFe(CO)(CN(CH2)3PPh2)]I

6276-54-6

3-chloropropylamine hydrochloride

[CpFe(CO)(C(NH(CH2)3Cl)NH(CH2)3PPh2)]I

Conditions
ConditionsYield
With NaOCH2CH3 In ethanol; dichloromethane byproducts: NaCl; (inert atm.); addn. of ethanolic soln. of sodium ethylate to soln. of amine hydrochloride deriv. at room temp., stirring for 10 min, filtration,addn. to CH2Cl2 soln. of iron compd. at room temp., stirring overnight; concg., addn. of diethyl ether, filtration, washing with pentane, dryingin vac., elem. anal.;95%

C18H11ClN2O2

6276-54-6

3-chloropropylamine hydrochloride

N-(3‑chloropropyl)-1-(2-chlorophenyl)-9H-β-carboline-3‑carboxamide

Conditions
ConditionsYield
With triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride In tetrahydrofuran; methanol at 20℃;95%
6276-54-6

3-chloropropylamine hydrochloride

78-84-2

isobutyraldehyde

N-(2-methyl-1-propylidene)-3-chloropropylamine

Conditions
ConditionsYield
With magnesium sulfate; triethylamine In dichloromethane for 1h; Ambient temperature;94%
872-85-5

pyridine-4-carbaldehyde

6276-54-6

3-chloropropylamine hydrochloride

(3-Chloro-propyl)-[1-pyridin-4-yl-meth-(E)-ylidene]-amine

Conditions
ConditionsYield
With potassium carbonate In dichloromethane; water for 0.666667h;94%
6276-54-6

3-chloropropylamine hydrochloride

147695-56-5

4-bromophenyl isoselenocyanate

(4-bromophenyl)(1,3-selenazan-2-yliden)amine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 4h;94%
Raw Materials
156-87-6
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    3-Chloropropylamine hydrochloride Basic information Product Name: 3-Chloropropylamine hydrochloride Synonyms: 3-AMINOPROPYL CHLORIDE HYDROCHLORIDE;3-CHLORPROPYLAMINE HYDROCHLORIDE;3-CHLOROPROPYLAMINE HCL;3-CHLO

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    1-Propanamine,3-chloro-, hydrochloride (9CI) 6276-54-6

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  • Pharmaceutical Intermediate, 1-Amino-3-chloropropane hydrochloride  CAS:6276-54-6

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    Pharmaceutical Intermediate, 1-Amino-3-chloropropane hydrochloride CAS:6276-54-6

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Chemistry

IUPAC Name: 3-Chloropropan-1-amine
Following is the structure of 3-chloropropylamine hydrochloride (CAS NO.6276-54-6):
                               
Empirical Formula: C3H8ClN
Molecular Weight: 93.5553 g/mol
EINECS: 228-474-6
Index of Refraction: 1.435
Molar Refractivity: 24.33 cm3
Molar Volume: 93.1 cm3
Density: 1.004 g/cm3
Flash Point: 32.9 °C
Surface Tension: 30.5 dyne/cm
Melting point: 145-150 °C(lit.)
Enthalpy of Vaporization: 36.84 kJ/mol
Boiling Point: 130.7 °C at 760 mmHg
Vapour Pressure: 9.58 mmHg at 25 °C
Product Categories of 3-chloropropylamine hydrochloride (CAS NO.6276-54-6): omega-Functional Alkanols, Carboxylic Acids, Amines & Halides; omega-Haloalkylamines
Appearance of 3-chloropropylamine hydrochloride (CAS NO.6276-54-6): off-white to yellow-beige crystalline
Canonical SMILES: C(CN)CCl
InChI: InChI=1S/C3H8ClN/c4-2-1-3-5/h1-3,5H2
InChIKey: BZFKSWOGZQMOMO-UHFFFAOYSA-N

Uses

 3-chloropropylamine hydrochloride (CAS NO.6276-54-6) , aliphatic amine with halogen, is used in manufacturing other compounds.
 

Toxicity Data With Reference

 3-chloropropylamine hydrochloride (CAS NO.6276-54-6) hasn't been listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65. And the toxicological properties have not been fully investigated.

Safety Profile

The Hazard Codes of 3-chloropropylamine hydrochloride(6276-54-6):  Xi
The Risk Statements information of  3-chloropropylamine hydrochloride (CAS NO.6276-54-6):
36/37/38:  Irritating to eyes, respiratory system and skin 
The Safety Statements information of  3-chloropropylamine hydrochloride (CAS NO.6276-54-6):
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
36:  Wear suitable protective clothing 
36/37:  Wear suitable protective clothing and gloves 
WGK Germany:  3

Specification

 3-chloropropylamine hydrochloride , its cas register number is 6276-54-6. It also can be called 1-Amino-3-chloropropane hydrochloride ; and 3-Chloropropylammonium chloride .
 3-chloropropylamine hydrochloride (CAS NO.6276-54-6) could be stable under normal temperatures and pressures.  It absorbs moisture or water from the air.It should avoid the condition like incompatible materials, exposure to moist air or water. It is not compatible with strong oxidizing agents. And also prevent it to broken down into hazardous decomposition products: hydrogen chloride, carbon monoxide, carbon dioxide. However, its hazardous polymerization will not occur.

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