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66-25-1

Basic Information
CAS No.: 66-25-1
Name: 1-HEXANAL
Molecular Structure:
Molecular Structure of 66-25-1 (1-HEXANAL)
Formula: C6H12O
Molecular Weight: 100.18
Synonyms: Caproaldehyde;Caproic aldehyde;Capronaldehyde;Hexaldehyde;Hexanaldehyde;Hexylaldehyde;NSC 2596;n-Caproaldehyde;n-Capronaldehyde;n-Hexanal;n-Hexylaldehyde;
EINECS: 200-624-5
Density: 0.801 g/cm3
Melting Point: -56 °C
Boiling Point: 127.9 °C at 760 mmHg
Flash Point: 26.2 °C
Solubility: 4.8 g/L (20 °C) in water
Appearance: liquid
Hazard Symbols: IrritantXi
Risk Codes: 10
Safety: 37/39-26-16
Transport Information: UN 1207 3/PG 3
PSA: 17.07000
LogP: 1.76560
Synthetic route
111-27-3

hexan-1-ol

66-25-1

hexanal

Conditions
ConditionsYield
With 4 A molecular sieve; tetrabutylammonium periodite; sodium ruthenate(VI) In dichloromethane at 20℃; for 24h; Oxidation;100%
With 4 A molecular sieve; tetrabutylammonium perchlorate; Ru-Cu-Al-hydrotalcite In toluene at 60℃; for 24h;100%
With iodosylbenzene; Cl-CH2-PS supported 5-amino-1,10-phenanthroline-Ru In acetonitrile at 60℃; for 2h;100%
3658-93-3

1,1-diethoxyhexane

66-25-1

hexanal

Conditions
ConditionsYield
With water In tetrahydrofuran; diethyl ether at 80℃; under 6000.6 Torr; Inert atmosphere; Autoclave;100%
With dibromotriphenylphosphorane In dichloromethane at -50℃; for 1h;74%
With 6C72H112O8*8H2O In chloroform-d1; water for 1h; Inert atmosphere;
64847-81-0

1,1-hexanediol diacetate

66-25-1

hexanal

Conditions
ConditionsYield
With beta zeolite modified with chlorosulphonic acid (28 wtpercent) In ethanol at 50℃; for 0.0833333h;100%
With ethanol at 50℃; for 0.166667h; chemoselective reaction;98%
With (NH4)3PW12O40 In methanol at 20℃; for 2h;92%
1599-47-9

1,1-dimethoxyhexane

66-25-1

hexanal

Conditions
ConditionsYield
With water In tetrahydrofuran; diethyl ether at 80℃; under 6000.6 Torr; Inert atmosphere; Autoclave;100%
142-62-1

hexanoic acid

66-25-1

hexanal

Conditions
ConditionsYield
With thexylchloroborane-Me2SO4 In dichloromethane for 0.25h; Ambient temperature;99%
With thexylchloroborane-Me2SO4 In dichloromethane for 0.25h; Product distribution; Ambient temperature; other aliphatic and aromatic acids, other products, other times;99%
With thexylbromoborane dimethyl sulfide complex In carbon disulfide; dichloromethane at -20 - 20℃; for 1h;94%
16577-51-8

hexanoic acid Li-salt

66-25-1

hexanal

Conditions
ConditionsYield
With 9-borabicyclo[3.3.1]nonane dimer In tetrahydrofuran for 1h; Ambient temperature;99%
6728-26-3

(E)-2-Hexenal

66-25-1

hexanal

Conditions
ConditionsYield
With hydrogen; sodium dodecyl-sulfate; palladium diacetate In tetrahydrofuran; water at 20℃; under 760.051 Torr; for 0.5h; Reagent/catalyst; chemoselective reaction;98%
With N,N,N,N,N,N-hexamethylphosphoric triamide; diisobutylaluminium hydride In tetrahydrofuran; hexane at 0℃; for 1h;89%
With hydrogen In isopropyl alcohol at 110℃; under 22502.3 Torr; for 3h; Autoclave;35.2%
64214-56-8

N-methoxy-N-methyl hexanamide

66-25-1

hexanal

Conditions
ConditionsYield
With lithium diisobutyl-tert-butoxyaluminum hydride In tetrahydrofuran; hexane at 0℃; Reagent/catalyst; Inert atmosphere; chemoselective reaction;97%
With benzoic acid ethyl ester; copper diisobutyl-t-butoxyaluminum hydride In tetrahydrofuran at 20℃; for 12h; Inert atmosphere; chemoselective reaction;99 %Chromat.
111-27-3

hexan-1-ol

A

6378-65-0

n-hexyl caproate

B

66-25-1

hexanal

Conditions
ConditionsYield
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide In dichloromethane; water at 0℃; Electrolysis; Saturated solution;A n/a
B 95%
With calcium dichloride dihydrate; oxone; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water In dichloromethane at 20℃; for 2.5h; Catalytic behavior; Reagent/catalyst; Time; Solvent; Overall yield = 59 %Chromat.;A 91%
B 9%
With oxone; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; water In dichloromethane at 20℃; for 4h; Catalytic behavior; Overall yield = 7 %Chromat.;A 9%
B 52%
26533-34-6

isopropyl amyl carbinol

66-25-1

hexanal

Conditions
ConditionsYield
With lead(IV) acetate; lithium chloride In benzene at 80℃;95%
693-02-7

hex-1-yne

66-25-1

hexanal

Conditions
ConditionsYield
With chloro(cyclopentadienyl)[bis(diphenylphosphino)methane]ruthenium; water In isopropyl alcohol at 100℃; for 12h;95%
With water; C46H53F3N4O4P2RuS In acetone at 69 - 72℃; for 36h; Product distribution; Further Variations:; Catalysts; Reagents; anti-Markovnikov hydration;96 % Spectr.
With water; ruthenium In benzene-d6 at 70℃; Product distribution; Further Variations:; Catalysts;
1927-63-5

2-hexyloxy-tetrahydro-pyran

66-25-1

hexanal

Conditions
ConditionsYield
With aluminium trichloride; tetramethylammonium chlorochromate In acetonitrile for 1h; Heating;94%
111-25-1

1-bromo-hexane

66-25-1

hexanal

Conditions
ConditionsYield
With 4-methylmorpholine N-oxide; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride; potassium iodide at 100℃; for 0.0833333h; Microwave irradiation; Ionic liquid;94%
With dihydrogen peroxide In ethanol for 7h; Reflux; Green chemistry;62%
73188-53-1

1,1'-bis(phenylthio)hexane

66-25-1

hexanal

Conditions
ConditionsYield
With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid In dichloromethane for 1h; Ambient temperature;92%
6033-61-0

hexanal oxime

66-25-1

hexanal

Conditions
ConditionsYield
With water; Dess-Martin periodane In dichloromethane at 5℃; for 0.5h;92%
With molybdenum(V) chloride; zinc In acetonitrile at 20℃; for 0.333333h;78%
With potassium sulfate; potassium hydrogensulfate; potassium peroxomonosulfate; acetic acid In water at 40 - 45℃; for 5h;70%
With iodine at 45 - 60℃; for 0.183333h; Reagent/catalyst; Microwave irradiation;70%
13389-42-9

trans-2-Octene

66-25-1

hexanal

Conditions
ConditionsYield
With cobalt(II) 5,10,15,20-tetraphenylporphyrin; naphthalene; oxygen; isovaleraldehyde at 80℃; under 760.051 Torr; for 6h;92%
Stage #1: trans-2-Octene With cis-[Ru(2,9-Me2phen)2(OH2)2](PF6)2 In acetonitrile at 55℃; for 0.5h;
Stage #2: With dihydrogen peroxide In acetonitrile for 8h;
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere
2: sulfuric acid / acetonitrile; water / 20 °C
3: C21H12Cl6NO4V / toluene / 3 h / 100 °C / 760.05 Torr
View Scheme
17888-62-9

hexanoxytrimethylsilane

66-25-1

hexanal

Conditions
ConditionsYield
With aluminium trichloride; tetramethylammonium chlorochromate In acetonitrile for 1.33333h; Heating;90%
764-60-3

hex-2-yn-1-ol

66-25-1

hexanal

Conditions
ConditionsYield
With 20 % Pd(OH)2/C; hydrogen In benzene at 20℃; for 0.5h;90%
10051-44-2

sodium caproate

66-25-1

hexanal

Conditions
ConditionsYield
With 9-borabicyclo[3.3.1]nonane dimer In tetrahydrofuran for 0.5h; Ambient temperature;87%
5830-30-8

N,N-dimethylhexanamide

66-25-1

hexanal

Conditions
ConditionsYield
With sodium aluminum tetrahydride In tetrahydrofuran at 0℃; for 3h;86%
With diethyl ether; lithium diethoxyaluminum hydride
With sodium diethylpiperidinohydroaluminate In tetrahydrofuran at 0℃; for 3h;96 % Chromat.
74585-39-0

2-n-pentyl-1,3-dithiolane

66-25-1

hexanal

Conditions
ConditionsYield
With sodium nitrate; sulfuric acid; silica gel In dichloromethane at 20℃; for 0.416667h;86%
With polystyryl-mercury trifluoroacetate; water In dichloromethane at 23℃; for 96h; Product distribution; var. temp., and time, var. solvents; other thioacetals and thioketals;42 % Chromat.
5063-65-0

1,2-epoxyheptane

66-25-1

hexanal

Conditions
ConditionsYield
With sodium paraperiodate; sulfuric acid In water at 20℃; for 0.5h;85%
109-67-1

1-penten

201230-82-2

carbon monoxide

A

123-15-9

2-methylvaleraldehyde

B

66-25-1

hexanal

Conditions
ConditionsYield
With acetylacetonatodicarbonylrhodium(l); hydrogen; triphenylphosphine In neat (no solvent) at 80℃; under 7500.75 Torr; for 1h; Catalytic behavior; Time; Autoclave;A 11.1%
B 83.7%
With hydrogen; (polymer-PPh2)2Ru(CO)3 In benzene at 140℃; under 51714.8 Torr; for 20h; Product distribution; further temperature, pressure; other catalysts;
With water; dodecacarbonyltetrairidium In methanol at 150℃; under 41371.8 Torr; for 0.5h; Product distribution; other group 8 transition-metal catalysts;

hex-1-enylboronic acid

66-25-1

hexanal

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In 1,4-dioxane at 20℃; under 760.051 Torr; for 31h; Irradiation; Green chemistry;83%
693-02-7

hex-1-yne

A

591-78-6

n-hexan-2-one

B

66-25-1

hexanal

Conditions
ConditionsYield
With sodium hydroxide; thexylbromoborane dimethyl sulfide complex; dihydrogen peroxide Product distribution; directive effect of thexylhaloborane-methyl sulfide in the hydroboration of alkynes; further reagents; multistep reaction;A n/a
B 82%
With water; ; (pentafluorophenyl)diphenylphosphine In isopropyl alcohol at 65℃; for 12h; Title compound not separated from byproducts;A 3.0 % Chromat.
B 71 % Chromat.
Stage #1: hex-1-yne With aniline; bis(trimethylsilyl)acetylenetitanocene In toluene at 85℃; for 24h;
Stage #2: With hydrogenchloride Title compound not separated from byproducts;
With C35H44F3N5O3PtS In benzene-d6; water; acetone for 24h; Glovebox; Sealed tube; Heating; Inert atmosphere;A 21 %Spectr.
B 79 %Spectr.
142-61-0

Hexanoyl chloride

66-25-1

hexanal

Conditions
ConditionsYield
With sodium tris(tert-butoxo)aluminium hydride In tetrahydrofuran; diethylene glycol dimethyl ether at -78℃; for 1h;81%
Stage #1: Hexanoyl chloride With aluminium hydride In tetrahydrofuran at 20℃; for 1h; Metallation;
Stage #2: With pyridinium chlorochromate In tetrahydrofuran; dichloromethane at 20℃; for 6h; Oxidation;
81%
With tri-n-butyl-tin hydride; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride In tetrahydrofuran at 25℃; for 0.25h;80%
61103-84-2

benzyl hexyl ether

A

638-51-7

1-hexyl nitrite

B

100-52-7

benzaldehyde

C

66-25-1

hexanal

D

111-27-3

hexan-1-ol

Conditions
ConditionsYield
With nitric acid In dichloromethane at 20℃; for 1h; Further byproducts given;A n/a
B 81%
C n/a
D n/a

(+/-)-4,5-dimethyl-3-(cis-2-methylcyclopentyloxy)-thiazole-2(3H)-thione

688-73-3

tri-n-butyl-tin hydride

A

35108-31-7

4,5-dimethyl-2-(tributylstannylsulfanyl)-thiazole

B

66-25-1

hexanal

Conditions
ConditionsYield
In benzene-d6 at 20℃; for 0.5h; Inert atmosphere; UV-irradiation;A 81%
B 71%
646-14-0

1-nitrohexane

66-25-1

hexanal

Conditions
ConditionsYield
With dihydrogen peroxide; potassium carbonate In methanol; water for 8h; Ambient temperature;80%
With sodium perborate for 6h; Ionic liquid;75%
Stage #1: 1-nitrohexane With potassium hydroxide In methanol Nef reaction; Continuous flow conditions;
Stage #2: With potassium permanganate; water In methanol at 25℃; Nef reaction; Sonication; Continuous flow conditions; chemoselective reaction;
74%
With sodium hydroxide; sodium chlorite; tetra(n-butyl)ammonium hydrogensulfate In dichloromethane for 0.7h; Ambient temperature; Yield given;
Multi-step reaction with 2 steps
1: 56 percent / AcONH4 / acetic acid / 10 h / 100 °C
2: aq. H2O2; OH(-); 1-butyl-3-methylimidazolim trifluoromethanesulfonate / 16 h / 25 °C
View Scheme
107-21-1

ethylene glycol

66-25-1

hexanal

3515-94-4

2-pentyl-1,3-dioxolane

Conditions
ConditionsYield
distannoxane 1a In benzene for 0.5h; Mechanism; Product distribution; Heating; other distannoxane catalysts, other aldehydes, other alcohol, other solvents, other reaction times;100%
With 9.0 wt% H4[SiW12O40] on SiO2 In neat (no solvent) at 60℃; for 6h; Reagent/catalyst; chemoselective reaction;99%
With Kaolinitic clay In benzene for 2h; Heating;90%
75-52-5

nitromethane

66-25-1

hexanal

6302-74-5

1-nitroheptan-2-ol

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran; tert-butyl alcohol at 0 - 20℃; for 24h; Henry reaction;100%
With potassium tert-butylate In tetrahydrofuran; tert-butyl alcohol Addition;99%
With (S,S)-1,2-diaminocyclohexane; copper(II) acetate monohydrate In ethanol at 20℃; for 12h; Henry reaction; Inert atmosphere; enantioselective reaction;99%
66-25-1

hexanal

142-62-1

hexanoic acid

Conditions
ConditionsYield
With N-hydroxyphthalimide; trans-Re(O)Cl2(OC(CH3)2C(CH3)2O)2P(Ph)3; oxygen In acetonitrile at 30℃; under 760.051 Torr; for 1.1h;100%
With diphenyl diselenide; dihydrogen peroxide In water at 20℃; for 3h; Green chemistry;99%
With N-hydroxyphthalimide; oxygen In acetonitrile at 30℃; for 3h; Schlenk technique;99%
66-25-1

hexanal

111-27-3

hexan-1-ol

Conditions
ConditionsYield
With Na-phosphate buffer; horse liver NADH; NAD; sodium formate; <(C5Me5)Rh(bpy-5-OAc)(H2O)>Cl2 at 25℃; for 30h; Product distribution; Mechanism; other ketones, other times, other temperatures, other enzymes;100%
With sodium aluminum tetrahydride In tetrahydrofuran at 0℃; for 0.0833333h; Product distribution; other aldehydes, ketones, carboxylic acids (also sodium salts), acid chlorides, esters, lactones, epoxides, amides, nitriles, nitrogen and sulfur compounds; var. temp., time and ratio of reagents;100%
With sodium aluminum tetrahydride In tetrahydrofuran at 0℃; for 0.0833333h;100%
107-19-7

propargyl alcohol

66-25-1

hexanal

98262-70-5

(R/S)-non-2-yne-1,4-diol

Conditions
ConditionsYield
Stage #1: propargyl alcohol With n-butyllithium In tetrahydrofuran; hexane at -40℃; for 0.333333h; Inert atmosphere;
Stage #2: hexanal With cerium(III) chloride In tetrahydrofuran; hexane Reagent/catalyst;
100%
With n-butyllithium In tetrahydrofuran at -78℃;93%
Stage #1: propargyl alcohol With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere;
Stage #2: hexanal In tetrahydrofuran; hexane at -78 - 0℃; for 2h; Inert atmosphere;
86%
420-90-6

3-bromo-3,3-difluropropene

66-25-1

hexanal

131437-07-5

3,3-difluoro-1-nonen-4-ol

Conditions
ConditionsYield
With indium In water for 3h;100%
With zinc In tetrahydrofuran47%
With indium In N,N-dimethyl-formamide
80436-57-3

[3-(2-Methyl-[1,3]dioxolan-2-yl)-1-methylsulfanyl-propyl]-phosphonic acid diethyl ester

66-25-1

hexanal

80436-58-4

{2-Hydroxy-1-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-1-methylsulfanyl-heptyl}-phosphonic acid diethyl ester

Conditions
ConditionsYield
With n-butyllithium100%
72931-54-5

(3,3-diisopropoxy-propyl)-triphenyl-phosphonium bromide

66-25-1

hexanal

120018-49-7

(Z)-3-nonenal diisopropyl acetal

Conditions
ConditionsYield
With sodium hexamethyldisilazane In tetrahydrofuran for 12h; -100 deg C to RT;100%
With sodium hexamethyldisilazane 1.) THF, toluene, RT, 1 h, 2.) from -100 to 0 deg C, 4 h; Yield given. Multistep reaction;
With sodium hexamethyldisilazane 1.) THF, room temp., 1 h; HMPA, 0 deg C, 1 h, 2.) -100 deg C to room temp., overnight; Yield given. Multistep reaction;
123445-64-7

2-methylseleno-2-phenylselenopropan

66-25-1

hexanal

A

32773-42-5

butyl methyl selenide

B

22233-89-2

(phenylseleno)-2-propane

C

123445-63-6

2-phenylseleno-2-methyl octane-3-ol

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.2h;A 100%
B 10%
C 90%
66-25-1

hexanal

101566-91-0

N-(2-methoxyphenyl)-2-<(tributylstannyl)methyl>propenamide

101566-97-6

4-hydroxy-N-(2-methoxyphenyl)-2-methylenenonanamide

Conditions
ConditionsYield
With boron trifluoride diethyl etherate In dichloromethane at -78 - 0℃; for 4h;100%
66-25-1

hexanal

1066-54-2

trimethylsilylacetylene

69498-66-4

1-trimethylsilyloct-1-yn-3-ol

Conditions
ConditionsYield
Stage #1: trimethylsilylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h;
Stage #2: hexanal In tetrahydrofuran; hexane at -78 - 20℃; for 3h;
100%
Stage #1: trimethylsilylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h;
Stage #2: hexanal In tetrahydrofuran; hexane at 0℃; for 4h;
96%
With n-butyllithium In hexane at 25℃; for 1.5h;80%
66-25-1

hexanal

Conditions
ConditionsYield
With 1,3-dimethylimidazolim iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,4-dioxane for 3h; Heating;100%
With N-benzyl-N,N,N-triethylammonium chloride; 1-chloro-1-fluoromethyl phenyl sulfone In tetrahydrofuran at 20℃; for 4h;85%
With L-Tryptophan In water at 20℃; for 3h; Catalytic behavior; Solvent; Sealed tube; Green chemistry;78%
72320-38-8

3-azidopropan-1-ol

66-25-1

hexanal

2-Pentyl-5,6-dihydro-4H-[1,3]oxazine

Conditions
ConditionsYield
With boron trifluoride diethyl etherate In dichloromethane Ambient temperature; other reagents: H2SO4, TiCl4, SnCl4, trimethylsilyl triflate;100%
66-25-1

hexanal

249890-38-8

(1S,5S,6S,7R)-6,7-epoxy-6-[(E)-2'-carbobenzyloxy-1'-vinyl]-2-oxabicyclo[3.3.0]octan-3-one

249890-37-7

(1S,5R,7R,2'R,S,3'R,S)-7-hydroxy-6-[(E,Z)-3'-hydroxyoct-2'-carbobenzyloxy-1'-ylidene]-2-oxabicyclo[3.3.0]octan-3-one

Conditions
ConditionsYield
With samarium diiodide In tetrahydrofuran at -78℃; for 0.833333h; Condensation;100%
66-25-1

hexanal

790699-58-0

(3R)-6,8-dibenzyloxy-9-hydroxy-3-methyl-3,4-dihydro-2H-anthracen-1-one

849692-99-5

6,8-bis-benzyloxy-9-hydroxy-2-(1-hydroxy-hexyl)-3-methyl-3,4-dihydro-2H-anthracen-1-one

Conditions
ConditionsYield
Stage #1: (3R)-6,8-dibenzyloxy-9-hydroxy-3-methyl-3,4-dihydro-2H-anthracen-1-one With TEA; t-butyldimethylsiyl triflate In dichloromethane
Stage #2: hexanal With boron trifluoride diethyl etherate at -70℃;
100%
66-25-1

hexanal

845960-16-9

(5-hexyl-furan-3-yloxy)-trimethyl-silane

5-hexyl-2-(1-hydroxy-hexyl)-furan-3-one

Conditions
ConditionsYield
With boron trifluoride diethyl etherate In dichloromethane at -78℃; for 1h;100%
66-25-1

hexanal

105-34-0

methyl 2-cyanoacetate

111735-80-9

(E)-2-cyano-oct-2-enoic acid methyl ester

Conditions
ConditionsYield
With piperidine; acetic acid at 20℃; for 14h;100%
64715-85-1, 91298-74-7, 127180-88-5

(R)-2-methoxy-1-phenylethylamine

66-25-1

hexanal

C15H23NO

Conditions
ConditionsYield
With magnesium sulfate In dichloromethane at 20℃; for 12h;100%
3095-95-2

diethylphosphonoacetic acid

66-25-1

hexanal

1871-67-6

(E)-oct-2-enoic acid

Conditions
ConditionsYield
With N,N,N,N,-tetramethylethylenediamine; zinc trifluoromethanesulfonate; 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 25℃; for 12h; Horner-Wadsworth-Emmons reaction;100%
866932-09-4

6-({4-[(4-methoxyphenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one

66-25-1

hexanal

866932-12-9

6-(hexyl{4-[(4-methoxyphenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one

Conditions
ConditionsYield
Stage #1: 6-({4-[(4-methoxyphenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one; hexanal With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 70℃; for 24h;
Stage #2: With sodium hydrogencarbonate In water; 1,2-dichloro-ethane
100%
110-44-1

sorbic Acid

66-25-1

hexanal

142077-75-6, 142077-76-7, 142247-75-4, 142247-76-5, 142247-77-6

(1RS,2SR)-2-(1-hydroxyhexyl)-3,5-hexadienoic acid

Conditions
ConditionsYield
In tetrahydrofuran; water; diisopropylamine; pentane100%
72748-99-3

(R)-1-Amino-2-(methoxymethyl)pyrrolidine

66-25-1

hexanal

128718-25-2

C12H24N2O

Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; Molecular sieve; Inert atmosphere;100%
5153-67-3

nitrostyrene

66-25-1

hexanal

(+)-(2S)-2-[(R)-2-nitro-1-phenyl-ethyl]-hexanal

Conditions
ConditionsYield
With : H-D-Pro-Pro-Glu supported on polyethyleneglycol-polystyrene (TentaGel resin) In chloroform; isopropyl alcohol at -15℃; for 19h; optical yield given as %ee; enantioselective reaction;100%
With 4-methyl-morpholine; C16H26N4O5 In neat (no solvent) at 20℃; for 24h; stereoselective reaction;100%
With 4-methyl-morpholine; H-D-Pro-L-Pro-L-Glu-NH2*TFA In chloroform; isopropyl alcohol at 20℃; optical yield given as %ee; enantioselective reaction;98%
18971-59-0

1-pentylisonitrile

66-25-1

hexanal

C18H35NO3

Conditions
ConditionsYield
With water; sodium sulfate at 20℃; for 7h; Passerini Condensation;100%
66-25-1

hexanal

ethyl isocyano formate

C11H21NO4

Conditions
ConditionsYield
With water; sodium tosylate at 20℃; for 7h; Passerini Condensation;100%
75-75-2

methanesulfonic acid

66-25-1

hexanal

C7H13O3S(1-)*Na(1+)

Conditions
ConditionsYield
With sodium butanolate In butan-1-ol Reflux;100%
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  • 1-HEXANAL Manufacturer/High quality/Best price/In stock

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    Business Type:Lab/Research institutions

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  •  Simagchem Corporation

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  • Casno:

    66-25-1

    Caproaldehyde

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    Business Type:Lab/Research institutions

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    66-25-1

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  • Caproaldehyde CAS NO.66-25-1

  • Casno:

    66-25-1

    Caproaldehyde CAS NO.66-25-1

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     China (Mainland)  |  Contact Details

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  • Caproaldehyde CAS NO.66-25-1 CAS NO.66-25-1

  • Casno:

    66-25-1

    Caproaldehyde CAS NO.66-25-1 CAS NO.66-25-1

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     China (Mainland)  |  Contact Details

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Address:Building 3 of Innovation Park, East District of the National University Science Park

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    1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume

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    Address:NO.56,Hongzhuan Road

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    Business Type:Lab/Research institutions

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    Business Type:Other

    Tel:+86 592 605 6448

    Address:No.31 Pingshan South Road, HaiCang District, Xiamen, China

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  • Casno:

    66-25-1

    Hexanal

    Min.Order: 1 Gram

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Address:Room 435, 4th floor, Building 9, No. 2568 Gudai Road,Minhang District, Shanghai,

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    66-25-1

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    Business Type:Other

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  • High Purity n-hexaldehyde supplier in China

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    Business Type:Lab/Research institutions

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    66-25-1

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     China (Mainland)  |  Contact Details

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    66-25-1

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    Business Type:Trading Company

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    66-25-1

    Hexanal

    Min.Order: 1 Gram

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Address:Room 260, Building 3, No. 76 Xingqiao North Road, Xingqiao Street, Yuhang District, Hangzhou City, Zhejiang Province, China

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    66-25-1

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    Business Type:Lab/Research institutions

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    Address:Dong Fang Road,

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  • Casno:

    66-25-1

    Hexanal

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    high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

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     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:86-29-86107037-8015

    Address:No.11 Daqing Road,Lianhu District,Xi’an 710082,China

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    66-25-1

    Hexanal

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    Business Type:Lab/Research institutions

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    Address:Huacai International Building,Sandun,Westlake District,Hangzhou 310030,Zhejiang,China

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  • Casno:

    66-25-1

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-579-82660891

    Address:47-204 No.288, Shida St., Wuchem Dist., Jinhua,Zhejiang, 321004 China

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    66-25-1

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    Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

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  •  Aecochem Corp.

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:+86-592 599 8717

    Address:No 611 Sishui Road,Huli

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  • Caproaldehyde

  • Casno:

    66-25-1

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    Located in Zhengdong New District,?Zhengzhou of Henan province, Henan Allgreen Chemical Co.,Ltd is a comprehensive high-tech modern enterprises integrating professional R&D, pro

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    Business Type:Manufacturers

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    Address:No 260 Dongming Road,Jinshui District

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    66-25-1

    1-HEXANAL

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    Synonyms :Caproaldehyde; Hexaldehyde Molecular Formula :C6H12O Molecular Weight :100.16 EINECS :200-624-5 FEMA :2557 Density :0.815 Meltin…Appearance:colorless transparent liquid Storage:Stored in a cool dry place, not open dumps. Package:200 l

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     China (Mainland)  |  Contact Details

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    Tel:86-543-8178171

    Address:428 Daixi Third Road Zouping County Shandong Province China

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  • Casno:

    66-25-1

    Hexanal(66-25-1)

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    Shaanxi Cuicheng Biomedical Technology Co., Ltd. is located in Chuangzhi Industrial Park, Economic and Technological Development Zone, Hanzhong City, Shaanxi Province, China. It is a company specializing in natural medicines and high-throughput scree

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  •  Shaanxi Cuicheng Biomedical Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:18791163155

    Address:economic development Zone

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  • CAS NO.:66-25-1

  • Casno:

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    factory supply, best price and top qualityAppearance:white powder Storage:Room temperature Package:bag Application:Pharmaceutical intermediates Transportation:By Sea/Air/DHL Port:China main port

    The company is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds,

  •  Henan Wentao Chemical Product Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-370-2722992

    Address:32 Room, 5th Floor, Building 11, No. 6 Yinxing Road, High-tech Industrial Development Zone, Zhengzhou City, Henan Province

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  • Casno:

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    Min.Order: 1 Kilogram

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    Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

    Zhuo Zhou Wen Xi Import and Export Co., Ltd. is a company mainly engaged in the export of pharmaceutical raw materials. Its parent company is (Wen Xi Pharma), including three subs

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-13111626072

    Address:Room 1710, Baoxin International Phase I, 19 Guanyun East Road, Zhuozhou, Hebei

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  • Casno:

    66-25-1

    Hexanal

    Min.Order: 0

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-21-50563169

    Address:Room1027,No.Jinyu Road,Pudong

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    66-25-1

    Hexanal

    Min.Order: 0

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    Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

    Amoychem integrates the sourcing ,marketing and support of the entire range of top-quality chemical products. We provide our customers with professional service and high performan

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     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86 592 605 1114

    Address:Factory 2/F, NO. 206 Weili Road

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  • Casno:

    66-25-1

    1-HEXANAL

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    Comply with CP,JP,EP,US GradeAppearance:White Solid Storage:Stored under room temperature in cool and dry place Package:In 25KG paper or plastic drums Application:Used as pharmaceutical Intermeidate Transportation:Shipped as non- dangerous chemicals

    Who we are ? Located in Zhengzhou City, China , Henan Daken Chemical Co.,Ltd was Established in June ,1983.We have a 35 years history for fine chemical synthesis .Daken has young

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-371-55541817

    Address:No.56 Hongzhuan Road,Jinshui,Zhengzhou,450000,China

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  • Casno:

    66-25-1

    Hexaldehyde

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    ≥99%, stockAppearance:A clear colorless liquid Storage:2-8°C Package:1kg/bag;25kg/cardboard drum Application:OLED Transportation:by air, by sea

    We are specialized in manufacturing Organic Optoelectronic Chemicals, especially for OLED (Organic Light Emitting Diode) and OPC (Organic Photo Conductor) materials, Pharmaceutical

  •  Springchem New Material Technology Co.,Limited

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-21-51752791, 51752788

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    Hexanal manufacture

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  • Hexanal

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Chemistry

MF: C6H12O
MW: 100.16
EINECS: 200-624-5
mp:  -56 °C 
bp:  130-131 °C(lit.)
density:  0.816 g/mL at 20 °C
vapor density:  >1 (vs air)
vapor pressure:  10 mm Hg ( 20 °C)
FEMA:  2557
refractive index:  n20/D 1.4035(lit.)
Fp:  90 °F
storage temp:  2-8°C
Water Solubility:  4.8 g/L (20 oC)
Sensitive:  Air Sensitive
Merck:  14,1760
BRN:  506198
CAS DataBase Reference: 66-25-1(CAS DataBase Reference)

Toxicity Data With Reference

1.   

skn-rbt 500 mg/24H MLD

   85JCAE    Prehled Prumyslove Toxikologie; Organicke Latky Marhold, J.,Prague, Czechoslovakia.: Avicenum,1986,272.
2.   

skn-rbt 14,178 μg/24H open MLD

   AIHAAP    American Industrial Hygiene Association Journal. 23 (1962),95.
3.   

eye-rbt 500 mg/24H MLD

   85JCAE    Prehled Prumyslove Toxikologie; Organicke Latky Marhold, J.,Prague, Czechoslovakia.: Avicenum,1986,272.
4.   

orl-rat LD50:4890 mg/kg

   AMIHBC    AMA Archives of Industrial Hygiene and Occupational Medicine. 10 (1954),61.
5.   

ihl-rat LCLo:2000 ppm/4H

   AMIHBC    AMA Archives of Industrial Hygiene and Occupational Medicine. 10 (1954),61.

Consensus Reports

1-HEXANAL is reported in EPA TSCA Inventory.

Safety Profile

Hazard Codes:  Xi
Risk Statements:  10
Safety Statements:  37/39-26-16
RIDADR:  UN 1207 3/PG 3
WGK Germany:  1
RTECS:  MN7175000
F:  13
Hazard Note:  Irritant
HazardClass:  3
PackingGroup:  III
Hazardous Substances Data: 66-25-1(Hazardous Substances Data)
Mildly toxic by ingestion and inhalation. An irritant to skin and eyes. Flammable liquid. A dangerous fire hazard when exposed to heat or flame; can react vigorously with oxidizing materials. When heated to decomposition it emits acrid smoke and fumes.

Standards and Recommendations

DOT Classification:  3; Label: Flammable Liquid

Specification

1、Fire Fighting Measures of Hexanal 
General Information: As in any fire, wear a self-contained breathing apparatus in pressure-demand, MSHA/NIOSH (approved or equivalent), and full protective gear. Vapors can travel to a source of ignition and flash back. Will burn if involved in a fire. Flammable liquid and vapor. 
Extinguishing Media: Use foam, dry chemical, or carbon dioxide. Cool containers with flooding quantities of water until well after fire is out. 
2、Handling and Storage of Hexanal  
Handling: Use with adequate ventilation. Use spark-proof tools and explosion proof equipment. Avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes. 
Storage: Keep away from sources of ignition. Store in a cool, dry place. Store in a tightly closed container. Flammables-area.