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CAS No.: | 6711-48-4 |
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Name: | 3,3'-Iminobis(N,N-dimethylpropylamine) |
Article Data: | 17 |
Molecular Structure: | |
Formula: | C10H25 N3 |
Molecular Weight: | 187.329 |
Synonyms: | 1,3-Propanediamine,N'-[3-(dimethylamino)propyl]-N,N-dimethyl- (9CI); Dipropylamine, 3,3'-bis(dimethylamino)-(7CI,8CI); 1,1,9,9-Tetramethyl-1,5,9-triazanonane;2,10-Dimethyl-2,6,10-triazaundecane; 2,6,10-Triazaundecane, 2,10-dimethyl-;3,3'-Iminobis(N,N-dimethylpropylamine); 3'-Iminobis(N,N-dimethylpropylamine);Bis[3-(dimethylamino)propyl]amine; Jeffcat Z 130;N,N,N',N'-Tetramethyliminobispropylamine;N,N-Bis[3-(dimethylamino)propyl]amine;N-(3-Dimethylaminopropyl)-N',N'-dimethylpropane-1,3-diamine; NSC 129937;N'-[3-(Dimethylamino)propyl]-N,N-dimethyl-1,3-propanediamine; Polycat 15;Polycat 70/15; Polycat 9; Tetramethyldipropylenetriamine; Z 130 |
EINECS: | 229-761-9 |
Density: | 0.841g/mLat25°C(lit.) |
Melting Point: | −78°C(lit.) |
Boiling Point: | 128-131°C20mmHg(lit.) |
Flash Point: | 209°F |
Solubility: | 425g/L at 20℃ |
Hazard Symbols: | C |
Risk Codes: | 21/22-34; |
Safety: | Poison by skin contact. Moderately toxic by ingestion. A skin irritant. When heated to decomposition it emits toxic fumes of NOx. See also AMINES. |
PSA: | 18.51000 |
LogP: | 0.87030 |
α-(dimethylamino)-propionitrile
B
N,N,N'N'-tetramethyl-1,3-propanediamine
C
1-amino-3-(dimethylamino)propane
D
N,N-bis-(3-dimethylaminopropyl)amine
Conditions | Yield |
---|---|
With caustic; hydrogen; nickel catalyst Degussa MC502 In water at 90℃; under 5932.2 Torr; for 0.45h; Product distribution / selectivity; | A n/a B n/a C 99.98% D n/a |
1-amino-3-(dimethylamino)propane
3-dimethylaminopropiononitrile
N,N-bis-(3-dimethylaminopropyl)amine
Conditions | Yield |
---|---|
With Cu-Cr2O3-CoO/γ-Al2O3; hydrogen In toluene at 100℃; under 7500.75 Torr; Reagent/catalyst; | 75.6% |
With Pd/γ-Al2O3; hydrogen In toluene at 80℃; under 30003 Torr; for 4h; Reagent/catalyst; Solvent; Autoclave; | 87.9 %Chromat. |
With hydrogen at 90 - 110℃; under 37503.8 - 45004.5 Torr; for 3h; Reagent/catalyst; Autoclave; | 745 g |
N,N-bis-(3-dimethylamino-propyl)-benzenesulfonamide
N,N-bis-(3-dimethylaminopropyl)amine
Conditions | Yield |
---|---|
(i) ClSO3H, (ii) aq. NaOH; Multistep reaction; |
Conditions | Yield |
---|---|
With hydrogen; rhodium on alumina In methanol | |
With hydrogen; Rh on carbon In ethanol under 2574.3 Torr; |
Conditions | Yield |
---|---|
With sodium; butan-1-ol Reduktion; |
3-dimethylaminopropiononitrile
butan-1-ol
A
1-amino-3-(dimethylamino)propane
B
N,N-bis-(3-dimethylaminopropyl)amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dimethylformamide 2: (i) ClSO3H, (ii) aq. NaOH View Scheme |
Conditions | Yield |
---|---|
With hydrogen at 140℃; under 22502.3 Torr; | |
With hydrogen; DE-A19 53 263 catalyst at 140℃; under 7500.75 - 60006 Torr; Conversion of starting material; | |
With hydrogen at 140℃; under 22502.3 Torr; |
α-(dimethylamino)-propionitrile
A
1-amino-3-(dimethylamino)propane
B
N,N-bis-(3-dimethylaminopropyl)amine
Conditions | Yield |
---|---|
With sodium hydroxide; hydrogen; nickel catalyst Degussa MC502 In water at 90℃; under 5688.78 Torr; Product distribution / selectivity; | |
With lithium hydroxide; hydrogen; nickel catalyst Degussa MC502 In water at 90℃; under 25858.1 Torr; Product distribution / selectivity; | |
With potassium hydroxide; hydrogen; nickel catalyst Degussa MC502 In water at 90℃; under 5171.62 Torr; Product distribution / selectivity; |
1-amino-3-(dimethylamino)propane
A
N,N-bis[3-(dimethylamino)propyl]-N',N'-dimethylpropane-1,3-diamine
B
N,N-bis-(3-dimethylaminopropyl)amine
Conditions | Yield |
---|---|
With hydrogen at 100 - 200℃; under 0 - 15001.5 Torr; Product distribution / selectivity; | |
With Pd/γ-Al2O3; hydrogen In toluene at 80℃; under 30003 Torr; for 4h; Autoclave; | A 67 %Chromat. B 10.9 %Chromat. |
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