CAS No.71-44-3,Spermine Suppliers

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Basic Information

Molecular Structure:
CAS No.:	71-44-3
Name:	Spermine
Article Data:	27

Formula:	C₁₀H₂₆N₄
Molecular Weight:	202.343
Synonyms:	1,4-Butanediamine,N,N'-bis(3-aminopropyl)- (8CI,9CI);Spermine (6CI);1,5,10,14-Tetraazatetradecane;4,9-Diazadodecane-1,12-diamine;Gerontine;Musculamine;N,N'-Bis(3-aminopropyl)-1,4-butanediamine;N,N'-Bis(3-aminopropyl)-1,4-tetramethylenediamine;NSC 268508;Neuridine;
EINECS:	200-754-2
Density:	0.925 g/cm³
Melting Point:	310-311 °C (dec.)(lit.)
Boiling Point:	308.4 °C at 760 mmHg
Flash Point:	175.6 °C
Solubility:	1 M at 20 °C, clear, colorless
Appearance:	white to slightly off-white powder crystal
Hazard Symbols:	Xi,C
Risk Codes:	36/38-34
Safety:	26-36-45-36/37/39-27
Transport Information:	UN 3259 8/PG 2
PSA:	76.10000
LogP:	1.82580

Synthetic route

: 14209-32-6
3-(4-[(2-cyanoethyl)amino]butylamino)propanenitrile

: 71-44-3
Spermine

Conditions

Conditions	Yield
With sodium; butan-1-ol
With diethyl ether; ammonia; nickel at 140℃; under 250073 Torr; Hydrogenation;
With hydrogenchloride; platinum Hydrogenation;

: 78706-92-0
1,2-bis(1,4,5,6-tetrahydropyrimidin-2-yl)ethane

: 71-44-3
Spermine

Conditions

Conditions	Yield
With sulfuric acid; diisobutylaluminium hydride; 1,1,1,3,3,3-hexamethyl-disilazane 1.) reflux, 12 h, 2.) xylene, reflux, 3 d; Yield given. Multistep reaction;

: 525-79-1
kinetin

A: 124-20-9
N-(3-aminopropyl)-1,4-diaminobutane

B: 71-44-3
Spermine

C: 110-60-1
1,4-diaminobutane

Conditions

Conditions	Yield
at 30℃; for 24h; effect on poliamine content and ratio in rice embryos of Oryza sativa;

...Expand

: 14398-53-9
(R)-(-)-abscisic acid

A: 124-20-9
N-(3-aminopropyl)-1,4-diaminobutane

B: 71-44-3
Spermine

C: 110-60-1
1,4-diaminobutane

Conditions

Conditions	Yield
at 30℃; for 24h; effect on poliamine content and ratio in rice embryos of Oryza sativa;

...Expand

: 12651-38-6
(-)-Verbaskine

A: 71-44-3
Spermine

B: 140-10-3
(E)-3-phenylacrylic acid

Conditions

Conditions	Yield
With hydrogenchloride at 150℃; for 18h; sealed tube;

: 73397-39-4
1-(4-Amino-butyl)-tetrahydro-pyrimidin-2-one

: 107-13-1
acrylonitrile

: 71-44-3
Spermine

Conditions

Conditions	Yield
Yield given. Multistep reaction;

: 77485-28-0
N'-(4-(N'-hexahydropyrimidyl) butyl)-hexahydro-pyrimidine

A: 50-00-0
formaldehyd

B: 71-44-3
Spermine

Conditions

Conditions	Yield
With hydrogenchloride Heating;

: 185250-13-9
1,1'-(butane-1,4-diyl)-2,2'-diphenylbis(hexahydropyrimidine)

A: 71-44-3
Spermine

B: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With hydrogenchloride at 20℃;

1.4-bis-<γ-bromo-propylamino>-butane dihydrobromide: 1.4-bis-<γ-bromo-propylamino>-butane dihydrobromide

: 71-44-3
Spermine

Conditions

Conditions	Yield
With ethanol; ammonia at 100℃;

: 110-60-1
1,4-diaminobutane

N-<γ-iodo-propyl>-phthalimide: N-<γ-iodo-propyl>-phthalimide

: 71-44-3
Spermine

Conditions

Conditions	Yield
at 100℃; anschl. mit wss. KOH, anschl. Erhitzen mit HCl auf 100grad;

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Chemistry

Product Name: Diaminopropyltetramethylenediamine (CAS NO.71-44-3)

Empirical Formula: C₁₀H₂₆N₄
Molecular Weight: 202.3402
EINECS: 206-189-8
Melting point: 310-311 °C (dec.)(lit.)
Appearance: Clear colorless liquid
Storage temp.: 2-8°C
Solubility: H₂O: 1 M at 20 °C, clear, colorless
Form: Powder
Sensitive: Air Sensitive & Hygroscopic
Stable: Stable. Reacts with water.
Index of Refraction: 1.484
Density: 0.925 g/cm³
Flash Point: 175.6 °C
Enthalpy of Vaporization: 54.91 kJ/mol
Boiling Point: 308.4 °C at 760 mmHg
Vapour Pressure: 0.000683 mmHg at 25 °C
Surface Tension: 38.3 dyne/cm
Index of Refraction: 1.484
Molar Refractivity: 62.63 cm³
Molar Volume: 218.5 cm³
XLogP3-AA: -1.1
H-Bond Donor: 4
H-Bond Acceptor: 4
Structure Descriptors of Diaminopropyltetramethylenediamine (CAS NO.71-44-3):
IUPAC Name: N,N'-bis(3-aminopropyl)butane-1,4-diamine
Canonical SMILES: C(CCNCCCN)CNCCCN
InChI: InChI=1S/C10H26N4/c11-5-3-9-13-7-1-2-8-14-10-4-6-12/h13-14H,1-12H2
InChIKey: PFNFFQXMRSDOHW-UHFFFAOYSA-N
Product Categories: Aliphatics; Amines

Uses

Diaminopropyltetramethylenediamine (CAS NO.71-44-3) can be used as an organic phosphorus pesticide intermediats. At the same time, it is a typical anionic surfactant with good penetration, emulsification, foam and decontamination capabilities, so it is widely used in chemical, pesticide, fiber, electric crossing, mineral and other industries, especiallily for cosmetics, toothpaste, shampoo and other manufacturings. In the textile industry, it is used for washing wool and silk.

Production

Take coconut oil as the raw material and then with Sulfuric acid by sulfonation to get: Diaminopropyltetramethylenediamine (CAS NO.71-44-3).

Toxicity Data With Reference

1.	mmo-sat 100 µmol/L	AMACCQ Antimicrobial Agents and Chemotherapy. 9 (1976),77.
2.	cyt-hmn:hla 2 mmol/L	JCLLAX Journal of Cellular Physiology. 78 (1971),217.
3.	dni-rat:lvr 100 µmol/L	BIJOAK Biochemical Journal. 146 (1975),697.
4.	ipr-rat LD50:33 mg/kg	TXAPA9 Toxicology and Applied Pharmacology. 88 (1987),433.
5.	ivn-rat LD50:65 mg/kg	AIPTAK Archives Internationales de Pharmacodynamie et de Therapie. 165 (1967),374.
6.	orl-mus LD30:650 mg/kg	AGACBH Agents and Actions, A Swiss Journal of Pharmacology. 14 (1984),228.
7.	ipr-mus LDLo:8 mg/kg	TXAPA9 Toxicology and Applied Pharmacology. 23 (1972),288.
8.	scu-mus LD30:280 mg/kg	AGACBH Agents and Actions, A Swiss Journal of Pharmacology. 14 (1984),228.
9.	ivn-mus LD50:56 mg/kg	CSLNX* U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. (Aberdeen Proving Ground, MD 21010) NX#00641 .

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by intraperitoneal, subcutaneous, and intravenous routes. Moderately toxic by ingestion. Human mutation data reported. When heated to decomposition it emits toxic fumes of NO_x. See also AMINES.
Safety Information of Diaminopropyltetramethylenediamine (CAS NO.71-44-3):
Hazard Codes: Irritant Xi, Corrosive C
Risk Statements: 36/38-34
R34:Causes burns.
R36/38:Irritating to eyes and skin.
Safety Statements: 26-36-45-36/37/39-27
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S27:Take off immediately all contaminated clothing.
S36:Wear suitable protective clothing.
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
S45:In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)

Specification

Diaminopropyltetramethylenediamine , its cas register number is 71-44-3. It also can be called N,N'-Bis(3-aminopropyl)-1,4-butandiamin ; N,N'-Bis(3-aminopropyl)tetramethylenediamine ; 4,9-Diazadodecamethylenediamine ; and 1,4-Butanediamine, N1,N4-bis(3-aminopropyl)- .