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Basic Information
| CAS No.: | 74058-71-2 |
|---|---|
| Name: | Hexadecanamide, N-(phenylmethyl)- |
| Article Data: | 16 |
| Molecular Structure: | |
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|
|
| Formula: | C23H39NO |
| Molecular Weight: | 345.569 |
| Synonyms: | N-benzylhexylhexadecanamide;N-hexadecanoyl benzylamine;N-Benzyl-palmitamid;N-benzylpalmitamide;N-Benzyl-palmitinamid;N-benzyl-hexadecanamide; |
| Density: | 0.919±0.06 g/cm3(Predicted) |
| Melting Point: | 95-96℃ |
| Boiling Point: | 501.9±29.0 °C(Predicted) |
| PSA: | 32.59000 |
| LogP: | 7.62440 |
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Synthetic route
- 100663-86-3
C28H40N2O2
- 100-46-9
benzylamine
A
- 74058-71-2
hexadecanoic acid benzylamide
B
- 14178-31-5
(E)-2-pyridylphenyl ketoxime
Conditions
| Conditions | Yield |
|---|---|
| In dichloromethane for 24h; Ambient temperature; | A 99% B 100% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| In dichloromethane for 0.0333333h; Ambient temperature; | 96% |
Conditions
| Conditions | Yield |
|---|---|
| at 50 - 60℃; for 16h; | 94% |
Conditions
| Conditions | Yield |
|---|---|
| With mesoporous silica MCM-41 In toluene for 12h; Reflux; | 92% |
| Stage #1: 1-hexadecylcarboxylic acid With Bromotrichloromethane; triphenylphosphine In dichloromethane for 0.75h; Reflux; Stage #2: benzylamine In dichloromethane for 14h; Reflux; | 89% |
| Stage #1: 1-hexadecylcarboxylic acid With 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 2h; Stage #2: benzylamine With dmap In dichloromethane at 20℃; for 18h; | 86% |
Conditions
| Conditions | Yield |
|---|---|
| With indium (III) iodide at 110 - 120℃; for 8.5h; | 91% |
| at 150℃; |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: n-tetradecanoic acid With 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 2h; Stage #2: benzylamine With dmap In dichloromethane at 20℃; for 18h; | 89% |
- 18414-58-9
diphenylmethylsilanecarboxylic acid
- 100-46-9
benzylamine
- 74058-71-2
hexadecanoic acid benzylamide
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: pentadecylzinc(II) bromide With (2-morpholino-N-(quinolin-8-yl)acetamido)nickel(II) chloride In tetrahydrofuran; N,N-dimethyl acetamide at 20℃; for 0.5h; Inert atmosphere; Glovebox; Stage #2: diphenylmethylsilanecarboxylic acid; benzylamine With potassium fluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 2h; Inert atmosphere; Sealed tube; Glovebox; | 46% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: DCC-DMAP 2: 99 percent / CH2Cl2 / 24 h / Ambient temperature View Scheme |
- 112-67-4
n-hexadecanoyl chloride
- 74058-71-2
hexadecanoic acid benzylamide
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: Et3N 2: 99 percent / CH2Cl2 / 24 h / Ambient temperature View Scheme |
