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CAS No.: | 7789-89-1 |
---|---|
Name: | 1,1,1-Trichloropropane |
Article Data: | 26 |
Molecular Structure: | |
Formula: | C3H5Cl3 |
Molecular Weight: | 147.432 |
Synonyms: | 1,1,1-trichloro-propane;ethyl ester of t-butyloxycarbonyl-L-phenylalanine;Propane, 1,1,1-trichloro-;Trichloro-1,1,1-propan;1,1,1-Trichlor-propan;propylidyne trichloride; |
Density: | 1.2835 |
Melting Point: | -36.84°C (estimate) |
Boiling Point: | 116.85°C |
Safety: | Mildly toxic by ingestion and inhalation routes. A human eye irritant. An experimental skin and severe eye irritant. When heated to decomposition it emits toxic fumes of Cl−. See also CHLORINATED HYDROCARBONS, ALIPHATIC. |
PSA: | 0.00000 |
LogP: | 2.76660 |
tetrachloromethane
ethyl bis(N-butyl-N-isobutenylamido)phosphite
A
1,1,1-trichloropropane
Conditions | Yield |
---|---|
at 20℃; for 3h; | A 83.8% B 53.1% |
ethyl bis(N-butyl-N-isobutenylamido)phosphite
A
1,1,1-trichloropropane
Conditions | Yield |
---|---|
With tetrachloromethane at 20℃; for 3h; | A 83.8% B 53.1% |
triethylsilane
3,3,3-trichloro-1-propene
A
1,1,1-trichloropropane
B
1,1-dichloropropene
C
3,3,3-trichloropropyltriethylsilane
D
hexa-Si-ethyl-Si,Si'-propanediyl-bis-silane
Conditions | Yield |
---|---|
With dihydrogen hexachloroplatinate; isopropyl alcohol at 20℃; for 48h; Further byproducts given. Title compound not separated from byproducts; | A 17% B 55% C 7% D 0.4% |
3,3,3-trichloro-1-propene
A
1,1,1-trichloropropane
B
1,1-dichloropropene
C
3,3,3-trichloropropyltriethylsilane
D
hexa-Si-ethyl-Si,Si'-propanediyl-bis-silane
Conditions | Yield |
---|---|
With triethylsilane; dihydrogen hexachloroplatinate; isopropyl alcohol at 20℃; for 48h; Further byproducts given; | A 17% B 55% C 7% D 0.4% |
3,3,3-trichloro-1-propene
A
1,1,1-trichloropropane
B
1,1-dichloropropene
C
((E)-1-Chloro-propenyl)-triethyl-silane
D
((Z)-1-Chloro-propenyl)-triethyl-silane
Conditions | Yield |
---|---|
With triethylsilane; dihydrogen hexachloroplatinate; isopropyl alcohol at 20℃; for 48h; Further byproducts given; | A 17% B 55% C n/a D n/a |
Conditions | Yield |
---|---|
With iodine; chlorine |
Conditions | Yield |
---|---|
Chlorierung in der Gasphase im Licht; |
Conditions | Yield |
---|---|
With water; dibenzoyl peroxide at 100℃; under 73550.8 Torr; |
Conditions | Yield |
---|---|
With hydrogenchloride; aluminium trichloride at 5 - 10℃; |
3,3,3-trichloro-1-propene
A
1,1,1-trichloropropane
B
1,1,1-trichloro-3-iodo-propane
Conditions | Yield |
---|---|
With hydrogen iodide |
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1. | eye-hmn 100 ppm/15M | JIHTAB Journal of Industrial Hygiene and Toxicology. 28 (1946),262. | ||
2. | skn-rbt 10 mg/24H MLD | AMIHBC AMA Archives of Industrial Hygiene and Occupational Medicine. 10 (1954),61. | ||
3. | eye-rbt 20 mg SEV | AMIHBC AMA Archives of Industrial Hygiene and Occupational Medicine. 10 (1954),61. | ||
4. | orl-rat LD50:7460 mg/kg | AIHAAP American Industrial Hygiene Association Journal. 23 (1962),95. | ||
5. | ihl-rat LCLo:8000 ppm/4H | AIHAAP American Industrial Hygiene Association Journal. 23 (1962),95. |