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Basic Information
CAS No.: 796-77-0
Name: 4-[2-(diethylamino)ethoxy]benzophenone
Molecular Structure:
Molecular Structure of 796-77-0 (4-[2-(diethylamino)ethoxy]benzophenone)
Formula: C19H23 N O2
Molecular Weight: 297.397
Synonyms: Benzophenone,4-[2-(diethylamino)ethoxy]- (6CI,7CI,8CI); 4-(b-Diethylaminoethoxy)benzophenone; 4-[2-(Diethylamino)ethoxy]benzophenone
Density: 1.057g/cm3
Boiling Point: 430.1°C at 760 mmHg
Flash Point: 213.9°C
PSA: 29.54000
LogP: 3.63820
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Conditions
ConditionsYield
With potassium carbonate In acetone for 6h; Heating;97%
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Conditions
ConditionsYield
(i) Na, (ii) /BRN= 605300/; Multistep reaction;
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4-[2-(N,N-diethylamino)ethoxy]benzophenone

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Conditions
ConditionsYield
With water-d2; magnesium; ethylene dibromide In tetrahydrofuran at 70℃; for 2h; Inert atmosphere; Schlenk technique;51%
With water-d2; magnesium; ethylene dibromide In tetrahydrofuran51%
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Conditions
ConditionsYield
With titanium tetrachloride; zinc In tetrahydrofuran 1) reflux, 2 h, 2) r.t.;49%
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benzyl ethyl ketone

796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

2-benzyl-1-phenyl-1-[4-(diethylaminoethoxy)phenyl]but-1-ene

Conditions
ConditionsYield
With titanium tetrachloride; zinc In 1,4-dioxane for 4h; Heating;40%
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3-methoxy-4-(phenylmethoxy)benzaldehyde

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Conditions
ConditionsYield
With titanium tetrachloride; zinc In tetrahydrofuran 1) reflux, 2 h, 2) r.t.;36%
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4-[2-(N,N-diethylamino)ethoxy]benzophenone

3536-96-7

vinylmagnesium chloride

56431-04-0

1-[4-(2-Diethylamino-ethoxy)-phenyl]-1-phenyl-prop-2-en-1-ol

Conditions
ConditionsYield
In tetrahydrofuran
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4-[2-(N,N-diethylamino)ethoxy]benzophenone

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ethylmagnesium bromide

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4-(β-diethylaminoethoxy)-α-ethyl-benzhydrol

Conditions
ConditionsYield
In diethyl ether
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4-[2-(N,N-diethylamino)ethoxy]benzophenone

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clomiphene

Conditions
ConditionsYield
With tert.-butyl lithium 1.) THF/pentane, -78 deg C, 30 min; 2.) THF, reflux; Yield given. Multistep reaction;
74-96-4

ethyl bromide

796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

56431-20-0

4-(β-diethylaminoethoxy)-α-ethyl-benzhydrol

Conditions
ConditionsYield
With magnesium
With magnesium
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