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CAS No.: | 869-24-9 |
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Name: | 2-Diethylaminoethylchloride hydrochloride |
Article Data: | 13 |
Molecular Structure: | |
Formula: | C6H14ClN.HCl |
Molecular Weight: | 172.098 |
Synonyms: | 1-Chloro-2-(diethylamino)ethane hydrochloride;2-Chlorotriethylamine hydrochloride;2-(N,N-Diethylamino)ethyl chloride hydrochloride;2-Chloro-N,N-diethylethylaminehydrochloride;2-Chloroethyldiethylammoniumchloride;N,N-Diethyl-b-chloroethylamine hydrochloride;N-2-Chloroethyl-N,N-diethylammoniumhydrochloride;b-Chloroethyldiethylamine hydrochloride;2-(Diethylamino)ethyl chloridehydrochloric acid salt;Ethanamine,2-chloro-N,N-diethyl-, hydrochloride (9CI);Triethylamine, 2-chloro-,hydrochloride (6CI,7CI,8CI);(2-Chloroethyl)diethylamine monohydrochloride;(N,N-Diethylamino)ethyl chloride hydrochloride;2-Diethylaminoethyl chloridemonohydrochloride;N,N-Diethyl-2-chloroethylamine hydrochloride; |
EINECS: | 212-786-4 |
Density: | 1.1919 (rough estimate) |
Melting Point: | 208-212 °C |
Boiling Point: | 114 °C at 760 mmHg |
Flash Point: | 22.8 °C |
Solubility: | 2000 g/L (20 °C) in water |
Appearance: | Colourless to beige crystals |
Hazard Symbols: | Xn, T, Xi, T+ |
Risk Codes: | 22-36/37/38-26-24/25-23/24/25 |
Safety: | 26-36-45-36/37/39-28A |
Transport Information: | UN 2811 6.1/PG 2 |
PSA: | 3.24000 |
LogP: | 2.36900 |
Conditions | Yield |
---|---|
Stage #1: 2-(Diethylamino)ethanol With thionyl chloride In dichloromethane at -10 - 35℃; for 2.5h; Stage #2: With hydrogenchloride | 98.08% |
With thionyl chloride; chloroform at -5℃; | |
With thionyl chloride In chloroform |
Conditions | Yield |
---|---|
Stage #1: diethylamine; 2-chloro-ethanol for 4h; Reflux; Stage #2: With thionyl chloride In tetrachloromethane at 20℃; for 4h; | 46.6% |
Stage #1: diethylamine; 2-chloro-ethanol In toluene for 2h; Reflux; Stage #2: With thionyl chloride In toluene at 20℃; for 4h; Cooling with ice; | 3.3 g |
Conditions | Yield |
---|---|
at 70℃; for 2h; | 44.7% |
1,1,4,4-tetraethyl-piperazinediium; dichloride
2-chloro-N,N-diethylethylamine hydrochloride
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 33℃; Equilibrium constant; Decomposition; |
B
2-chloro-N,N-diethylethylamine hydrochloride
B
2-chloro-N,N-diethylethylamine hydrochloride
2-chloro-N,N-diethylethylamine hydrochloride
3-methyl-1,8-dihydrocycloheptapyrazol-8-one
1-<2-(diethylamino)ethyl>-3-methyl-1,8-dihydrocycloheptapyrazol-8-one
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 6h; Heating; | 100% |
2-chloro-N,N-diethylethylamine hydrochloride
methyl 4-butyloxy-3-hydroxybenzoate
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 16h; Heating; | 100% |
2-chloro-N,N-diethylethylamine hydrochloride
Conditions | Yield |
---|---|
Stage #1: 2-oxo-7-(trifluoromethyl)-1-[3-(trifluoromethyl)benzyl]-2,3-dihydro-1H-benzimidazole-5-carbonitrile With sodium hydride In DMF (N,N-dimethyl-formamide) at 20℃; for 0.166667h; Stage #2: 2-chloro-N,N-diethylethylamine hydrochloride With triethylamine In DMF (N,N-dimethyl-formamide) at 70℃; for 1.5h; | 100% |
2-chloro-N,N-diethylethylamine hydrochloride
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 16h; | 100% |
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1. | mmo-sat 500 µmol/L | ENMUDM Environmental Mutagenesis. 3 (1981),11. | ||
2. | mmo-esc 1 µmol/L | JPPMAB Journal of Pharmacy and Pharmacology. 31 (1979),67P. | ||
3. | dns-rat:lvr 100 µmol/L | ENMUDM Environmental Mutagenesis. 3 (1981),11. | ||
4. | msc-mus:lym 22 µmol/L | ENMUDM Environmental Mutagenesis. 3 (1981),33. | ||
5. | ipr-rat LD50:30 mg/kg | CPBTAL Chemical and Pharmaceutical Bulletin. 8 (1960),807. | ||
6. | orl-mus LDLo:320 mg/kg | AECTCV Archives of Environmental Contamination and Toxicology. 14 (1985),111. | ||
7. | ipr-mus LD50:71 mg/kg | JPETAB Journal of Pharmacology and Experimental Therapeutics. 94 (1948),249. | ||
8. | scu-mus LD50:100 mg/kg | JPETAB Journal of Pharmacology and Experimental Therapeutics. 91 (1947),224. | ||
9. | ivn-mus LD50:100 mg/kg | JPETAB Journal of Pharmacology and Experimental Therapeutics. 91 (1947),224. | ||
10. | ivn-rbt LDLo:40 mg/kg | JPETAB Journal of Pharmacology and Experimental Therapeutics. 91 (1947),224. | ||