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86087-23-2

Basic Information
CAS No.: 86087-23-2
Name: (S)-(+)-3-Hydroxytetrahydrofuran
Molecular Structure:
Molecular Structure of 86087-23-2 ((S)-(+)-3-Hydroxytetrahydrofuran)
Formula: C4H8O2
Molecular Weight: 88.11
Synonyms: 3-Furanol,tetrahydro-, (S)-;(+)-3-Hydroxytetrahydrofuran;(S)-(+)-Tetrahydrofuran-3-ol;(S)-3-Hydroxytetrahydrofuran;(S)-Tetrahydro-3-furanol;3S-Hydroxytetrahydrofuran;
EINECS: 1308068-626-2
Density: 1.148 g/cm3
Melting Point:
Boiling Point: 181 °C at 760 mmHg
Flash Point: 81.1 °C
Solubility: soluble in water
Appearance: clear liquid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-37/39
Transport Information:
PSA: 29.46000
LogP: -0.23240
Synthetic route
139013-68-6

(3S)-4-chloro-1,3-butanediol

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With hydrogenchloride; sodium hydroxide In methanol; water99.8%
With potassium hydroxide In methanol at 40℃; for 4h; Reagent/catalyst;97%
In anhydrous ethylene glycol dimethyl ether at 110℃; for 5h; Product distribution / selectivity;90%
145873-44-5

4-chloro-3-hydroxy-1-butanol

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With hydrogenchloride In water at 50℃; for 4h; Solvent; Reagent/catalyst;94.6%

(S)-3-(4-Methoxy-benzyloxy)-tetrahydro-furan

A

83318-92-7

ethyl p-methoxybenzyl sulfide

B

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With aluminium trichloride; ethanethiol In dichloromethane for 5h; Ambient temperature;A n/a
B 93%
42890-76-6

(S)-1,2,4-butanetriol

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With toluene-4-sulfonic acid (3a preparation above 7a);87%
toluene-4-sulfonic acid In PEG-400 at 120 - 160℃; under 10 Torr; for 12h; Product distribution / selectivity;83%
strong acid ion exchange resin (Amberlyst 15, H+ form) In 1,4-dioxane at 90 - 120℃; under 760.051 - 5931.67 Torr; Product distribution / selectivity;70%
With toluene-4-sulfonic acid
With toluene-4-sulfonic acid In water at 90℃;10 g

(S)-tetrahydrofuran-3-yl acetate

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 20℃; for 3h;83%

(S)-3-benzyloxytetrahydrofuran

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen at 40℃;81.5%
86087-24-3

(R)-3-Hydroxytetrahydrofuran

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
Stage #1: (R)-3-Hydroxytetrahydrofuran With azodicarboxylic acid bis(2-methoxyethyl) ester; 4-diphenylphosphanobenzoic acid In tetrahydrofuran at 20℃; for 0.166667h;
Stage #2: With water; sodium hydroxide In tetrahydrofuran at 20℃; stereospecific reaction;
64%
115914-74-4

2-(oxiran-2-yl)ethyl 4-methylbenzenesulfonate

A

86087-23-2

(S)-3-hydroxytetyrahydrofurane

B

2-((R)-oxiran-2-yl)ethyl 4-methylbenzenesulfonate

Conditions
ConditionsYield
With (S,S)-(salen)cobalt(III)(OAc); water In tetrahydrofuran at 0 - 25℃; for 14h; optical yield given as %ee; enantioselective reaction;A 48%
B 47%
1191-99-7

2,3-dihydro-2H-furan

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
Yield given. Multistep reaction;
1708-29-8

2,5-dihydrofuran

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
Multistep reaction;
Yield given. Multistep reaction;

(S)-3-(trichlorosilyl)tetrahydrofuran

A

86087-24-3

(R)-3-Hydroxytetrahydrofuran

B

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate In tetrahydrofuran; methanol for 16h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
145873-44-5

4-chloro-3-hydroxy-1-butanol

A

1708-29-8

2,5-dihydrofuran

B

86087-24-3

(R)-3-Hydroxytetrahydrofuran

C

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With hydrogenchloride for 2h; Heating;A 15 % Chromat.
B n/a
C n/a
With hydrogenchloride for 2h; Heating; Yields of byproduct given. Title compound not separated from byproducts;A 15 % Chromat.
B n/a
C n/a
453-20-3

3-Hydroxytetrahydrofuran

A

86087-24-3

(R)-3-Hydroxytetrahydrofuran

B

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With vinyl acetate; Candida antarctica B lipase on carrier C3 In hexane at 37℃; for 0.0833333h; Title compound not separated from byproducts;
27999-96-8

(+/-)-tetrahydrofuran-3-yl acetate

A

86087-24-3

(R)-3-Hydroxytetrahydrofuran

B

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With sodium phosphate buffer; esterase B from Candida antarctica In water at 37℃; for 1h; pH=7.3; Product distribution;
167971-73-5

(2S)-2-tert-Butoxy-1,4-butanediol

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With toluene-4-sulfonic acid at 18 - 77℃; under 12.5 - 15 Torr;
453-20-3

3-Hydroxytetrahydrofuran

108-05-4

vinyl acetate

A

86087-24-3

(R)-3-Hydroxytetrahydrofuran

B

86087-23-2

(S)-3-hydroxytetyrahydrofurane

C

(R)-tetrahydrofuran-3-yl acetate

D

(S)-tetrahydrofuran-3-yl acetate

Conditions
ConditionsYield
With EL-14 lipase In hexane at 4℃; for 16h; Enzymatic reaction; optical yield given as %ee; enantioselective reaction;
778-29-0

but-3-enyl 4-methylbenzenesulfonate

A

86087-24-3

(R)-3-Hydroxytetrahydrofuran

B

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With potassium osmate(VI) dihydrate; methanesulfonamide; water; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III) In tert-butyl alcohol at 0℃; for 6h; Sharpless asymmetric dihydroxylation; optical yield given as %ee;
27999-96-8

(+/-)-tetrahydrofuran-3-yl acetate

A

86087-23-2

(S)-3-hydroxytetyrahydrofurane

B

(R)-tetrahydrofuran-3-yl acetate

Conditions
ConditionsYield
With crude extract of Escherichia coli DH5α cells containing Bacillus stearothermophilus esterase, D31T/L93F mutant In aq. phosphate buffer at 37℃; for 42h; pH=7.5; Reagent/catalyst; Enzymatic reaction; enantioselective reaction;
22929-52-8

tetrahydrofuran-3-one

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With nicotinamide adenine dinucleotide In aq. phosphate buffer; acetonitrile at 30℃; for 4h; pH=7.4; Kinetics; Reagent/catalyst; Enzymatic reaction; enantioselective reaction;n/a
With alcohol dehydrogenase fromThermoanaerobacter brockii, A85V/I86L/L294Q mutant; NADP; lysozyme; DNase I In isopropyl alcohol at 30℃; for 16h; Enzymatic reaction; stereoselective reaction;n/a

C7H18NO2(1+)*Cl(1-)

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With sodium hydroxide In dimethyl sulfoxide at 170 - 190℃; Reagent/catalyst; Inert atmosphere;
22929-52-8

tetrahydrofuran-3-one

A

86087-24-3

(R)-3-Hydroxytetrahydrofuran

B

86087-23-2

(S)-3-hydroxytetyrahydrofurane

Conditions
ConditionsYield
With alcohol dehydrogenase fromThermoanaerobacter brockii, A85V/I86L/L294H mutant; NADP; lysozyme; DNase I In isopropyl alcohol at 30℃; for 16h; Enzymatic reaction; stereoselective reaction;A n/a
B n/a
With alcohol dehydrogenase fromThermoanaerobacter brockii, L294C mutant; NADP; lysozyme; DNase I In isopropyl alcohol at 30℃; for 16h; Enzymatic reaction; stereoselective reaction;A n/a
B n/a
74124-79-1

di(succinimido) carbonate

86087-23-2

(S)-3-hydroxytetyrahydrofurane

138499-08-8

1-({[(3S)-tetrahydro-3-furanyloxy]carbonyl}oxy)-2,5-pyrrolidinedione

Conditions
ConditionsYield
With triethylamine In acetonitrile at 20℃; for 18h;100%
With triethylamine In acetonitrile at 20℃; for 18h;100%
With triethylamine In acetonitrile at 20℃; for 21.5h;94%
86087-23-2

(S)-3-hydroxytetyrahydrofurane

3-cyanocarbonyl-3'-methoxycarbonyl-2,2'-binaphthalene

[2,2']Binaphthalenyl-1,3'-dicarboxylic acid 1-methyl ester 3'-(S)-(tetrahydro-furan-3-yl) ester

Conditions
ConditionsYield
With dmap In acetonitrile at 20℃;100%
86087-23-2

(S)-3-hydroxytetyrahydrofurane

229495-94-7

Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester 4-nitro-phenyl ester

229495-71-0

Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester (S)-(tetrahydro-furan-3-yl) ester

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane for 48h; Heating;100%
752242-45-8

3-hydroxy-5-(4-methanesulfonylphenoxy)benzoic acid methyl ester

86087-23-2

(S)-3-hydroxytetyrahydrofurane

1001420-25-2

C19H20O7S

Conditions
ConditionsYield
With 4,4-(dimethyl-1,1-dioxido-1,2,5-thiadiazolidin-2-yl)-triphenyl phosphonium In dichloromethane; toluene at 20℃; for 15h;100%
86087-23-2

(S)-3-hydroxytetyrahydrofurane

98-59-9

p-toluenesulfonyl chloride

112052-11-6

toluene-4-sulfonic acid (S)-(tetrahydrofuran-3-yl)ester

Conditions
ConditionsYield
With 1H-imidazole; dmap In dichloromethane at 20℃; for 16h;100%
With pyridine100%
With trimethylamine hydrochloride; triethylamine In dichloromethane at 0 - 20℃; for 4h;99%
1037093-11-0

(3-fluoro-2-hydroxy-5-nitro-benzyl)-methyl-carbamic acid tert-butyl ester

86087-23-2

(S)-3-hydroxytetyrahydrofurane

1508296-65-8

(R)-tert-butyl 3-fluoro-5-nitro-2-((tetrahydrofuran-3-yl)oxy)benzyl(methyl)carbamate

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 16.5h;100%
358-23-6

trifluoromethylsulfonic anhydride

86087-23-2

(S)-3-hydroxytetyrahydrofurane

(S)-tetrahydrofuran-3-yl trifluoromethanesulfonate

Conditions
ConditionsYield
Stage #1: trifluoromethylsulfonic anhydride With N-ethyl-N,N-diisopropylamine In dichloromethane at -78℃; for 0.0833333h; Inert atmosphere;
Stage #2: (S)-3-hydroxytetyrahydrofurane In dichloromethane at -78 - 20℃; for 3h; Inert atmosphere;
100%
With pyridine In dichloromethane at -10℃; for 0.5h;
86087-23-2

(S)-3-hydroxytetyrahydrofurane

162012-67-1

N-(3-chloro-4-fluorophenyl)-7-fluoro-6-nitroquinazolin-4-amine

4-[(3-chloro-4-fluorophenyl)amino]-6-nitro-7-[(S)-(tetrahydrofuran-3-yl)oxy]quinazoline

Conditions
ConditionsYield
Stage #1: (S)-3-hydroxytetyrahydrofurane With potassium tert-butylate In tetrahydrofuran at 20℃; for 1h;
Stage #2: N-(3-chloro-4-fluorophenyl)-7-fluoro-6-nitroquinazolin-4-amine In tetrahydrofuran at 20℃; for 3h;
99.5%
Stage #1: (S)-3-hydroxytetyrahydrofurane With sodium hydride In tetrahydrofuran; mineral oil for 0.75h; Cooling with ice;
Stage #2: N-(3-chloro-4-fluorophenyl)-7-fluoro-6-nitroquinazolin-4-amine In tetrahydrofuran at 20℃; for 5h;
99.5%
Stage #1: (S)-3-hydroxytetyrahydrofurane With sodium hydride In tetrahydrofuran; mineral oil for 0.75h; Cooling with ice;
Stage #2: N-(3-chloro-4-fluorophenyl)-7-fluoro-6-nitroquinazolin-4-amine In tetrahydrofuran; mineral oil at 20℃; for 5h;
99.5%

4-[(3-chloro-4-fluorophenyl)amino]-6-nitro-7-fluoroquinazoline

86087-23-2

(S)-3-hydroxytetyrahydrofurane

4-nitro-7-[(S)-(tetrahydrofuran-3-yl)oxy]quinazoline

Conditions
ConditionsYield
Stage #1: (S)-3-hydroxytetyrahydrofurane With sodium hydride In tetrahydrofuran; mineral oil for 0.75h; Cooling with ice;
Stage #2: 4-[(3-chloro-4-fluorophenyl)amino]-6-nitro-7-fluoroquinazoline In tetrahydrofuran; mineral oil at 20℃; for 5h;
99.5%
1309831-35-3

1-(2-fluoro-5-nitrophenyl)-4-methyl-1H-tetrazol-5(4H)-one

86087-23-2

(S)-3-hydroxytetyrahydrofurane

1-(2-((S)-tetrahydrofuran-3-yloxy)-5-nitrophenyl)-4-methyl-1H-tetrazol-5(4H)-one

Conditions
ConditionsYield
Stage #1: (S)-3-hydroxytetyrahydrofurane With potassium tert-butylate In tetrahydrofuran at 0℃; for 0.333333h; Inert atmosphere;
Stage #2: 1-(2-fluoro-5-nitrophenyl)-4-methyl-1H-tetrazol-5(4H)-one In tetrahydrofuran at 0 - 20℃; for 2.16667h;
98%
179552-73-9

4-((3-chloro-4-fluorophenyl)amino)-6-nitro-7-chloroquinazoline

86087-23-2

(S)-3-hydroxytetyrahydrofurane

4-[(3-chloro-4-fluorophenyl)amino]-6-nitro-7-[(S)-(tetrahydrofuran-3-yl)oxy]quinazoline

Conditions
ConditionsYield
Stage #1: (S)-3-hydroxytetyrahydrofurane With potassium tert-butylate In N,N-dimethyl-formamide at 0℃; for 2h;
Stage #2: 7-chloro-N-(3-chloro-4-fluorophenyl)-6-nitroquinazolin-4-amine With sodium benzenesulfonate In N,N-dimethyl-formamide at 30 - 90℃; for 6h;
97.8%
With potassium tert-butylate; sodium methansulfinate In N,N-dimethyl-formamide at 80℃; for 3h; Reagent/catalyst; Solvent; Temperature;93%

2-(chloromethyl)-4-hydroxy-5,8-dihydropyridine[3,4-d]pyrimidine-7(6H)-carboxylic acid tert-butyl ester

86087-23-2

(S)-3-hydroxytetyrahydrofurane

3(S)-4-hydroxy-2-(((tetrahydrofuran-3-yl)oxy)methyl)-5,8-dihydropyridin[3,4-d]pyrimidine-7(6H)-carboxylic acid tert butyl ester

Conditions
ConditionsYield
Stage #1: (S)-3-hydroxytetyrahydrofurane With sodium hydride In N,N-dimethyl-formamide for 0.5h;
Stage #2: 2-(chloromethyl)-4-hydroxy-5,8-dihydropyridine[3,4-d]pyrimidine-7(6H)-carboxylic acid tert-butyl ester In N,N-dimethyl-formamide at 20℃; for 1h;
97%
86087-23-2

(S)-3-hydroxytetyrahydrofurane

124-63-0

methanesulfonyl chloride

347885-35-2

[(3S)-tetrahydrofuran-3-yl] methanesulfonate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice;96%
With triethylamine In dichloromethane at 20℃; Cooling with ice;83%
With triethylamine In dichloromethane at 0℃; for 4h;80%
1355011-30-1

methyl 6-(2,6-difluoro-4-hydroxyphenyl)-5-fluoropyridine-2-carboxylate

86087-23-2

(S)-3-hydroxytetyrahydrofurane

1395992-69-4

methyl 6-{2,6-difluoro-4-[(3R)-tetrahydrofuran-3-yloxy]phenyl}-5-fluoropyridine-2-carboxylate

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃;96%
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; for 2h;96%
86087-23-2

(S)-3-hydroxytetyrahydrofurane

104-15-4

toluene-4-sulfonic acid

112052-11-6

toluene-4-sulfonic acid (S)-(tetrahydrofuran-3-yl)ester

Conditions
ConditionsYield
Stage #1: (S)-3-hydroxytetyrahydrofurane With dmap; triethylamine In dichloromethane at 0℃; for 0.166667h;
Stage #2: toluene-4-sulfonic acid at 20 - 50℃; for 1.66667h;
96%
35421-08-0

4-hydroxybenzyl chloride

86087-23-2

(S)-3-hydroxytetyrahydrofurane

(3S)-3-[p-(chloromethyl)phenoxy]tetrahydrofuran

Conditions
ConditionsYield
Stage #1: 4-hydroxybenzyl chloride In dichloromethane at -5 - 0℃; for 3h;
Stage #2: (S)-3-hydroxytetyrahydrofurane With N-ethyl-N,N-diisopropylamine In tetrahydrofuran for 4.5h; Reagent/catalyst; Reflux;
95.3%
86087-23-2

(S)-3-hydroxytetyrahydrofurane

350-46-9

4-Fluoronitrobenzene

(S)-3-(4-nitrophenoxy)tetrahydrofuran

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 20 - 25℃; for 1h; Inert atmosphere;95%

C12H11Cl3N2O

86087-23-2

(S)-3-hydroxytetyrahydrofurane

C16H18Cl2N2O3

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃;94.3%
462-06-6

fluorobenzene

86087-23-2

(S)-3-hydroxytetyrahydrofurane

(S)-3-phenoxytetrahydrofuran

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran; tert-butyl alcohol at 0 - 10℃; for 1.5h; Inert atmosphere; Large scale;94%
With potassium tert-butylate In tetrahydrofuran at 0 - 10℃; for 1h; Inert atmosphere; Large scale;94%
915095-85-1

(2-chloro-5-bromophenyl)(4-fluorophenyl)methanone

86087-23-2

(S)-3-hydroxytetyrahydrofurane

915095-84-0

(S)-(5-bromo-2-chlorophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 100 - 110℃;93%
With potassium tert-butylate In tetrahydrofuran at 7 - 10℃; for 0.5h;87%
With potassium tert-butylate In tetrahydrofuran at 0 - 10℃; for 2h;85.3%

6-bromo-2-(2,5-dimethyl-1H-pyrrol-1-yl)-4-methylquinazolin-8-ol

86087-23-2

(S)-3-hydroxytetyrahydrofurane

(S)-6-bromo-2-(2,5-dimethyl-1H-pyrrol-1-yl)-4-methyl-8-((tetrahydrofuran-3-yl)oxy)quinazoline

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; Mitsunobu Displacement; Inert atmosphere;93%
86087-23-2

(S)-3-hydroxytetyrahydrofurane

149947-16-0

1-bromo-3-(bromomethyl)-2-fluorobenzene

(S)-3-((3-bromo-2-fluorobenzyl)oxy)tetrahydrofuran

Conditions
ConditionsYield
Stage #1: (S)-3-hydroxytetyrahydrofurane With sodium hydride In N,N-dimethyl-formamide for 1h; Inert atmosphere;
Stage #2: 1-bromo-3-(bromomethyl)-2-fluorobenzene In N,N-dimethyl-formamide for 17h; Inert atmosphere;
92.51%

C20H18ClF2N5O

86087-23-2

(S)-3-hydroxytetyrahydrofurane

4-[(3-chloro-4-fluorophenyl)amino]-6-{[4-(N,N-dimethylamino)-1-oxo-2-buten-1-yl]amino}-7-[(S)-(tetrahydrofuran-3-yl)oxy]quinazoline

Conditions
ConditionsYield
With potassium tert-butylate In methanol; tert-butyl alcohol at 50℃; for 1h; Solvent;92.5%
With potassium tert-butylate In tert-butyl alcohol at 50℃; for 1h; Reagent/catalyst; Solvent;89%
With potassium tert-butylate In tert-butyl alcohol at 50℃; for 1h; Solvent; Reagent/catalyst;89%
915095-86-2

(2-chloro-5-iodophenyl)(4-fluorophenyl)methanone

86087-23-2

(S)-3-hydroxytetyrahydrofurane

915095-87-3

(S)-(2-chloro-5-iodophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran at 16 - 25℃; for 3h;91.8%
Stage #1: (2-chloro-5-iodophenyl)(4-fluorophenyl)methanone; (S)-3-hydroxytetyrahydrofurane With potassium tert-butylate In tetrahydrofuran at 16 - 25℃; for 4h;
Stage #2: With water at 20 - 21℃; for 1.83333h;
91.8%
With potassium tert-butylate In tetrahydrofuran at 16 - 25℃; for 4h; Industry scale;91.8%
352-32-9

p-fluorotoluene

86087-23-2

(S)-3-hydroxytetyrahydrofurane

(S)-3-p-cresyltetrahydrofuran

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran at 0 - 10℃; for 1.5h; Inert atmosphere; Large scale;91%
86087-23-2

(S)-3-hydroxytetyrahydrofurane

74-88-4

methyl iodide

(S)-(+)-3-methoxytetrahydrofuran

Conditions
ConditionsYield
With sodium hydride In diethyl ether at 25℃; for 24h; Etherification;90%
1618663-21-0

6-(2,4-dichloro-7-((2-(trimethylsilyl)ethoxy)methyl)-7H-pyrrolo[2,3-d]pyrimidin-5-yl)-2-methylbenzo[d]oxazole

86087-23-2

(S)-3-hydroxytetyrahydrofurane

1618663-42-5

(S)-6-(2-chloro-4-((tetrahydrofuran-3-yl)oxy)-7-((2-(trimethylsilyl)ethoxy)methyl)-7H-pyrrolo[2,3-d]pyrimidin-5-yl)-2-methylbenzo[d]oxazole

Conditions
ConditionsYield
With sodium t-butanolate In 1,4-dioxane at 75℃; for 5h;90%
With sodium t-butanolate In 1,4-dioxane at 25℃; for 16h;68%
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  • (S)-(+)-3-Hydroxytetrahydrofuran

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    86087-23-2

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    (S)-(+)-3-Hydroxytetrahydrofuran

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    Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi

    Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,an

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  • (S)-(+)-3-Hydroxytetrahydrofuran

  • Casno:

    86087-23-2

    (S)-(+)-3-Hydroxytetrahydrofuran

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0/Gram

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    Business Type:Trading Company

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    1.Compitive Price 2.Best price 3. Best after-sale service Nanjing Chemipioneer Pharma&Tech Co.,Ltd founded in 2010, is a high-tech enterprise in pharma and chemical field, We mainly provide pharmaceutical raw materials and intermediates a

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    Business Type:Lab/Research institutions

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    Business Type:Lab/Research institutions

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    86087-23-2

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     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

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    86087-23-2

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    86087-23-2

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    Product Description Product website: http://www.finerchem.com/pro01en/id/1378.html Product Name (S)-(+)-3-Hydroxytetrahydrofuran CAS No. 86087-23-2

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    Business Type:Lab/Research institutions

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    86087-23-2

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    86087-23-2

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    Business Type:Lab/Research institutions

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    Business Type:Trading Company

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    86087-23-2

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    Business Type:Trading Company

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     China (Mainland)  |  Contact Details

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    Business Type:Lab/Research institutions

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    Business Type:Lab/Research institutions

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    86087-23-2

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    86087-23-2

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Chemistry

Product Name: (S)-(+)-3-Hydroxytetrahydrofuran (CAS NO.86087-23-2)

Molecular Formula: C4H8O2
Molecular Weight: 88.11g/mol
Mol File: 86087-23-2.mol
Appearance: Colourless Liquid
Boiling point: 181 °C at 760 mmHg
Flash Point:  81.1 °C 
Density: 1.148 g/cm3
Refractive index: n20/D 1.45(lit.)
Water Solubility: soluble
Stability: Stable. Combustible. Incompatible with strong oxidizing agents.
Index of Refraction: 1.475 
Molar Refractivity: 21.64 cm
Molar Volume: 76.7 cm3 
Surface Tension: 38.7 dyne/cm
Enthalpy of Vaporization: 48.57 kJ/mol
Vapour Pressure: 0.255 mmHg at 25°C
Product Categories: Alcohols, Hydroxy Esters and Derivatives; Chiral Compounds; Starting Raw Materials & Intermediates; Small molecule; Tetrahydrofuran Series; Chiral Reagents; Furans; Chiral Building Blocks; Simple Alcohols (Chiral); Synthetic Organic Chemistry

Safety Profile

Safety Information of (S)-(+)-3-Hydroxytetrahydrofuran (CAS NO.86087-23-2):
Hazard Codes: XiIrritant
Risk Statements: 36/37/38   
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-37/39 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S37/39:Wear suitable gloves and eye/face protection.
WGK Germany: 3

Specification

 (S)-(+)-3-Hydroxytetrahydrofuran , its CAS NO. is 86087-23-2, the synonyms are (3S)-tetrahydrofuran-3-ol  ; (S)-(+)-Tetrahydro-3-furanol .