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870-24-6

Basic Information
CAS No.: 870-24-6
Name: 2-Chloroethylamine hydrochloride
Article Data: 24
Molecular Structure:
Molecular Structure of 870-24-6 (2-Chloroethylamine hydrochloride)
Formula: C2H7Cl2N
Molecular Weight: 115.99
Synonyms: Ethanamine,2-chloro-, hydrochloride (9CI);Ethylamine, 2-chloro-, hydrochloride(6CI,7CI,8CI);1-Amino-2-chloroethane hydrochloride;2-Aminoethyl chloridehydrochloride;2-Chloroethylamine monohydrochloride;b-Chloroethylaminehydrochloride;2-Chloroethylamino Hydrochloride;
EINECS: 212-793-2
Density: 1.038 g/cm3
Melting Point: 140-150 °C(lit.)
Boiling Point: 108.9 °C at 760 mmHg
Flash Point: 19.7 °C
Solubility: Soluble in water
Appearance: white to light beige crystalline powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36-37/39
Transport Information: UN 3261
PSA: 26.02000
LogP: 1.68620
Synthetic route
2002-24-6

2-amino-ethanol hydrochloride

870-24-6

2-chloroethanamine hydrochloride

Conditions
ConditionsYield
With thionyl chloride In chloroform for 5h; Heating;100%
With thionyl chloride In N-methyl-acetamide; water; benzene98%
With thionyl chloride In toluene at 75℃; for 3h; Temperature; Concentration;95%
7719-09-7

thionyl chloride

2002-24-6

2-amino-ethanol hydrochloride

68-12-2, 33513-42-7

N,N-dimethyl-formamide

870-24-6

2-chloroethanamine hydrochloride

Conditions
ConditionsYield
In benzene97%
141-43-5

ethanolamine

870-24-6

2-chloroethanamine hydrochloride

Conditions
ConditionsYield
Stage #1: ethanolamine With hydrogenchloride; sodium hydroxide In water at 20℃; for 0.75h;
Stage #2: With hydrogenchloride; Adipic acid In water at 120℃; for 4h; Temperature; Reagent/catalyst;
92.2%
With hydrogenchloride; thionyl chloride 1) 0 deg C then toluene, azeotropic dist., 2) 85 deg C, 1 h; Yield given. Multistep reaction;
With thionyl chloride In chloroform for 0.5h; Reflux;
With thionyl chloride In chloroform Reflux; Cooling with ice;
151-56-4

ethyleneimine

870-24-6

2-chloroethanamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride
3891-07-4

N-(2-Hydroxyethyl)phthalimide

870-24-6

2-chloroethanamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride at 180 - 200℃;
870-24-6

2-chloroethanamine hydrochloride

689-98-5

chloroethylamine

Conditions
ConditionsYield
With triethylamine In acetonitrile at 5℃; for 1.5h; Inert atmosphere;100%
With triethylamine In acetonitrile at 5℃; for 1h; Inert atmosphere;100%
With sodium hydroxide In chloroform at 0℃;
24424-99-5

di-tert-butyl dicarbonate

870-24-6

2-chloroethanamine hydrochloride

71999-74-1

tert-butyl N-(2-chloroethyl)carbamate

Conditions
ConditionsYield
With sodium hydrogencarbonate In tetrahydrofuran; water at -10 - 25℃; for 24.5h; Inert atmosphere;100%
With triethylamine In dichloromethane for 72h;99%
With triethylamine In dichloromethane at 0 - 20℃; for 4h; Inert atmosphere;99%
2552-45-6

methyl 4-chloro-3,5-dinitrobenzoate

870-24-6

2-chloroethanamine hydrochloride

110991-77-0

methyl 4-((2-chloroethyl)amino)-3,5-dinitrobenzoate

Conditions
ConditionsYield
With triethylamine In methanol for 0.0833333h; Heating / reflux;100%
With triethylamine In ethanol Reflux;86%
With triethylamine In methanol at 80℃; for 1h;
870-24-6

2-chloroethanamine hydrochloride

24801-88-5

3-(triethoxypropyl) isocyanate

10387-40-3

potassium thioacetate

C14H30N2O5SSi

Conditions
ConditionsYield
Stage #1: 2-chloroethanamine hydrochloride; 3-(triethoxypropyl) isocyanate With sodium ethanolate In ethanol at -78 - -65℃; for 3h;
Stage #2: potassium thioacetate In ethanol at 50℃; for 4h; Reflux;
100%
870-24-6

2-chloroethanamine hydrochloride

60-34-4

methylhydrazine

14478-62-7

2-(1-methylhydrazinyl)ethan-1-amine

Conditions
ConditionsYield
In neat liquid at 20℃; for 18h; Inert atmosphere;100%
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Chemistry

Molecular Structure of 2-chloroethanamine hydrochloride (CAS NO.870-24-6):

IUPAC Name: 2-chloroethanamine hydrochloride 
Empirical Formula: C2H6ClN
Molecular Weight: 79.5287
H bond acceptors: 1
H bond donors: 2
Freely Rotating Bonds: 2
Polar Surface Area: 3.24 Å2
Index of Refraction: 1.427
Molar Refractivity: 19.69 cm3
Molar Volume: 76.6 cm3
Surface Tension: 29.9 dyne/cm
Density: 1.038 g/cm3
Flash Point: 19.7 °C
Enthalpy of Vaporization: 34.77 kJ/mol
Boiling Point: 108.9 °C at 760 mmHg
Vapour Pressure: 25.3 mmHg at 25°C
CAS Registry Number: 870-24-6
EINECS: 212-793-2
Melting point: 140-150 oC
Water solubility: Soluble
Sensitive: Hygroscopic
InChI
InChI=1/C2H6ClN.ClH/c3-1-2-4;/h1-2,4H2;1H
Smiles
C(C[NH3+])Cl.[ClH-]
Product Categories: omega-Functional Alkanols, Carboxylic Acids, Amines & Halides; omega-Haloalkylamines

Toxicity Data With Reference

1.    

mmo-sat 8600 µmol/L

    ENMUDM    Environmental Mutagenesis. 3 (1981),11.
2.    

mmo-esc 8600 µmol/L

    ENMUDM    Environmental Mutagenesis. 3 (1981),11.
3.    

dns-rat:lvr 100 µmol/L

    ENMUDM    Environmental Mutagenesis. 3 (1981),11.
4.    

ipr-mus LD50:2204 mg/kg

    JPETAB    Journal of Pharmacology and Experimental Therapeutics. 94 (1948),249.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Moderately toxic by intraperitoneal route. Mutation data reported. Explosive reaction with concentrated alkali above 50°C. When heated to decomposition it emits toxic fumes of Cl, NH3, and NOx.
Hazard Codes: IrritantXi
Risk Statements: 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36-37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
RIDADR: UN3261
WGK Germany: 3
RTECS: KR1800000
F: 3-10-34
HazardClass: 8
PackingGroup: III
HS Code: 29211980

Specification

  2-Chloroethylamine hydrochloride , with CAS number of 870-24-6, can be called Ethanamine,2-chloro-, hydrochloride (9CI) ; 1-Amino-2-chloroethane hydrochloride ; 2-Aminoethyl chloridehydrochloride ; 2-Chloroethylamine hydrochloride ; 2-Chloroethylamine monohydrochloride . It is a white to light beige crystalline powder.