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941678-49-5

Basic Information
CAS No.: 941678-49-5
Name: Ruxolitinib
Article Data: 13
Molecular Structure:
Molecular Structure of 941678-49-5 (Ruxolitinib)
Formula: C17H18N6
Molecular Weight: 306.37
Synonyms: Ruxolitinib;
EINECS: 1312995-182-4
Density: 1.40g/cm3
PSA: 83.18000
LogP: 3.46638
Synthetic route
1146629-80-2

(R)-(4-(1-(2-cyano-1-cyclopentylethyl)-1H-pyrazol-4-yl)-7H-pyrrolo[2,3-d]pyrimidin-7-yl)methyl pivalate

941678-49-5

ruxolitinib

Conditions
ConditionsYield
With water; sodium hydroxide In methanol at 20℃; Product distribution / selectivity;100%
With sodium hydroxide; water In methanol at 20℃; for 15h;
941685-40-1

(3R)-3-cyclopentyl-3-[4-(7-[2-(trimethylsilyl)ethoxy]methyl-7H-pyrrolo[2,3-d]-pyrimidin-4-yl)-1H-pyrazol-1-yl]propanenitrile

941678-49-5

ruxolitinib

Conditions
ConditionsYield
Stage #1: (3R)-3-cyclopentyl-3-[4-(7-[2-(trimethylsilyl)ethoxy]methyl-7H-pyrrolo[2,3-d]-pyrimidin-4-yl)-1H-pyrazol-1-yl]propanenitrile With boron trifluoride diethyl etherate In acetonitrile at 60 - 70℃; for 5h;
Stage #2: With ammonium hydroxide; water In acetonitrile at 20℃; for 12h;
92.1%
Stage #1: (3R)-3-cyclopentyl-3-[4-(7-[2-(trimethylsilyl)ethoxy]methyl-7H-pyrrolo[2,3-d]-pyrimidin-4-yl)-1H-pyrazol-1-yl]propanenitrile With lithium tetrafluoroborate; water In acetonitrile Inert atmosphere; Reflux;
Stage #2: With ammonia; water at 5 - 20℃; pH=9 - 10; Inert atmosphere; optical yield given as %ee;
84%
With trifluoroacetic acid In dichloromethane for 6h;58%

(R)-3-(4-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)-1H-pyrazol-1-yl)-3-cyclopentylpropionamide

941678-49-5

ruxolitinib

Conditions
ConditionsYield
With trichlorophosphate In 1-methyl-pyrrolidin-2-one; dichloromethane at 20 - 30℃; for 3h;77.3%
1146629-84-6

(3R)-3-cyclopentyl-3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl]propanenitrile

3680-69-1

4-chloro-1H-pyrrolo[2,3-d]pyrimidine

941678-49-5

ruxolitinib

Conditions
ConditionsYield
With potassium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane; water at 20 - 95℃; Product distribution / selectivity; Inert atmosphere;64.3%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 100℃; for 21h; Suzuki coupling; Inert atmosphere;
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate In 1,4-dioxane; water at 120℃; for 24h; Inert atmosphere;0.84 g

(R)-3-(4-(6-amino-5-(2,2-dimethoxyethyl)pyrimidin-4-yl)-1H- pyrazol-1-yl)-3-cyclopentylpropanenitrile

941678-49-5

ruxolitinib

Conditions
ConditionsYield
With trifluoroacetic acid; trifluoroacetic anhydride In toluene at 100℃; for 1h;61%
941685-40-1

(3R)-3-cyclopentyl-3-[4-(7-[2-(trimethylsilyl)ethoxy]methyl-7H-pyrrolo[2,3-d]-pyrimidin-4-yl)-1H-pyrazol-1-yl]propanenitrile

A

941678-49-5

ruxolitinib

B

1236033-03-6

C18H20N6O

Conditions
ConditionsYield
With lithium tetrafluoroborate; water In acetonitrile Inert atmosphere; Reflux;
With lithium tetrafluoroborate; water In acetonitrile at 12 - 80℃;
1146629-83-5

(R)-3-(4-bromo-1H-pyrazol-1-yl)-3-cyclopentylpropanecarbonitrile

941678-49-5

ruxolitinib

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / dimethyl sulfoxide / 24 h / 20 - 90 °C / Inert atmosphere
2: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / 1,4-dioxane; water / 24 h / 120 °C / Inert atmosphere
View Scheme
Multi-step reaction with 3 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 1 h / -15 - 5 °C / Inert atmosphere
1.2: -5 - 5 °C / Inert atmosphere
2.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / 50 - 60 °C / Inert atmosphere
3.1: hydrogenchloride / tetrahydrofuran; water / 20 °C / Reflux
View Scheme
1236033-03-6

C18H20N6O

941678-49-5

ruxolitinib

Conditions
ConditionsYield
With ammonia; water In acetonitrile at 0 - 20℃; Product distribution / selectivity;n/a
941685-27-4

4-(1H-pyrazol-4-yl)-7-((2-(trimethylsilyl)ethoxy)methyl)-7H-pyrrolo[2,3-d]pyrimidine

941678-49-5

ruxolitinib

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C
2: ethanol; hexane / Resolution of racemate
3: trifluoroacetic acid / dichloromethane / 6 h
View Scheme
Multi-step reaction with 3 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C
2: Resolution of racemate
3: trifluoroacetic acid / dichloromethane / 6 h
View Scheme
Multi-step reaction with 4 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 26 h / 60 - 80 °C / Inert atmosphere
2: acetonitrile; tetrahydrofuran; acetone / 50 - 80 °C / Large scale
3: sodium hydroxide / ethyl acetate; water / 0 °C
4: lithium tetrafluoroborate / acetonitrile; water / 11 h / 0.8 - 27 °C
View Scheme
591769-05-0

3-cyclopentaneacrylonitrile

941678-49-5

ruxolitinib

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C
2: ethanol; hexane / Resolution of racemate
3: trifluoroacetic acid / dichloromethane / 6 h
View Scheme
Multi-step reaction with 3 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C
2: Resolution of racemate
3: trifluoroacetic acid / dichloromethane / 6 h
View Scheme
Multi-step reaction with 4 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 26 h / 60 - 80 °C / Inert atmosphere
2: acetonitrile; tetrahydrofuran; acetone / 50 - 80 °C / Large scale
3: sodium hydroxide / ethyl acetate; water / 0 °C
4: lithium tetrafluoroborate / acetonitrile; water / 11 h / 0.8 - 27 °C
View Scheme
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    Name: Ruxolitinib Synonyms: (betar)-beta-cyclopentyl-4-(7h-pyrrolo(2,3-d)pyrimidin-4-yl)-1h-pyrazole-1-propanenitrile CAS:941678-49-5 MF: C17H18N6 Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kg

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    Tel:027-84306245

    Address:Wuhan Private Science and Technology Park , Wuhan, China

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  • Ruxolitinib

  • Casno:

    941678-49-5

    Ruxolitinib

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

    The company is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds,

  •  Henan Wentao Chemical Product Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-370-2722992

    Address:32 Room, 5th Floor, Building 11, No. 6 Yinxing Road, High-tech Industrial Development Zone, Zhengzhou City, Henan Province

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  • INCB018424

  • Casno:

    941678-49-5

    INCB018424

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

    Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

    Shandong Hanjiang Chemical Co., Ltd. is located in Zibo City, Shandong Province, China. It is a biotechnology enterprise engaged in the R&D, production and sales of drugs, steroids

  •  Shandong Hanjiang Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 18369939125

    Address:No.25A Qilu Industrial Park

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  • 99%  Ruxolitinib ,CAS941678-49-5

  • Casno:

    941678-49-5

    99% Ruxolitinib ,CAS941678-49-5

    Min.Order: 100 Kilogram

    FOB Price:  USD $ 0.0-0.0

    Superiority We can customize and synthesize products that other suppliers may not be able to provide. 1. best service, high quality and reasonable way for his produccts from many recent effective packing way.best s

    Changchun Artel Import and Export Trade Co., Ltd. is located in Changchun City, Jilin Province. It is a high-tech modern private enterprise specializing in the research, developme

  •  Changchun Artel lmport and Export trade company

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-0431-80543058

    Address:Dianshi Plazza,Chaoyang District

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  • ruxolitinib 941678-49-5

  • Casno:

    941678-49-5

    ruxolitinib 941678-49-5

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 10.0-10.0

    Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:As customer request Port:Qingda

    Triumph International Development Limilted is engaged in the API, pharmaceutical intermediates research and developmen.Adhering to the "customer first" business philosophy,we suppl

  •  Triumph International Development Limilted

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-536-7971999

    Address:Yinhai Road,Shouguang

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  • Factory supply Ruxolitinib powder with best price

  • Casno:

    941678-49-5

    Factory supply Ruxolitinib powder with best price

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Q1: Are you a manufacturer?Answer: Yes, we are factory founded on 2002. Q2: How to contact with us?Click "contact supplier" And then send us message the product you interest in, you will get reply within 12 hours. Q3:Which kind of payment terms do yo

    DB Biotech co., ltd is a global and professional supplier for plant extracts and functional ingredients, the company is based in XI’an city, which is famous city for the producttio

  •  DB BIOTECH CO., LTD

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86--1829 2989 553

    Address:No.99 Road, Xi'an, China

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  • High Purity Ruxolitinib CAS 941678-49-5 with Fast Shipment

  • Casno:

    941678-49-5

    High Purity Ruxolitinib CAS 941678-49-5 with Fast Shipment

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 3.0-5.0

    Hubei Yuanmeng Biological Technology Co., Ltd., which is located in Wuhan, China. We are specializing in the exportation of APIs, and plant extracts ect. Our products has been exported to America, Australia, Brazil, the Europe, Middle East and other

    Hubei Yuanmeng Biological Technology Co., Ltd., which is located in Wuhan, China. We are specializing in the exportation of APIs, and plant extracts ect. Our products has been exp

  •  Hubei Yuanmeng Biological Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-027-68897569

    Address:Hongshan District

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  • Ruxolitinib 941678-49-5

  • Casno:

    941678-49-5

    Ruxolitinib 941678-49-5

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-

    Taizhou Crene Biotechnology Co., Ltd.is a leading supplier of active pharmaceutical ingredients (APIs), with GLP labs and GMP manufacturing facilities engaging in organic synthesis

  •  Taizhou Crene Biotechnology co.ltd

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-576-88813233 88205808

    Address:Economic Developed Zone of Taizhou Zhejiang China

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  • Ruxolitinib CAS 941678-49-5

  • Casno:

    941678-49-5

    Ruxolitinib CAS 941678-49-5

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 10.0-50.0

    Ruxolitinib CAS 941678-49-5 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality control sys

    Hefei Zhaobo Technology Co.,Ltd is a professional manufacturer which integrate research and development, production and sales of chemical products in Hefei, China. Our former facto

  •  Hefei Zhaobo Technology Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+8619322001456

    Address:No. 18, 1st Floor, Zhonglv Plaza, Intersection of Zhanqian Road and Tongling Road, Yaohai District, Hefei City, Anhui Province

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  • RUXOLITINIB

  • Casno:

    941678-49-5

    RUXOLITINIB

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

    AFINE CHEMICALS LIMITED is specialized in the fine chemicals and pharmaceuticals and we have enjoyed great popularity in world markets. Since 2005, we have been rapidly growing to

  •  Afine Chemicals Limited

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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  • Ruxolitinib

  • Casno:

    941678-49-5

    Ruxolitinib

    Min.Order: 100 Gram

    FOB Price:  USD $ 1.0-1.0

    We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to provide excellence in researching, manufacturing and drug discovery process. Our research team of scienti

    ACHIEVER SYSTEAM BIOCHEM CO., LTD. is one of the professional suppliers in Chinese pharmaceutical market and is specialized in custom synthesis, chemical/pharmaceutical/ pesticides

  •  ACHIEVER SYSTEAM BIOCHEM CO., LTD.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-021-58380978

    Address:Building 87,Lane 669, Dong Jing Road Shanghai,P.R.China

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  • Ruxolitinib

  • Casno:

    941678-49-5

    Ruxolitinib

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    1. Product advantages: exquisite appearance and unique functions. 2. Product Advantages: Our products are the best,fast speed ,in large stock 3. High-quality products and thoughtful service are your greatest satisfaction. 4. The product

    Shanghai Hope Chem Co., Ltd. was founded in 2014 with registered capital of RMB 2 million Yuan. Our company is specialized in the researching, discovering and manufacturing of new

  •  Shanghai Hope Chem Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-21-58090396-805

    Address:Floor 4, Building 5, No.588 Tianxiong Road, Zhoupu International Medical Zone, ShangHai, China

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  • (R)-3-(4-(7H-Pyrrolo[2,3-d]pyrimidin-4-yl)-1H-pyrazol-1-yl)-3-cyclopentylpropanenitrile

  • Casno:

    941678-49-5

    (R)-3-(4-(7H-Pyrrolo[2,3-d]pyrimidin-4-yl)-1H-pyrazol-1-yl)-3-cyclopentylpropanenitrile

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

    J&H Chemical is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other

  •  Hangzhou J&H Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

       Inquiry Now

  • Ruxolitinib/High quality/Best price

  • Casno:

    941678-49-5

    Ruxolitinib/High quality/Best price

    Min.Order: 1 Gram

    FOB Price:  USD $ 1.0-1.0

    Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

    Shanghai Massive Chemical Technology Co., Ltd. is engaged in development, production and marketing Specialty Chemicals to satisfy the changing needs of the chemical industry. We sp

  •  Shanghai Massive Chemical Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 21 34943721

    Address:Room 435, 4th floor, Building 9, No. 2568 Gudai Road,Minhang District, Shanghai,

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  • High purity Ruxolitinib

  • Casno:

    941678-49-5

    High purity Ruxolitinib

    Min.Order: 10 Gram

    FOB Price:  USD $ 100.0-100.0

    Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

    Hangyu Biotech is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and O

  •  Zibo Hangyu Biotechnology Development Co., Ltd

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-15965530500

    Address:Room1701, Tianxing Building,Licheng district, jinan, Shandong, China

       Inquiry Now

  • INCB018424

  • Casno:

    941678-49-5

    INCB018424

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    INCB018424Appearance:White or Almost White crystalline powder Storage:Store in refrigerator Package:according to customers' requirements Application:Steroids injection For Body building Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by s

    Established in 2010, located in Hangzhou Qinglan science park, lingruichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various

  •  Hangzhou Lingrui Chemical Co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:86 571-88092529

    Address:201-B 2# Building Qinglan science park, 321# JinPeng Str. Xihu District Hangzhou City, PR.CHINA

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