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| CAS No.: | 10025-82-8 |
|---|---|
| Name: | Indium chloride |
| Article Data: | 81 |
| Molecular Structure: | |
|
|
|
| Formula: | InCl3 |
| Molecular Weight: | 221.179 |
| Synonyms: | Indium trichloride;Indium(III) chloride;Trichloroindium;Indium(Ⅲ)chloride; |
| EINECS: | 233-043-0 |
| Density: | 3.46 g/mL at 25 °C(lit.) |
| Melting Point: | 262 °C (dec.)(lit.) |
| Boiling Point: | 300 °C |
| Flash Point: | 300°C subl. |
| Solubility: | reacts with water |
| Appearance: | white crystalline powder |
| Hazard Symbols: |
 C
|
| Risk Codes: | 36/37/38-34-29-22 |
| Safety: | 26-36/37/39-45 |
| Transport Information: | UN 3260 8/PG 2 |
| PSA: | 0.00000 |
| LogP: | 2.06850 |
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| Conditions | Yield |
|---|---|
| In neat (no solvent) Kinetics; heating from 550 to 750°C; | |
| In neat (no solvent) on In2O3 surface; not isolated, detd. by thermal desorption (20-650°C) and mass spectroscopy; |
| Conditions | Yield |
|---|---|
| In neat (no solvent) 300°C;; | |
| In neat (no solvent) 300°C;; |
| Conditions | Yield |
|---|---|
| In neat (no solvent) 300°C;; | |
| In neat (no solvent) 300°C;; |
- 10026-04-7, 53609-55-5
tetrachlorosilane
A
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silica gel
B
- 10025-82-8
indium(III) chloride
| Conditions | Yield |
|---|---|
| 780-800°C in vac.; Two-fold vacuum sublimation with prior distilling off SiCl4.; |
| Conditions | Yield |
|---|---|
| 450°C;; | |
| In neat (no solvent) chlorination of In2O3 with CCl4 at ca 450°C; | |
| In not given react. of In2O3 with CCl4; |
| Conditions | Yield |
|---|---|
| In gas Kinetics; flow method (600 - 800°C, 5 - 50 vol.% SnCl4, 20 - 120 min); |
| Conditions | Yield |
|---|---|
| With tin(IV) chloride In neat (no solvent) byproducts: O2; chlorination of equimolar mixt. of In2O3 by Cl2/SnCl4 mixt. (4 vol % SnCl4, const. temp. in range 550-700°C, 60 min); chem. anal.; |
| Conditions | Yield |
|---|---|
| With pyrographite heating in dry flow of Cl2; | |
| In neat (no solvent) Kinetics; byproducts: O2; heating to 700°C; |
| Conditions | Yield |
|---|---|
| Cl2/Ar mixt. flowing over In2O3 (const. temp. in range 500-700°C,gas flow rate 2ml/min, complete satn. of carrier gas by vapours of gase ous products, duration 3 h); monitoring by gravimetric and chem. anal.; |
- 7782-50-5
chlorine
A
- 27693-84-1, 21563-01-9
In2Cl6
B
- 10025-82-8
indium(III) chloride
C
- 7646-78-8
tin(IV) chloride
| Conditions | Yield |
|---|---|
| In neat (no solvent) Kinetics; byproducts: O2; chlorination of equimolar mixt. of In2O3/SnO2 at const. temp. in range 500-700°C (Cl2 flow 100 ml/min); chem. anal.; | |
| With sulfur dioxide In neat (no solvent) Kinetics; byproducts: O2, SO3, In2(SO4)3; chlorination of equimolar mixt. of In2O3/SnO2 at const. temp. in range 500-700°C (Cl2/SO2 flow 100 ml/min); chem. anal.; |
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Chemistry
Molecular Formula: InCl3
Molecular Weight: 221.18g/mol
Mol File: 10025-82-8.mol
Einecs: 233-043-0
Appearance: White flakes
Melting Point: 586 °C
Boiling point: 800 °C
Flash Point: 300 °C subl
Density: 3.46 g/mL at 25 °C(lit.)
Water Solubility: Reacts
Sensitive: Hygroscopic
Structure of Indium trichloride (CAS NO.10025-82-8):
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IUPAC Name: Trichloroindigane
Canonical SMILES: Cl[In](Cl)Cl
InChI: InChI=1S/3ClH.In/h3*1H;/q;;;+3/p-3
InChIKey: PSCMQHVBLHHWTO-UHFFFAOYSA-K
Product Categories of Indium trichloride(CAS NO.10025-82-8): Inorganics ; Catalysis and Inorganic Chemistry ; Chemical Synthesis ; Crystal Grade Inorganics ; Indium Salts ; IndiumMetal and Ceramic Science ;Salts;Indium .
Uses
Indium trichloride (CAS NO.10025-82-8) is a lewis acid catalyst in organic reactions such as Friedel-Crafts acylations and Diels-Alder reactions,and it's also the imporant materials to manufacture other indium salt.
Production
Indium trichloride (CAS NO.10025-82-8) will be placed in dry metal quartz tube, which leads to a fully dry chlorine gas, heated to 150 to 300 ° C for the reactions to produce a shiny sheet metal indium trichloride, 600 ° C sublimation, the sublimation process which leads to a small amount of chlorine-containing nitrogen or carbon dioxide flow, which leads to non-final chlorine carbon dioxide, obtained by cooling. Two by three indium chloride and hydrogen chloride at 100 ° C reaction progressive derived. Four hydration from hydrochloric acid-soluble metal indium obtained after crystallization.
Toxicity Data With Reference
| Organism | Test Type | Route | Reported Dose (Normalized Dose) | Effect | Source |
|---|---|---|---|---|---|
| mouse | LD50 | intraperitoneal | 4950ug/kg (4.95mg/kg) | Comptes Rendus Hebdomadaires des Seances, Academie des Sciences. Vol. 256, Pg. 1043, 1963. | |
| mouse | LD50 | intravenous | 11900ug/kg (11.9mg/kg) | Drugs in Japan Vol. -, Pg. 136, 1990. | |
| mouse | LDLo | subcutaneous | 60mg/kg (60mg/kg) | Environmental Quality and Safety, Supplement. Vol. 1, Pg. 1, 1975. | |
| rabbit | LDLo | intravenous | 640ug/kg (0.64mg/kg) | Environmental Quality and Safety, Supplement. Vol. 1, Pg. 1, 1975. | |
| rabbit | LDLo | subcutaneous | 2mg/kg (2mg/kg) | Gigiena i Sanitariya. For English translation, see HYSAAV. Vol. 30(10), Pg. 28, 1965. | |
| rat | LD50 | intraperitoneal | 2370ug/kg (2.37mg/kg) | Drugs in Japan Vol. -, Pg. 136, 1990. | |
| rat | LD50 | intravenous | 4460ug/kg (4.46mg/kg) | Drugs in Japan Vol. -, Pg. 136, 1990. | |
| rat | LDLo | subcutaneous | 10mg/kg (10mg/kg) | SENSE ORGANS AND SPECIAL SENSES: OTHER CHANGES: OLFACTION SKIN AND APPENDAGES (SKIN): HAIR: OTHER | Journal of Industrial Hygiene and Toxicology. Vol. 24, Pg. 243, 1942. |
Consensus Reports
Reported in EPA TSCA Inventory.
Safety Profile
A poison by subcutaneous, intraperitoneal, and intravenous routes. Mutation data reported. When heated to decomposition it emits toxic fumes of Cl−. See also INDIUM.
Hazard Codes of Indium trichloride (CAS NO.10025-82-8): C .gif){kind=small}
Risk Statements: 36/37/38-34-29-22
36: Irritating to the eyes
37: Irritating to the respiratory system
38: Irritating to the skin
34: Causes burns
29: Contact with water liberates toxic gas
22: Harmful if swallowed
Safety Statements: 26-36/37/39-45
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
37: Wear suitable gloves
39: Wear eye/face protection
45: In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
Specification
Indium trichloride , its cas register number is 10025-82-8. It also can be called Indium trichloride ; Indium (III) chloride ; and Indium In 111 Chloride .