30120-58-2Relevant articles and documents
Synthesis of aminopyrazoles from α- oxoketene O,N-acetals using Montmorillonite K-10/Ultrasound
Braibante, Mara E. F.,Braibante, Hugo T. S.,Da Roza, Juliano K.,Henriques, Danielle M.,De Carvalho Tavares, Luciana
, p. 1160 - 1162 (2003)
5(3)-Amino-3(5) phenylpyrazoles 3a-f have been conveniently prepared by condensation of α-oxoketene O,N-acetals 2a-g with hydrazine using montmorillonite K-10 as solid support under sonication.
A facile one-pot synthesis of novel substituted 1,2,3,4- tetrahydropyrimidines part 5 [1]: Synthesis of bis[(1-alkyl/aralkyl)-5-benzoyl- 6-methylthio-1,2,3,4-tetrahydropyrimidinyl]alkane and benzene, bis[3-phenyl-7-methyl-4,5,6,7-tetrahydropyrazolo[3,4-d]
Dutta, Milan Ch.,Chanda, Kaushik,Helissey, Philippe,Vishwakarma, Jai N.
, p. 975 - 978 (2007/10/03)
Bis-1,2,3,4-tetrahydropyrimidinylalkanes/benzenes 2a-f have been synthesized by the reaction of N,S-acetals with formaldehyde and diamines. Reaction of pyrazoles 3a and 3b with diamines and formaldehyde yield bis-4,5,6,7-tetrahydropyrazolo[3,4-d]pyrimidin
Synthesis of N-alkylated derivatives of pyrazolo[1,5-a]-pyrimidine and their reaction with methylamine
Danagulyan,Panosyan,Boyakhchyan
, p. 581 - 585 (2007/10/03)
With the object of studying the factors influencing the course of enamine rearrangements, we have carried out the N-alkylation of alkyl- and aryl-substituted pyrazolo[1,5-a]pyrimidines. Using the NOEDIF NMR spectroscopic method for the cases of 5,7-dimeth
NITROAZINES. 15. CONTRACTION OF THE PYRIMIDINE RING IN 6-NITROAZOLOPYRIMIDINES
Rusinov, V. L.,Myasnikov, A. V.,Chupakhin, O. N.,Aleksandrov, G. G.
, p. 530 - 533 (2007/10/02)
It is shown that contraction of the pyrimidine ring occurs when 6-nitro-7-oxo-4,7-dihydroazolopyrimidines are heated with hydrazine hydrate.Complexes of 4-nitropyrazole with 5-aminoazoles, the structures of which were proved by x-ray diffraction analysis, are formed in a similar reaction of nitrosubstituted azolopyrimidines that do not contain an oxo function.
Reaction of Polarized Keten S,N-Acetals with Hydrazine: A Facile General Route to 3(5)-Substitutedamino-4,5(3)-substitutedpyrazoles
Vishwakarma, J. N.,Chowdhury, B. K. Roy,Ila, H.,Junjappa, H.
, p. 472 - 476 (2007/10/02)
A convenient general route for 3(5)-aryl-5(3)-N-aryl/alkyl/benzyl/amino-1(H)-pyrazoles (2a-r) and 3(5)-amino-5(3)-arylamino-4-cyano/aryl-pyrazoles (5a-c) has been developed involving the reaction of respective polarized keten S,N-acetals with hydrazine hy