32089-78-4Relevant articles and documents
Method for synthesizing 2-benzamido-3-aryl acrylate
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Paragraph 0016, (2017/07/07)
The invention discloses a method for preparing 2-benzamido-3-aryl acrylate, and belongs to the field of organic chemical synthesis. The method is mainly implemented by the following steps: adding aromatic aldehyde, ethylhippurate, acetic anhydride and an alkali catalyst into a three-mouth flask according to a certain proportion under the protection of argon, and performing condensation reaction under a certain temperature condition to obtain a 2-benzamido-3-aryl acrylate compound by one step. According to the method, production steps are shortened, the method is easy to operate and control, the production operation environment is improved, the yield and the quality of a product are improved, and the reaction time is shortened; the 2-benzamido-3-aryl acrylate is mainly used for evaluation of the activity of a chiral ligand and catalyst thereof, medicinal synthesis, a pesticide, a photoelectric material and the like.
One flask synthesis of esters of the corresponding 3-substituted 2-benzoylamino acrylic acids using 2-oxazolin-5-ones as synthons
Ahmed, Md. Mizanur,Borthakur, Somadrita,Tripathy, Pradeep K.
, p. 371 - 372 (2019/01/21)
A modified route for the fast and facile synthesis of an alkyl 3-substituted 2- benzoylamino acrylate (4) is hereby developed. All the required steps are carried out in the same flask.
STUDIES ON ORGANOPHOSPHORUS COMPOUNDS; PART IX. THA ACTION OF Di-, TRIALKYL PHOSPHITES AND THIOL ACIDS ON SOME ENAMINOLACTONES
Shabana, R.,Sidky, M. M.,El-Kateb, A. A.,Soliman, F. M.
, p. 57 - 62 (2007/10/02)
Di-, and trimethylphosphites react with enaminolactone, 4, only in methanol to give N-benzoyl-3-phenyl-3-phosphonoalanine-trimethylester (7) in good yields.Diphenylphosphinodithioic acid also reacts with 4 to give N-benzoyl-3-phenylcysteine-methyl ester-d