4265-49-0Relevant articles and documents
Solvent-free mechanochemical synthesis of bisthioglycolic acid derivatives: an efficient and versatile strategy for carbon–sulfur bond formation
Bhargava, Gaurav,Kumar, Rupesh,Naikoo, Rayees Ahmad,Singh, Parvesh
, (2021/10/07)
An eco-friendly, easily achievable and efficient strategy has been explored to synthesize functionalized bisthioglycolic acids using a variety of aldehydes and thioglycolic acid. The employed protocol is solvent free and provides the desirable products in
Syntheses of some novel and symmetrical bis(4-amino-4H-1,2,4-triazole-3- thiols)
Ebrahimi, Sattar,Sayadi, Masoomeh
, p. 647 - 652 (2013/02/22)
A series of bis(4-amino-4H-1,2,4-triazole-3-thiols) 3a-e were prepared by condensation reactions of 2,2-(phenylmethylene)bis(sulfanediyl)diacetic acids 2a-e with thiocarbohydrazide. The starting diacid 2a-e was prepared by reactions of aromatic aldehydes
SYNTHESIS, SPECTRAL STUDIES AND C-S BOND FISSION THROUGH PUMMERER REACTION OF SOME ALKYLDIACETATES
Gohar, Gamal A.
, p. 171 - 178 (2007/10/02)
A series of methyl and ethyldiacetates have been synthesized and their structures were identified.Correlation between δ-values of the benzylidene protons and ?-Hammett values has been found.The internal chemical shift Δν of the methylene protons was found to be correlated linearly with ?-Hammett constants indicating that the sulfur atom could transmit a polar effect to the substituent.Studies of H2O2 oxidation suggested that a competition between Pummerer and elimination reactions of the intermediate was involved. Key words: Benzylidene dithio diacetates; (1)HNMR spectra; Pummerer reaction
142. Praeparative chromatographische Enantiomerentrennung von synthetisch nuetzlichen cyclischen Acetalen
Seebach, Dieter,Mueller, Stefan G.,Gysel, Urs,Zimmermann, Juerg
, p. 1303 - 1318 (2007/10/02)
Preparative Chromatographic Resolution of Sunthetically Useful Cyclic Acetals Racemic cyclic acetals derived from aldehydes and glycine, glycolic acid, thioglycolic acid, formylacetic acid, and acetoacetic acid (oxazolidinones 4-13, dioxolanones 14,15, ox