552857-10-0

Basic information

• Product Name: 2-bromo-N-phenyl-1-cyclohexene-1-carboxamide
• Synonyms: 2-bromo-N-phenyl-1-cyclohexene-1-carboxamide
• CAS NO: 552857-10-0
• Molecular Weight: 280.164
• Mol File: 552857-10-0.mol
• Article Data: 2

Chemical Properties

• CAS DataBase Reference: 2-bromo-N-phenyl-1-cyclohexene-1-carboxamide(CAS DataBase Reference)
• NIST Chemistry Reference: 2-bromo-N-phenyl-1-cyclohexene-1-carboxamide(552857-10-0)
• EPA Substance Registry System: 2-bromo-N-phenyl-1-cyclohexene-1-carboxamide(552857-10-0)

Safety Data

• Hazardous Substances Data: 552857-10-0(Hazardous Substances Data)

Upstream product

• 68965-62-8 2-bromocyclohex-1-enecarboxylic acid 
• 62-53-3 aniline 
• 159389-47-6 2-bromo-1-cyclohexene-1-carbonyl chloride 
• 38127-47-8 2-bromocyclohex-1-ene-1-carbaldehyde 
• 108-94-1 cyclohexanone 
• 72422-64-1 2-bromocyclohex-1-ene-1-carboxylic acid methyl ester 

Downstream Products

• 34127-13-4 2-phenyl-5,6,7,8-tetrahydronquinazolin-4(3H)-one 
• 52850-98-3 5-methyl-7,8,9,10-tetrahydrophenanthridin-6(5H)-one 
• 552857-08-6 2-bromo-N-methyl-N-phenyl-1-cyclohexene-1-carboxamide 

Relevant articles and documents

Concise synthesis of tetrahydrophenanthridone by palladium reagent

Heck reaction of N-(2-halophenyl)-N-methyl-1-cyclohexene-1carboxamide (1) and 2-bromo-N-methyl-N-phenyl-1-cyclohexene-1-carboxamide (4) using a palladium reagent under several reaction conditions was examined. Reaction of 4 using Pd(OAc)2, DPPP, and Bu3P afforded tetrahydrophenanthridone (5) in excellent yield.