Heterocycles p. 541 - 546 (2003)
Update date:2022-07-29
Topics:
Harayama, Takashi
Toko, Hiroko
Nishioka, Hiromi
Abe, Hitoshi
Takeuchi, Yasuo
Heck reaction of N-(2-halophenyl)-N-methyl-1-cyclohexene-1carboxamide (1) and 2-bromo-N-methyl-N-phenyl-1-cyclohexene-1-carboxamide (4) using a palladium reagent under several reaction conditions was examined. Reaction of 4 using Pd(OAc)2, DPPP, and Bu3P afforded tetrahydrophenanthridone (5) in excellent yield.
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(2002)
