56975-77-0Relevant academic research and scientific papers
One-pot synthesis of sulfonylhydrazones from sulfonyl chloride, hydrazine hydrate and vinyl azide in water
Luo, Mengqiang,Wang, Hai,Ren, Xiaorong,Lu, Ruijuan,Qi, Chenze,Zhang, Yaohong,Shen, Runpu
, p. 2713 - 2722 (2021/03/19)
A facile and eco-friendly protocol for the synthesis of sulfonylhydrazones from sulfonyl chlorides, hydrazine hydrate and vinyl azides was developed. The unique advantage of this approach is that desired products can be obtained efficiently in water, which meets the requirements of green chemistry and provides good perspectives for the sustainable production of new drug candidate. Also, this reaction proceeded in moderate to good yields with a wide tolerance of functional groups.
A Green Synthesis and Antibacterial Activity of N-Arylsulfonylhydrazone Compounds
Yang, Qian,Hao, Wangwang,He, Yangqing,Zhang, Qian,Yu, Xiaojiao,Hua, Yaobing
, p. 152 - 156 (2020/01/28)
A green method has been developed for the synthesis of N-arylsulfonylhydrazones via a simple grindstone procedure. By grinding mixtures of benzensulfonyl hydrazides and a series of aryl aldehydes or ketones in the mortar using L-tyrosine as catalyst, 24 N
Synthesis of Multi-substituted Dihydropyrazoles by Copper-Mediated [4+1] Cycloaddition Reaction of N-Sulfonylhydrazones and Sulfoxonium Ylides
Hu, Sipei,Du, Shiying,Yang, Zuguang,Ni, Lingfang,Chen, Zhengkai
supporting information, p. 3124 - 3136 (2019/05/01)
A general and expeditious approach for the copper mediated synthesis of multi-functionalized dihydropyrazoles from N-sulfonylhydrazones and sulfoxonium ylides has been achieved under aerobic oxidative conditions. The formal [4+1] cycloaddition reaction ex
Sulfonylhydrazone derivative, and preparation method and application thereof
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Paragraph 0036; 0037; 0053-0055; 0056; 0057, (2020/01/03)
The invention discloses a sulfonylhydrazone derivative, and a preparation method and application thereof. The preparation method comprises the following step of taking olefin azide and sulfonyl hydrazine as starting materials to carry out a reaction, wher
Torsional Angles in Vinylarenes Determined by High-Field NMR Spectroscopy
Facchine, Kevin L.,Staley, Stuart W.,Zijl, Peter C. M. van,Mishra, Prasanna K.,Bothner-By, Aksel A.
, p. 4900 - 4905 (2007/10/02)
High-resolution deuterium NMR spectra of styrene-α-d, styrene-d8, 1-vinylnaphthalene-α-d, and 2-vinylnaphthalene-α-d in hydrocarbon solvents were recorded at field strengths of 14.11 to 14.57 T.Quadropolar splittings were observed as a conseque
