896121-49-6Relevant articles and documents
A catechin preparation method of compound (by machine translation)
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Paragraph 0044; 0045, (2017/02/23)
The invention relates to a method for preparing a catechin compound. The method comprises the following steps: by taking 2,4,6-trihydroxy acetophenone and p-hydroxy benzaldehyde as raw materials, carrying out condensation reaction, restored deoxidation, cyclization reaction of acid catalysis, so as to obtain the catechin compound. The invention also provides a technology for producing the catechin compound. In the synthesis process of an immediate 9, reduction is carried out by using sodium borohydride which is catalyzed by a lewis acid, so that side reaction caused by double bond transfer is greatly reduced while a highly toxic reagent osmium tetroxide is replaced with hydrogen peroxide oxidation.
Synthetic methods for preparation of protected proanthocyanidin(s)
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, (2008/06/13)
A process is disclosed for the production of polyphenol oligomers having n polyphenol monomeric units, n being an integer from 2-18. The process includes coupling of a protected polyphenol, having protected phenolic hydroxyl groups, with a C-4 functionali
8+Z 8, 6+Z 6, and 6+Z 8 catechin and epicatechin dimers and methods for their preparation
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, (2008/06/13)
Novel catechin and epicatechin dimers with (8+Z 8), (6+Z 6), and (8+Z 6) linkages are prepared, as well as digallated dimers. A novel process for preparing these compounds is disclosed which involves the oxidative or reductive coupling of protected monome