Self-protonation upon the electroreduction of 2- and 4-nitrophenylhydroxylamine (cas 16169-16-7)s in aprotic media

Add time:07/20/2019    Source:sciencedirect.com

Cyclic voltammetry and controlled potential electrolysis were used to show that radical anions of 2- and 4-nitrophenylhydroxylamines electrochemically generated in a 0.1 M Bu4NClO4 solution in DMF undergo protonation with the starting compounds (self-protonation) followed by the formation of the corresponding nitroanilines.

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