Synthesis of NIOBIUM ALUMINIDE (cas 12003-75-7)s by electro-deoxidation of oxides

Add time:07/21/2019    Source:sciencedirect.com

Niobium aluminides were produced by the direct reduction of mixtures of niobium and aluminium oxides. Pellets of the mixed oxides were made the cathode in molten CaCl2 or a CaCl2–XCl melt, where X was either Na or Li. The oxygen in the pellets ionised, dissolved in the melt, and was discharged at the anode. The cathode reduced to a mixture of Nb3Al and Nb2Al which corresponded to the ratio of Nb to Al in the original oxide pellets.

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