Direct synthesis of thiophosphates by reaction of diphenylphosphine oxide with sulfonyl chlorides
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Add time:07/23/2019 Source:sciencedirect.com
A new method for the synthesis of thiophosphates by reductive coupling reaction of diphenylphosphine oxide and sulfonyl chlorides has been developed. The reaction is metal-free and needs no additives, affording various aryl and alkyl substituted thiophosphates in good to excellent yields under mild conditions.
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