Crystal structure of poly[{tris-μ-iodo-bis<(2,2′,2″-nitrilodiethoxyethanol)dilead(II)>}-μ-iodo] obtained by direct methods using Lead(II) oxide as a starting material

Add time:07/29/2019    Source:sciencedirect.com

A direct method of obtaining (Pb4I4L2)n, where L is twice deprotonated 2,2′,2″-nitrilotriethanol (triethanolamine), is reported. The crystal structure of the compound was determined by X-ray techniques. The crystallographically independent fragments of Pb4I4L2 are associated by bridging oxygen and iodine atoms in endless layers parallel to the bc-plane of the crystal. Tetradentate twice deprotonated triethanolamine is coordinated to lead(II) via oxygen and nitrogen atoms.

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