Some tetraphenylcyclobutadiene complexes of rhodium
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Add time:08/06/2019 Source:sciencedirect.com
[RhCl(PF3)2]2 (II) reacts with diphenylacetylene to give the tetraphenylcyclobutadiene complex [RhCl(C4Ph4)]2, which on treatment with thallium salts TlR (R = π-C5H5, acac, facac), afford good yields of Rh(π-C5H5)(C4Ph4), Rh(acac)(C4Ph4), and Rh(facac)(C4Ph4) respectively. The reactions of II with other alkynes are discussed.
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