1H NMR Study of the solution structure of sarafotoxin-S6b
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Add time:08/05/2019 Source:sciencedirect.com
Sarafotoxin-S6b has been synthesized and studied by 1H NMR in 5050 acetonitrile/water mixture. All spin systems were identified and assigned with the aid of 2D experiments. On the basis of these data, a 3D structure of sarafotoxin is proposed and compared to that of [Nle7]endothelin obtained in the same conditions.From this study, it appeared that sarafotoxin-S6b and [Nle7]endothelin roughly share the same 3D structure, the main differences being located in the 4–7 loop bearing the sequence variation.
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