Rapid spectrophotometric determination of vanadium(V) with 1-(2′-thiazolylazo)-2-naphthol

Add time:08/08/2019    Source:sciencedirect.com

The sparingly soluble complex formed between vanadium(V) and 4-(2-thiazolylazo)resorcinol (5) requires extraction with chloroform, whereas maximum color development for the complex with 4-(2-pyridylazo)resorcinol (4) takes place after 60 min. Heating of reactants is required in the methods with 2-(3,5-dibromo-4-methyl-2-pyridylazo)-5-diethylaminophenol (3) and 4-(2,3-dihydroxy-4-pyridylazo)benzene sulfonic acid (6), whereas absorbance of the complex with 2-methyl-4-(4-methyl-2-thiazolylazo)resorcinol (1) is measured after 30 min. Since 1-(2′-thiazolylazo)-2-naphthol (TAN) has been found to be a sensitive chromogenic reagent (2), its reaction with vanadium(V) has been studied.

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