A new strategy for the synthesis of Asp-Gly units-containing glycopeptides using Fmoc/Bzl protection

Add time:08/06/2019    Source:sciencedirect.com

The nephritogenostde peptide fragment could be successfully synthesized using the Fmoc/Bzl strategy, coupling the fully protected Asp(OBzl) fragment 3–10, produced in high purity on a 2-chlorotrityl support, to the N-terminal glycine residue of the resin-bound C-terminal segment 11–21 and thereby avoiding the highly disturbing cyclization reaction of the Asp-Gly moiety.

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