Synthesis of nortropane alkaloid calystegine B(2) (cas 127414-85-1) from methyl α-d

Add time:08/07/2019    Source:sciencedirect.com

A new synthetic route for formation of a central cycloheptanone intermediate leading to the nortropane alkaloid calystegine B2 is described. The approach installs the desired ketone functionality directly in a ring-closing metathesis step. The target compound was prepared over 10 steps from commercially available methyl α-d-xylopyranoside.

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