Photosonosynthesis of 1,2,4-tris(methylthio)-3-H-hexafluoro-n-butane

Add time:08/14/2019    Source:sciencedirect.com

The preparation of neat 1,2,4-tris(methylthio)-3-H-hexafluoro-n-butane is described. The mechanism, which involves the elimination of hydrogen fluoride with the subsequent isomerization in forming the cis- and trans- 1,2,4-tris(methylthio)hexafluoro-l-butene, is discussed. This study also supports the presence of methanethiol as an intermediate during the photosonoreaction of bis(methylthio)hexafluoro-2-butene with an excess of methyl disulfide.

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