Electrochemical reduction of o-nitrophenylthioacetic derivatives. Production of 2H-1,4-benzothiazines
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Add time:08/24/2019 Source:sciencedirect.com
Comparative studies of the electrochemical reduction of 2-(o-nitrophenylthio)-acetic acid and its methyl ester in aqueous media of different acidity show that reduction of the ester in an ammoniacal buffer is the best adapted for electrosynthesis of 4-hydroxy-2H-1,4-benzothiazin-3(4H)-one. The electrochemical behaviours of the corresponding phenylhydroxylamines and azoxy compounds are also investigated.
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