Synthesis of (S)-3-hydroxytetrahydropyran from l-glutamic acid

Add time:08/24/2019    Source:sciencedirect.com

A concise synthesis of (S)-3-hydroxytetrahydropyran from natural l-glutamic acid has been developed. The intramolecular etherification starting from 1,5-diol was promoted by trifluoromethanesulfonic anhydride. The clinnamates of the alcohols were prepared for accurately determining the optical purity by HPLC method.

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