ArticleSynthesis of 3-benzyloxy-2,2-dimethyl-propan-1-ol by hydrogenation of 5,5-dimethyl-2-phenyl-[1,3]dioxane using copper catalysts. Part II: investigations in the liquid phase

Add time:08/25/2019    Source:sciencedirect.com

The hydrogenation of 5,5-dimethyl-2-phenyl-[1,3]dioxane to 3-benzyloxy-2,2-dimethyl-propan-1-ol has been investigated within the temperature range from 150°C to 220°C over copper-loaded catalysts. Under elevated pressure in a continuous flow reactor, good results have been obtained using the catalyst system CuH-[B]-silicalite-1. The results have been compared to those obtained over two catalyst systems known in the literature, i.e. nickel oxide on silica and copper chromite.

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