Data articleSynthesis, characterization and crystal structure of 4-[(6-ethoxy benzothiazol-2-yl) diazenyl] phenyl 2-(2, 3-dihydro-1H-inden-2-yl) acetate
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Add time:09/02/2019 Source:sciencedirect.com
The title compound C26H23N3O3S was synthesized by Steglich esterification of 4-[(6-ethoxy benzothiazol-2-yl) diazenyl] phenol with Indan-2-ylacetic acid. The synthesized compound was recrystallized by slow evaporation of the saturated solution of ethanol and single crystal was selected for X-ray Diffraction study and was characterized by UV–Vis, FT-IR, 1H NMR spectroscopic techniques. A triclinic unit cell of C26H23N3O3S was diffracted for X-ray beam of wavelength 0.71075 Å generated from Mo-Kα, data were solved by SHELXL-97 and molecular and packing diagram were determined by MERCURY, from which R value obtained was 0.0613.
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