ChemistryNa2K[WN3] and Na11Rb[(WN3)4], two new alkali metal nitrido tungstates(VI) with closely related structures
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Add time:09/01/2019 Source:sciencedirect.com
Tungsten powder reacts with an excess of the respective mixtures of alkali metal amides in autoclaves above 600°C to give the quarternary alkali metal nitrido tungstates(VI) Na2K[WN3] and Na11Rb[(WN3)4] embedded in alkali metals. The nitrides were isolated by extracting the metals with liquid ammonia. The structures were determined from X-ray single crystal data. Na2K[WN3]: Pbem, (No.57), Z=8, a=6.3948(9) Å, b=11.924(3) Å, c=12.292(3) Å
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