Synthesis of α-azido aldehydes Stereoselective access to a protected lincosamine (cas 13006-69-4) analogue
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Add time:08/29/2019 Source:sciencedirect.com
Reaction of ketone 3 with dichloromethyllithium gave a unique branched-chain dichloromethyl sugar 7 whose structure was ascertained by X-ray crystallography. Transformation of 7 in seven steps, involving the key-intermediate α-azido-aldehyde 9, afforded the protected lincosamine (cas 13006-69-4) analogue 14.
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