Synthesis, Growth and Characterization of [DAMS]2[CdI4] single crystal [DAMS =4‐N, N‐dimethylamino‐N‐methyl‐stilbazolium iodide]

Add time:09/01/2019    Source:sciencedirect.com

The hybrid complex of inorganic-organic [DAMS]2[CdI4] [[DAMS =4‐N, N‐dimethylamino‐N‐methyl‐stilbazolium iodide] was synthesized by metathesization of the 4-N,N-dimethylamino -N-methyl stilbazolium iodide [DAMS.I-] salt with cadmium acetate. The [DAMS]2[CdI4] single crystals were grown by slow evaporation method using methanol as solvent. The single crystal X-ray diffraction analysis was carried out and the cell parameters a = 11.0569(3) Å, b = 12.8526(3) Å, c = 14.1427(4) Å, α = 73.7240(10)°, β = 73.9810(10)°, γ = 83.6640(10)° and Volume1853.17 (9) Å3were determined. The presence of functional groups and their corresponding vibrational modes are evaluated by FT-IR spectrum. The linear optical properties are investigated by UV-vis absorption. The melting point and thermal behavior of [DAMS] 2 [CdI4] were investigated by Thermogravimetric / Differential Thermal Analysis [TG/DTA].

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