Structural and spectroscopic study of condensed piperidine bicyclanols. 3-Phenethyl-3-azabicyclo[3.2.1]octan-8-α-ol

Add time:09/01/2019    Source:sciencedirect.com

The IR and 1H and 13C NMR spectra of 3-phenethyl-3-azabicyclo[3.2.1]octan-8-α-ol have been studied in several media, and its crystal structure has been determined by X-ray diffraction. The bicyclic system adopts a chair—envelope conformation with both OH and phenethyl groups in equatorial positions with respect to the piperidine ring. The existence of OH⋯N intermolecular hydrogen bonding in the solid state has been revealed by X-ray and IR data. The results obtained are compared with those previously found for the corresponding β-epimer.

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